MX2023007214A - Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da. - Google Patents
Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da.Info
- Publication number
- MX2023007214A MX2023007214A MX2023007214A MX2023007214A MX2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A MX 2023007214 A MX2023007214 A MX 2023007214A
- Authority
- MX
- Mexico
- Prior art keywords
- ammonium
- byproduct
- fluorosulfate
- fluorosulfonyl
- imide
- Prior art date
Links
- HRXDYOKVWGTDPD-UHFFFAOYSA-N ctk4b9193 Chemical compound [NH4+].[O-]S(F)(=O)=O HRXDYOKVWGTDPD-UHFFFAOYSA-N 0.000 title abstract 7
- 239000006227 byproduct Substances 0.000 title abstract 5
- KTQDYGVEEFGIIL-UHFFFAOYSA-N n-fluorosulfonylsulfamoyl fluoride Chemical compound FS(=O)(=O)NS(F)(=O)=O KTQDYGVEEFGIIL-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 2
- BIGPRXCJEDHCLP-UHFFFAOYSA-N ammonium bisulfate Chemical compound [NH4+].OS([O-])(=O)=O BIGPRXCJEDHCLP-UHFFFAOYSA-N 0.000 abstract 2
- UQSQSQZYBQSBJZ-UHFFFAOYSA-N fluorosulfonic acid Chemical compound OS(F)(=O)=O UQSQSQZYBQSBJZ-UHFFFAOYSA-N 0.000 abstract 2
- 229910000040 hydrogen fluoride Inorganic materials 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/24—Sulfates of ammonium
- C01C1/245—Preparation from compounds containing nitrogen and sulfur
- C01C1/246—Preparation from compounds containing nitrogen and sulfur from sulfur-containing ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
- C01B7/195—Separation; Purification
- C01B7/196—Separation; Purification by distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/026—Preparation of ammonia from inorganic compounds
- C01C1/028—Preparation of ammonia from inorganic compounds from ammonium sulfate or sulfite
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/16—Halides of ammonium
- C01C1/162—Ammonium fluoride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/28—Methods of preparing ammonium salts in general
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/02—Fluorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/06—Preparation of sulfates by double decomposition
- C01D5/08—Preparation of sulfates by double decomposition with each other or with ammonium sulfate
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/20—Halides
- C01F11/22—Fluorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/46—Sulfates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un proceso para tratar un subproducto de fluorosulfato de amonio incluye proporcionar un subproducto de fluorosulfato de amonio que incluye principalmente fluorosulfato de amonio y cantidades menores de ácido fluorosulfónico y bis(fluorosulfonil)imida, mezclar el subproducto de fluorosulfato de amonio con agua, hacer reaccionar la mezcla del subproducto de fluorosulfato de amonio y el agua a una temperatura de reacción hidrolítica para hidrolizar el fluorosulfato de amonio, el ácido fluorosulfónico y la bis(fluorosulfonil)imida para formar bisulfato de amonio y fluoruro de hidrógeno acuoso; y separar el bisulfato de amonio del fluoruro de hidrógeno acuoso.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US202163134883P | 2021-01-07 | 2021-01-07 | |
US17/554,977 US11772967B2 (en) | 2021-01-07 | 2021-12-17 | Integrated processes for treatment of an ammonium fluorosulfate byproduct of the production of bis (fluorosulfonyl) imide |
PCT/US2022/070021 WO2022150808A1 (en) | 2021-01-07 | 2022-01-04 | Integrated processes for treatment of an ammonium fluorosulfate byproduct of the production of bis(fluorosulfonyl) imide |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2023007214A true MX2023007214A (es) | 2023-06-26 |
Family
ID=82219396
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2023007214A MX2023007214A (es) | 2021-01-07 | 2022-01-04 | Procesos integrados para el tratamiento de un subproducto de fluorosulfato de amonio de la produccion de bis(fluorosulfonil)imi da. |
Country Status (7)
Country | Link |
---|---|
US (1) | US11772967B2 (es) |
EP (1) | EP4274807A1 (es) |
JP (1) | JP2024504275A (es) |
KR (1) | KR20230127238A (es) |
CN (1) | CN116783140A (es) |
MX (1) | MX2023007214A (es) |
WO (1) | WO2022150808A1 (es) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115594280A (zh) * | 2022-11-08 | 2023-01-13 | 苏州淡林环境科技有限公司(Cn) | 一种含氟磺酸根废水预处理工艺 |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4086419A (en) | 1976-02-24 | 1978-04-25 | National Starch And Chemical Corporation | Preparation of starch sulfate esters |
JP5443118B2 (ja) | 2009-03-31 | 2014-03-19 | 三菱マテリアル株式会社 | ビス(フルオロスルホニル)イミド塩の製造方法、ビス(フルオロスルホニル)イミド塩及びフルオロ硫酸塩の製造方法、並びにビス(フルオロスルホニル)イミド・オニウム塩の製造方法 |
JP5527993B2 (ja) | 2009-03-31 | 2014-06-25 | 三菱マテリアル株式会社 | ビス(フルオロスルホニル)イミドの製造方法 |
WO2011111780A1 (ja) | 2010-03-11 | 2011-09-15 | 三菱マテリアル株式会社 | ビス(フルオロスルホニル)イミドの製造方法 |
JP5560136B2 (ja) | 2010-08-06 | 2014-07-23 | 三菱マテリアル株式会社 | ビス(フルオロスルホニル)イミドの製造方法 |
CN103347811B (zh) | 2011-02-10 | 2015-08-19 | 日本曹达株式会社 | 氟磺酰亚胺铵盐的制造方法 |
KR101702656B1 (ko) | 2011-03-03 | 2017-02-03 | 닛뽕소다 가부시키가이샤 | 플루오로술포닐이미드암모늄염의 제조 방법 |
US8377406B1 (en) | 2012-08-29 | 2013-02-19 | Boulder Ionics Corporation | Synthesis of bis(fluorosulfonyl)imide |
EP2920147B1 (en) | 2012-11-16 | 2019-02-13 | Trinapco, Inc | Synthesis of tetrabutylammonium bis(fluorosulfonyl)imide and related salts |
JP2014105115A (ja) | 2012-11-22 | 2014-06-09 | Mitsubishi Materials Corp | 高純度ビス(フルオロスルホニル)イミドおよびその製造方法 |
US8722005B1 (en) | 2013-07-26 | 2014-05-13 | Boulder Ionics Corporation | Synthesis of hydrogen bis(fluorosulfonyl)imide |
FR3014439B1 (fr) | 2013-12-05 | 2018-03-23 | Rhodia Operations | Procede de preparation de l'acide bis-fluorosulfonylimide et de ses sels. |
KR101687374B1 (ko) | 2016-06-07 | 2016-12-16 | 카보텍재료개발주식회사 | 디플루오로술포닐 이미드 또는 그 염의 제조 방법 |
CN109264682B (zh) | 2017-07-18 | 2019-11-29 | 九江天赐高新材料有限公司 | 一种高纯度二氟磺酰亚胺的制备方法 |
CN107986248B (zh) | 2017-11-17 | 2021-11-26 | 南京红太阳生物化学有限责任公司 | 一种双氟磺酰亚胺的制备方法 |
CN108975292A (zh) | 2018-09-17 | 2018-12-11 | 九江天赐高新材料有限公司 | 一种双氟磺酰亚胺类化合物的制备方法 |
CN109264683B (zh) | 2018-10-16 | 2021-07-27 | 广州理文科技有限公司 | 一种双(氟磺酰)亚胺的提取与纯化方法 |
CN109592655B (zh) | 2019-01-17 | 2020-07-28 | 联化科技股份有限公司 | 一种催化氟化高效制备双氟磺酰亚胺的方法 |
US10734664B1 (en) | 2019-03-01 | 2020-08-04 | Ses Holdings Pte. Ltd. | Purified hydrogen bis(fluorosulfonyl)imide (HFSI) products, methods of purifying crude HFSI, and uses of purified HFSI products |
CN110436424A (zh) | 2019-07-04 | 2019-11-12 | 湖南福邦新材料有限公司 | 一种双氟磺酰亚胺及双氟磺酰亚胺锂的制备方法 |
CN112340713A (zh) | 2020-11-23 | 2021-02-09 | 泰兴华盛精细化工有限公司 | 一种双氟代磺酰亚胺的提纯方法 |
-
2021
- 2021-12-17 US US17/554,977 patent/US11772967B2/en active Active
-
2022
- 2022-01-04 CN CN202280008255.5A patent/CN116783140A/zh active Pending
- 2022-01-04 KR KR1020237022009A patent/KR20230127238A/ko unknown
- 2022-01-04 WO PCT/US2022/070021 patent/WO2022150808A1/en active Application Filing
- 2022-01-04 JP JP2023539853A patent/JP2024504275A/ja active Pending
- 2022-01-04 EP EP22737327.1A patent/EP4274807A1/en active Pending
- 2022-01-04 MX MX2023007214A patent/MX2023007214A/es unknown
Also Published As
Publication number | Publication date |
---|---|
KR20230127238A (ko) | 2023-08-31 |
JP2024504275A (ja) | 2024-01-31 |
CN116783140A (zh) | 2023-09-19 |
WO2022150808A1 (en) | 2022-07-14 |
US20220212929A1 (en) | 2022-07-07 |
EP4274807A1 (en) | 2023-11-15 |
US11772967B2 (en) | 2023-10-03 |
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