MX2020000654A - Recuperacion del litio de una solucion acida. - Google Patents
Recuperacion del litio de una solucion acida.Info
- Publication number
- MX2020000654A MX2020000654A MX2020000654A MX2020000654A MX2020000654A MX 2020000654 A MX2020000654 A MX 2020000654A MX 2020000654 A MX2020000654 A MX 2020000654A MX 2020000654 A MX2020000654 A MX 2020000654A MX 2020000654 A MX2020000654 A MX 2020000654A
- Authority
- MX
- Mexico
- Prior art keywords
- lithium
- recovery
- acid solution
- low
- containing material
- Prior art date
Links
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title abstract 9
- 229910052744 lithium Inorganic materials 0.000 title abstract 9
- 238000011084 recovery Methods 0.000 title abstract 2
- 239000002253 acid Substances 0.000 title 1
- 239000000463 material Substances 0.000 abstract 3
- 239000012528 membrane Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 230000029087 digestion Effects 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 229910001416 lithium ion Inorganic materials 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/10—Obtaining alkali metals
- C22B26/12—Obtaining lithium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
- B01D61/025—Reverse osmosis; Hyperfiltration
- B01D61/026—Reverse osmosis; Hyperfiltration comprising multiple reverse osmosis steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
- B01D61/027—Nanofiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
- B01D61/029—Multistep processes comprising different kinds of membrane processes selected from reverse osmosis, hyperfiltration or nanofiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/58—Multistep processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/02—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
- B01D71/06—Organic material
- B01D71/76—Macromolecular material not specifically provided for in a single one of groups B01D71/08 - B01D71/74
- B01D71/82—Macromolecular material not specifically provided for in a single one of groups B01D71/08 - B01D71/74 characterised by the presence of specified groups, e.g. introduced by chemical after-treatment
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/16—Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/16—Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
- C22B3/1608—Leaching with acyclic or carbocyclic agents
- C22B3/1616—Leaching with acyclic or carbocyclic agents of a single type
- C22B3/165—Leaching with acyclic or carbocyclic agents of a single type with organic acids
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/54—Reclaiming serviceable parts of waste accumulators
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/02—Specific process operations before starting the membrane separation process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/08—Specific process operations in the concentrate stream
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/25—Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/25—Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
- B01D2311/251—Recirculation of permeate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/25—Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
- B01D2311/251—Recirculation of permeate
- B01D2311/2512—Recirculation of permeate to feed side
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/26—Further operations combined with membrane separation processes
- B01D2311/2623—Ion-Exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2317/00—Membrane module arrangements within a plant or an apparatus
- B01D2317/02—Elements in series
- B01D2317/025—Permeate series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/145—Ultrafiltration
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/84—Recycling of batteries or fuel cells
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Water Supply & Treatment (AREA)
- Metallurgy (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Nanotechnology (AREA)
- General Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Secondary Cells (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Processing Of Solid Wastes (AREA)
- Carbon And Carbon Compounds (AREA)
- Removal Of Specific Substances (AREA)
Abstract
Métodos para recuperar litio de una fuente de litio o un material con contenido de litio usando soluciones con bajo pH y tecnologías de membrana para purificar y concentrar el litio recuperado. Las fuentes de litio pueden incluir una batería/celda de ion de litio gastada, un depósito mineral con contenido de litio, u otros materiales con contenido de litio. Loa procesos descritos en el presente documento recuperan el litio después de la digestión del material con contenido de litio con una solución con un bajo pH a través de una o más membranas semipermeables, estables con el ácido.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US15/656,759 US10450633B2 (en) | 2017-07-21 | 2017-07-21 | Recovery of lithium from an acid solution |
PCT/US2018/042378 WO2019018333A1 (en) | 2017-07-21 | 2018-07-17 | RECOVERING LITHIUM FROM AN ACID SOLUTION |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2020000654A true MX2020000654A (es) | 2020-07-29 |
Family
ID=65015833
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2020000654A MX2020000654A (es) | 2017-07-21 | 2018-07-17 | Recuperacion del litio de una solucion acida. |
Country Status (12)
Country | Link |
---|---|
US (2) | US10450633B2 (es) |
EP (2) | EP3926062A1 (es) |
JP (2) | JP6896166B2 (es) |
KR (2) | KR102523686B1 (es) |
CN (1) | CN111194236A (es) |
AU (2) | AU2018304150C1 (es) |
HU (1) | HUE057291T2 (es) |
MX (1) | MX2020000654A (es) |
PL (1) | PL3641918T3 (es) |
RU (2) | RU2020141390A (es) |
SG (2) | SG11202000587VA (es) |
WO (1) | WO2019018333A1 (es) |
Families Citing this family (21)
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JP7427598B2 (ja) * | 2018-02-28 | 2024-02-05 | ライラック ソリューションズ,インク. | リチウム抽出用の粒子トラップを備えたイオン交換反応器 |
BR112021015422A2 (pt) | 2019-02-05 | 2021-11-16 | Bright Minz Pty Ltd | Processos para recuperar hidróxido de lítio a partir de soluções contendo sulfato de lítio |
WO2021018372A1 (de) * | 2019-07-26 | 2021-02-04 | Duesenfeld Gmbh | Verfahren zum verwerten von lithium-batterien |
CN110534833B (zh) * | 2019-09-02 | 2021-09-17 | 江西迈特循环科技有限公司 | 一种处理含有磷酸铁锂的物质的方法及设备 |
CN110589812A (zh) * | 2019-09-17 | 2019-12-20 | 华南理工大学 | 一种利用废旧动力电池回收石墨负极材料制备多孔石墨烯的方法 |
RU2713360C2 (ru) * | 2019-09-25 | 2020-02-04 | Общество с ограниченной ответственностью "Экостар-Наутех" | Способ получения моногидрата гидроксида лития из рассолов |
KR102378528B1 (ko) * | 2019-12-20 | 2022-03-23 | 재단법인 포항산업과학연구원 | 폐리튬이온배터리의 폐수 처리방법 |
WO2021215484A1 (ja) * | 2020-04-21 | 2021-10-28 | 東レ株式会社 | レアメタル塩の回収方法 |
CN115697533A (zh) | 2020-05-29 | 2023-02-03 | 东丽株式会社 | 钴盐及镍盐的分离回收方法 |
KR20230023714A (ko) | 2020-06-09 | 2023-02-17 | 리락 솔루션즈, 인크. | 스케일런트의 존재 하에서의 리튬 추출 |
AR122639A1 (es) * | 2020-06-16 | 2022-09-28 | Larry Allen Lien | Concentración de metales preciosos y elementos de tierras raras |
CN112086703B (zh) * | 2020-09-10 | 2021-08-06 | 中南大学 | 一种退役电池炭渣的资源化处理方法 |
KR102255898B1 (ko) * | 2020-11-18 | 2021-05-25 | (주)세화이에스 | 리튬이온 이차전지의 폐 양극재로부터 리튬을 회수하는 방법 |
WO2022226219A1 (en) | 2021-04-23 | 2022-10-27 | Lilac Solutions, Inc. | Ion exchange devices for lithium extraction |
CN113582171B (zh) * | 2021-07-19 | 2023-07-18 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种回收锂离子电池石墨负极的方法 |
CN115198109A (zh) * | 2022-05-27 | 2022-10-18 | 安徽大学绿色产业创新研究院 | 一种通过混合酸从含锂粘土中提锂的方法 |
WO2024073485A1 (en) * | 2022-09-28 | 2024-04-04 | Gradiant Corporation | Lithium recovery from liquid streams using solute-permeable membranes |
US20240113350A1 (en) * | 2022-09-30 | 2024-04-04 | Ascend Elements, Inc. | Nickel-rich battery recycling |
CN115784274B (zh) * | 2022-11-02 | 2024-01-09 | 四川顺应锂材料科技有限公司 | 一种硝酸铝溶液中微量锂的分离回收方法 |
CN115893457A (zh) * | 2022-11-25 | 2023-04-04 | 河南佰利新能源材料有限公司 | 从废旧磷酸铁锂中回收碳酸锂和磷酸铁的方法及其应用 |
CN116240401A (zh) * | 2023-03-03 | 2023-06-09 | 桂林理工大学 | 一种从拜耳法铝酸钠溶液中提取稀散元素锂的方法 |
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CN105449305A (zh) | 2015-12-30 | 2016-03-30 | 深圳先进技术研究院 | 一种锂电池材料回收利用方法 |
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-
2017
- 2017-07-21 US US15/656,759 patent/US10450633B2/en active Active
-
2018
- 2018-07-17 MX MX2020000654A patent/MX2020000654A/es unknown
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- 2018-07-17 KR KR1020207029081A patent/KR102523686B1/ko active IP Right Grant
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- 2018-07-17 RU RU2020107676A patent/RU2739764C1/ru active
- 2018-07-17 CN CN201880060364.5A patent/CN111194236A/zh active Pending
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2019
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US20190024212A1 (en) | 2019-01-24 |
HUE057291T2 (hu) | 2022-05-28 |
AU2018304150C1 (en) | 2020-07-09 |
AU2018304150A1 (en) | 2020-02-06 |
US10450633B2 (en) | 2019-10-22 |
AU2018304150B2 (en) | 2020-02-27 |
JP7248739B2 (ja) | 2023-03-29 |
WO2019018333A1 (en) | 2019-01-24 |
SG11202000587VA (en) | 2020-02-27 |
JP6896166B2 (ja) | 2021-06-30 |
RU2020141390A (ru) | 2020-12-28 |
US20200115774A1 (en) | 2020-04-16 |
PL3641918T3 (pl) | 2022-01-31 |
EP3641918A1 (en) | 2020-04-29 |
KR20200022514A (ko) | 2020-03-03 |
EP3641918A4 (en) | 2020-07-01 |
SG10202111750VA (en) | 2021-12-30 |
KR102165981B1 (ko) | 2020-10-16 |
KR20200119906A (ko) | 2020-10-20 |
JP2020527196A (ja) | 2020-09-03 |
RU2739764C1 (ru) | 2020-12-28 |
AU2020201803B2 (en) | 2022-07-07 |
KR102523686B1 (ko) | 2023-04-20 |
CN111194236A (zh) | 2020-05-22 |
AU2020201803A1 (en) | 2020-04-02 |
EP3641918B1 (en) | 2021-09-22 |
JP2021176990A (ja) | 2021-11-11 |
EP3926062A1 (en) | 2021-12-22 |
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