MX2023007214A - Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da. - Google Patents

Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da.

Info

Publication number
MX2023007214A
MX2023007214A MX2023007214A MX2023007214A MX2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A
Authority
MX
Mexico
Prior art keywords
ammonium
byproduct
fluorosulfate
fluorosulfonyl
imide
Prior art date
Application number
MX2023007214A
Other languages
English (en)
Inventor
Bernard E Pointner
Matthew H Luly
James V Guiheen
Brian Leone
Original Assignee
Honeywell Int Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Honeywell Int Inc filed Critical Honeywell Int Inc
Publication of MX2023007214A publication Critical patent/MX2023007214A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/24Sulfates of ammonium
    • C01C1/245Preparation from compounds containing nitrogen and sulfur
    • C01C1/246Preparation from compounds containing nitrogen and sulfur from sulfur-containing ammonium compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/19Fluorine; Hydrogen fluoride
    • C01B7/191Hydrogen fluoride
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/19Fluorine; Hydrogen fluoride
    • C01B7/191Hydrogen fluoride
    • C01B7/195Separation; Purification
    • C01B7/196Separation; Purification by distillation
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/026Preparation of ammonia from inorganic compounds
    • C01C1/028Preparation of ammonia from inorganic compounds from ammonium sulfate or sulfite
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/16Halides of ammonium
    • C01C1/162Ammonium fluoride
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/28Methods of preparing ammonium salts in general
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/02Fluorides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00Sulfates or sulfites of sodium, potassium or alkali metals in general
    • C01D5/06Preparation of sulfates by double decomposition
    • C01D5/08Preparation of sulfates by double decomposition with each other or with ammonium sulfate
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/20Halides
    • C01F11/22Fluorides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/46Sulfates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Un proceso para tratar un subproducto de fluorosulfato de amonio incluye proporcionar un subproducto de fluorosulfato de amonio que incluye principalmente fluorosulfato de amonio y cantidades menores de ácido fluorosulfónico y bis(fluorosulfonil)imida, mezclar el subproducto de fluorosulfato de amonio con agua, hacer reaccionar la mezcla del subproducto de fluorosulfato de amonio y el agua a una temperatura de reacción hidrolítica para hidrolizar el fluorosulfato de amonio, el ácido fluorosulfónico y la bis(fluorosulfonil)imida para formar bisulfato de amonio y fluoruro de hidrógeno acuoso; y separar el bisulfato de amonio del fluoruro de hidrógeno acuoso.
MX2023007214A 2021-01-07 2022-01-04 Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da. MX2023007214A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US202163134883P 2021-01-07 2021-01-07
US17/554,977 US11772967B2 (en) 2021-01-07 2021-12-17 Integrated processes for treatment of an ammonium fluorosulfate byproduct of the production of bis (fluorosulfonyl) imide
PCT/US2022/070021 WO2022150808A1 (en) 2021-01-07 2022-01-04 Integrated processes for treatment of an ammonium fluorosulfate byproduct of the production of bis(fluorosulfonyl) imide

Publications (1)

Publication Number Publication Date
MX2023007214A true MX2023007214A (es) 2023-06-26

Family

ID=82219396

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2023007214A MX2023007214A (es) 2021-01-07 2022-01-04 Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da.

Country Status (7)

Country Link
US (1) US11772967B2 (es)
EP (1) EP4274807A1 (es)
JP (1) JP2024504275A (es)
KR (1) KR20230127238A (es)
CN (1) CN116783140A (es)
MX (1) MX2023007214A (es)
WO (1) WO2022150808A1 (es)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115594280A (zh) * 2022-11-08 2023-01-13 苏州淡林环境科技有限公司(Cn) 一种含氟磺酸根废水预处理工艺

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4086419A (en) 1976-02-24 1978-04-25 National Starch And Chemical Corporation Preparation of starch sulfate esters
JP5443118B2 (ja) 2009-03-31 2014-03-19 三菱マテリアル株式会社 ビス(フルオロスルホニル)イミド塩の製造方法、ビス(フルオロスルホニル)イミド塩及びフルオロ硫酸塩の製造方法、並びにビス(フルオロスルホニル)イミド・オニウム塩の製造方法
JP5527993B2 (ja) 2009-03-31 2014-06-25 三菱マテリアル株式会社 ビス(フルオロスルホニル)イミドの製造方法
WO2011111780A1 (ja) 2010-03-11 2011-09-15 三菱マテリアル株式会社 ビス(フルオロスルホニル)イミドの製造方法
JP5560136B2 (ja) 2010-08-06 2014-07-23 三菱マテリアル株式会社 ビス(フルオロスルホニル)イミドの製造方法
CN103347811B (zh) 2011-02-10 2015-08-19 日本曹达株式会社 氟磺酰亚胺铵盐的制造方法
KR101702656B1 (ko) 2011-03-03 2017-02-03 닛뽕소다 가부시키가이샤 플루오로술포닐이미드암모늄염의 제조 방법
US8377406B1 (en) 2012-08-29 2013-02-19 Boulder Ionics Corporation Synthesis of bis(fluorosulfonyl)imide
EP2920147B1 (en) 2012-11-16 2019-02-13 Trinapco, Inc Synthesis of tetrabutylammonium bis(fluorosulfonyl)imide and related salts
JP2014105115A (ja) 2012-11-22 2014-06-09 Mitsubishi Materials Corp 高純度ビス(フルオロスルホニル)イミドおよびその製造方法
US8722005B1 (en) 2013-07-26 2014-05-13 Boulder Ionics Corporation Synthesis of hydrogen bis(fluorosulfonyl)imide
FR3014439B1 (fr) 2013-12-05 2018-03-23 Rhodia Operations Procede de preparation de l'acide bis-fluorosulfonylimide et de ses sels.
KR101687374B1 (ko) 2016-06-07 2016-12-16 카보텍재료개발주식회사 디플루오로술포닐 이미드 또는 그 염의 제조 방법
CN109264682B (zh) 2017-07-18 2019-11-29 九江天赐高新材料有限公司 一种高纯度二氟磺酰亚胺的制备方法
CN107986248B (zh) 2017-11-17 2021-11-26 南京红太阳生物化学有限责任公司 一种双氟磺酰亚胺的制备方法
CN108975292A (zh) 2018-09-17 2018-12-11 九江天赐高新材料有限公司 一种双氟磺酰亚胺类化合物的制备方法
CN109264683B (zh) 2018-10-16 2021-07-27 广州理文科技有限公司 一种双(氟磺酰)亚胺的提取与纯化方法
CN109592655B (zh) 2019-01-17 2020-07-28 联化科技股份有限公司 一种催化氟化高效制备双氟磺酰亚胺的方法
US10734664B1 (en) 2019-03-01 2020-08-04 Ses Holdings Pte. Ltd. Purified hydrogen bis(fluorosulfonyl)imide (HFSI) products, methods of purifying crude HFSI, and uses of purified HFSI products
CN110436424A (zh) 2019-07-04 2019-11-12 湖南福邦新材料有限公司 一种双氟磺酰亚胺及双氟磺酰亚胺锂的制备方法
CN112340713A (zh) 2020-11-23 2021-02-09 泰兴华盛精细化工有限公司 一种双氟代磺酰亚胺的提纯方法

Also Published As

Publication number Publication date
KR20230127238A (ko) 2023-08-31
JP2024504275A (ja) 2024-01-31
CN116783140A (zh) 2023-09-19
WO2022150808A1 (en) 2022-07-14
US20220212929A1 (en) 2022-07-07
EP4274807A1 (en) 2023-11-15
US11772967B2 (en) 2023-10-03

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