CL2017000964A1 - Proceso para la concentración de soluciones que contienen litio - Google Patents

Proceso para la concentración de soluciones que contienen litio

Info

Publication number
CL2017000964A1
CL2017000964A1 CL2017000964A CL2017000964A CL2017000964A1 CL 2017000964 A1 CL2017000964 A1 CL 2017000964A1 CL 2017000964 A CL2017000964 A CL 2017000964A CL 2017000964 A CL2017000964 A CL 2017000964A CL 2017000964 A1 CL2017000964 A1 CL 2017000964A1
Authority
CL
Chile
Prior art keywords
pressure
containing lithium
direct osmosis
solutions containing
osmosis process
Prior art date
Application number
CL2017000964A
Other languages
English (en)
Inventor
Jackson R Switzer
Neal J Colonius
Chi Hung Cheng
Pieter Johannes Daudey
Original Assignee
Albemarle Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Albemarle Corp filed Critical Albemarle Corp
Publication of CL2017000964A1 publication Critical patent/CL2017000964A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58—Multistep processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/002—Forward osmosis or direct osmosis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/002—Forward osmosis or direct osmosis
    • B01D61/0021—Forward osmosis or direct osmosis comprising multiple forward osmosis steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/025—Reverse osmosis; Hyperfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B01D69/125—In situ manufacturing by polymerisation, polycondensation, cross-linking or chemical reaction
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/04—Halides
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/445—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by forward osmosis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/10—Temperature control
    • B01D2311/103—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/25—Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/25—Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed
    • B01D2311/252—Recirculation of concentrate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2315/00—Details relating to the membrane module operation
    • B01D2315/10—Cross-flow filtration
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/02—Non-contaminated water, e.g. for industrial water supply
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/08—Seawater, e.g. for desalination
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/10—Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00—Controlling or monitoring parameters in water treatment
    • C02F2209/001—Upstream control, i.e. monitoring for predictive control
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00—Controlling or monitoring parameters in water treatment
    • C02F2209/02—Temperature
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00—General aspects of water treatment
    • C02F2301/08—Multistage treatments, e.g. repetition of the same process step under different conditions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A20/00—Water conservation; Efficient water supply; Efficient water use
    • Y02A20/124—Water desalination
    • Y02A20/131—Reverse-osmosis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00—Technologies for wastewater treatment
    • Y02W10/30—Wastewater or sewage treatment systems using renewable energies
    • Y02W10/37—Wastewater or sewage treatment systems using renewable energies using solar energy

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

<p>SE DESCRIBE UN PROCESO DE OSMOSIS DIRECTA ARA LA CONCENTRACIÓN DE SOLUCIONES DE SAL QUE CONTIENEN LITIO. UNA DIFERENCIA DE PRESIÓN OSMÓTICA ENTRE UNA SOLUCIÓN DE SAL QUE CONTIENE LITIO Y UNA SEGUNDA SOLUCIÓN DE SAL DE MAYOR PRESIÓN OSMÓTICA SE UTILIZA COMO FUERZA MOTRIZ PARA PASAR AGUA A TRAVÉS DE UNA MEMBRANA DE OSMOSIS DIRECTA SEMI-PERMEABLE DE DICHA SOLUCIÓN DE SAL QUE CONTIENE LITIO DE MENOR PRESIÓN OSMÓTICA HACIA LA SOLUCIÓN DE SAL DE MAYOR PRESIÓN OSMÓTICA. ADEMÁS, SE DESCRIBE UNA OPERACIÓN DE DOS PARTES EN LA QUE LA TECNOLOGÍA DE PROCESO DE OSMOSIS INVERSA Y LA TECNOLOGÍA DE PROCESO DE OSMOSIS DIRECTA SE UTILIZAN EN TÁNDEM PARA CONCENTRAR SOLUCIONES DE SAL QUE CONTIENEN LITIO Y RECUPERAR EL AGUA QUE PUEDE SER RECICLADA AL PROCESO. EL PROCESO DE OSMOSIS DIRECTA SE LLEVA A CABO SIN NECESIDAD DE (I) EL USO DE UNA PRESIÓN SUPERIOR A LA ATMOSFÉRICA O (II) EL USA DE UNA PRESIÓN INFERIOR A LA ATMOSFÉRICA A (III) EL USO DE AMBAS TALES PRESIONES, A (IV) EL USO DE UNO O MÁS ADITIVOS PARA AYUDAR A ENCAUZAR EL FLUJO DE AGUA A TRAVÉS DE UNA MEMBRANA DE OSMOSIS DIRECTA.</p>
CL2017000964A 2014-10-20 2017-04-18 Proceso para la concentración de soluciones que contienen litio CL2017000964A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US201462065965P 2014-10-20 2014-10-20

Publications (1)

Publication Number Publication Date
CL2017000964A1 true CL2017000964A1 (es) 2017-11-03

Family

ID=55310889

Family Applications (2)

Application Number Title Priority Date Filing Date
CL2017000964A CL2017000964A1 (es) 2014-10-20 2017-04-18 Proceso para la concentración de soluciones que contienen litio
CL2019002546A CL2019002546A1 (es) 2014-10-20 2019-09-04 Proceso para la concentración de soluciones que contienen litio. (divisional solicitud 201700964)

Family Applications After (1)

Application Number Title Priority Date Filing Date
CL2019002546A CL2019002546A1 (es) 2014-10-20 2019-09-04 Proceso para la concentración de soluciones que contienen litio. (divisional solicitud 201700964)

Country Status (8)

Country Link
US (1) US20180147532A1 (es)
JP (1) JP2017532197A (es)
KR (1) KR20170071502A (es)
AR (1) AR102363A1 (es)
AU (1) AU2015336234A1 (es)
CA (1) CA2963565A1 (es)
CL (2) CL2017000964A1 (es)
WO (1) WO2016064689A2 (es)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10150056B2 (en) 2016-11-14 2018-12-11 Lilac Solutions, Inc. Lithium extraction with coated ion exchange particles
EP3570965A4 (en) * 2017-01-20 2021-02-17 Trevi Systems Inc. REVERSE OSMOSIS MEMBRANE AND MODULE SUPPORTED BY OSMOTIC PRESSURE
EP3661619A4 (en) 2017-08-02 2021-05-05 Lilac Solutions, Inc. LITHIUM EXTRACTION WITH POROUS ION EXCHANGE BEADS
CN111182953A (zh) 2017-08-02 2020-05-19 锂莱克解决方案公司 用于锂提取的离子交换系统
US10648090B2 (en) 2018-02-17 2020-05-12 Lilac Solutions, Inc. Integrated system for lithium extraction and conversion
JP7379351B2 (ja) * 2018-02-17 2023-11-14 ライラック ソリューションズ，インク． リチウムの抽出と変換のための統合システム
WO2019168941A1 (en) 2018-02-28 2019-09-06 Lilac Solutions, Inc. Ion exchange reactor with particle traps for lithium extraction
US11235282B2 (en) * 2018-03-09 2022-02-01 Terralithium Llc Processes for producing lithium compounds using forward osmosis
WO2020033668A1 (en) * 2018-08-09 2020-02-13 Ut-Battelle, Llc Forward osmosis composite membranes for concentration of lithium containing solutions
JP7186557B2 (ja) 2018-09-14 2022-12-09 旭化成株式会社 溶媒含有物品の濃縮システム
US11643703B2 (en) 2019-06-18 2023-05-09 Schlumberger Technology Corporation Method of recovering alkali metals from an aqueous source
CN112108001B (zh) * 2019-06-20 2022-09-13 国家能源投资集团有限责任公司 一种反渗透系统及其浓缩含锂盐水的方法
JP2023514803A (ja) 2020-01-09 2023-04-11 ライラック ソリューションズ，インク． 望ましくない金属を分離するための方法
GB202003685D0 (en) * 2020-03-13 2020-04-29 Ide Projects Ltd Forward osmotic separation system and method
JP2023529444A (ja) 2020-06-09 2023-07-10 ライラック ソリューションズ，インク． スケール物質存在下におけるリチウム抽出
EP4247759A1 (en) 2020-11-20 2023-09-27 Lilac Solutions, Inc. Lithium production with volatile acid
WO2023028281A1 (en) * 2021-08-26 2023-03-02 Massachusetts Institute Of Technology Harnessing metal ions from brines
US11502323B1 (en) 2022-05-09 2022-11-15 Rahul S Nana Reverse electrodialysis cell and methods of use thereof
US11502322B1 (en) 2022-05-09 2022-11-15 Rahul S Nana Reverse electrodialysis cell with heat pump
US11855324B1 (en) 2022-11-15 2023-12-26 Rahul S. Nana Reverse electrodialysis or pressure-retarded osmosis cell with heat pump

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3130156A (en) 1960-12-13 1964-04-21 Ray A Neff Solvent extractor
US5158683A (en) * 1991-09-03 1992-10-27 Ethyl Corporation Bromide separation and concentration using semipermeable membranes
EP1833595A1 (en) * 2004-10-25 2007-09-19 Cascade Designs, Inc. Forward osmosis utilizing a controllable osmotic agent
US7445712B2 (en) 2005-04-07 2008-11-04 Hydration Technologies Inc. Asymmetric forward osmosis membranes
MX2010010163A (es) * 2008-03-20 2010-12-06 Univ Yale Modulo de membrana enrollada helicoidal para uso en osmosis forzada.
KR101577769B1 (ko) 2008-06-20 2015-12-15 예일 유니버시티 정삼투 분리 방법
WO2010104895A2 (en) 2009-03-09 2010-09-16 Herron John R Center tube configuration for a multiple spiral wound forward osmosis element
KR101749159B1 (ko) 2009-10-28 2017-07-04 오아시스 워터, 인크. 정 삼투 분리 방법
US9044711B2 (en) * 2009-10-28 2015-06-02 Oasys Water, Inc. Osmotically driven membrane processes and systems and methods for draw solute recovery
KR101272868B1 (ko) * 2010-11-11 2013-06-11 한국과학기술원 정삼투압을 이용한 저농도 발효액의 농축 방법
BR112013027449A2 (pt) * 2011-04-25 2019-09-24 Oasys Water Inc sistemas e métodos de separação osmótica
US20130048564A1 (en) * 2011-08-26 2013-02-28 Battelle Energy Alliance, Llc Draw solutes, methods of forming draw solutes, and methods of using draw solutes to treat an aqueous liquid
CN103182246A (zh) * 2011-12-28 2013-07-03 新加坡三泰水技术有限公司 一种溶液的膜分离工艺方法及系统
US20130341272A1 (en) * 2012-06-26 2013-12-26 Algae Systems, LLC Dewatering Systems and Methods for Biomass Concentration
AU2013344847A1 (en) * 2012-11-16 2015-05-14 Oasys Water, Inc. Draw solutions and draw solute recovery for osmotically driven membrane processes

Also Published As

Publication number Publication date
JP2017532197A (ja) 2017-11-02
WO2016064689A2 (en) 2016-04-28
CA2963565A1 (en) 2016-04-28
KR20170071502A (ko) 2017-06-23
CL2019002546A1 (es) 2019-11-15
WO2016064689A3 (en) 2016-07-28
AR102363A1 (es) 2017-02-22
AU2015336234A1 (en) 2017-04-20
US20180147532A1 (en) 2018-05-31

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