MX2016012125A - Procedimiento y dispositivo para separar una sustancia de una solucion. - Google Patents

Procedimiento y dispositivo para separar una sustancia de una solucion.

Info

Publication number
MX2016012125A
MX2016012125A MX2016012125A MX2016012125A MX2016012125A MX 2016012125 A MX2016012125 A MX 2016012125A MX 2016012125 A MX2016012125 A MX 2016012125A MX 2016012125 A MX2016012125 A MX 2016012125A MX 2016012125 A MX2016012125 A MX 2016012125A
Authority
MX
Mexico
Prior art keywords
solution
intensity
separating
detected
difference
Prior art date
Application number
MX2016012125A
Other languages
English (en)
Inventor
Ziegler Stefan
Rauls Matthias
Haubner Martin
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2016012125A publication Critical patent/MX2016012125A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B01D9/0031—Evaporation of components of the mixture to be separated by heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0063—Control or regulation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0077—Screening for crystallisation conditions or for crystal forms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • C07C29/172—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds with the obtention of a fully saturated alcohol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/56—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by isomerisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
    • C07F5/06—Aluminium compounds
    • C07F5/069—Aluminium compounds without C-aluminium linkages
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/47—Scattering, i.e. diffuse reflection
    • G01N21/49—Scattering, i.e. diffuse reflection within a body or fluid
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N21/85—Investigating moving fluids or granular solids
    • G01N21/8507—Probe photometers, i.e. with optical measuring part dipped into fluid sample
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84—Systems specially adapted for particular applications
    • G01N2021/8405—Application to two-phase or mixed materials, e.g. gas dissolved in liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invención se refiere a un procedimiento para separar una sustancia de una solución, en el cual se irradia radiación electromagnética en la solución, se detecta una intensidad de la radiación electromagnética, que fue dispersada por los cristales que se encuentran en la solución, la intensidad detectada es comparada con una intensidad nominal (ls) y la temperatura de la solución es regulada en función de la diferencia entre la intensidad detectada y la intensidad nominal (ls) de tal modo que se reduce el monto de esta diferencia. Cuando el monto de la diferencia de la intensidad detectada y la intensidad nominal (ls) es menor que un valor límite, se inicia un procedimiento de cristalización, en el cual se obtienen cristales de la sustancia, los que a continuación se separan.
MX2016012125A 2014-03-19 2015-03-13 Procedimiento y dispositivo para separar una sustancia de una solucion. MX2016012125A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP14160645 2014-03-19
PCT/EP2015/055279 WO2015140062A1 (de) 2014-03-19 2015-03-13 Verfahren und vorrichtung zum abtrennen eines stoffes aus einer lösung

Publications (1)

Publication Number Publication Date
MX2016012125A true MX2016012125A (es) 2017-01-19

Family

ID=50287987

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2016012125A MX2016012125A (es) 2014-03-19 2015-03-13 Procedimiento y dispositivo para separar una sustancia de una solucion.

Country Status (8)

Country Link
US (1) US10294182B2 (es)
EP (2) EP3119489B1 (es)
JP (1) JP6702880B2 (es)
CN (1) CN106132496B (es)
ES (1) ES2898659T3 (es)
MX (1) MX2016012125A (es)
PL (1) PL3119489T3 (es)
WO (1) WO2015140062A1 (es)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018034305A1 (ja) * 2016-08-19 2018-02-22 日本碍子株式会社 有機化合物の精製方法
US10983044B2 (en) * 2018-06-26 2021-04-20 Arometrix, Inc. Device, system and method for in-situ optical monitoring and control of extraction and purification of plant materials
CN109908621A (zh) * 2019-04-12 2019-06-21 四川永祥多晶硅有限公司 渣浆分离前置输送系统及方法
DE102019130781A1 (de) * 2019-11-14 2021-05-20 Hochschule Mannheim Sensor und Vorrichtung zur Erfassung des Kristallisationsgrades
CN115315298B (zh) * 2020-07-13 2023-09-15 日本碍子株式会社 精制方法

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CH350461A (de) 1957-12-06 1960-11-30 Ciba Geigy Verwendung von Oxyketonen zum Schutze gegen ultraviolette Strahlung
US3357196A (en) * 1965-01-13 1967-12-12 Phillips Petroleum Co Heated melt recycle responsive to temperature differential of crystal mass
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DE19536792A1 (de) * 1995-10-02 1997-04-03 Basf Ag Verfahren zur Stofftrennung aus einem flüssigen Gemisch durch Kristallisation
DE19617210A1 (de) 1996-04-30 1997-11-06 Basf Ag Trennwandkolonne zur kontinuierlichen destillativen Zerlegung von Mehrstoffgemischen
DE59701724D1 (de) * 1996-07-05 2000-06-21 Haarmann & Reimer Gmbh Kristallisationsvorrichtung und -verfahren
EP1053974A1 (en) 1999-05-17 2000-11-22 Quest International B.V. Reactions using lewis acids
CZ20011726A3 (cs) * 2000-05-26 2002-02-13 Pfizer Products Inc. Způsob reakční krystalizace, který umoľňuje řídit velikost částic
JP4676617B2 (ja) 2001-01-18 2011-04-27 高砂香料工業株式会社 イソプレゴールの製造方法
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Also Published As

Publication number Publication date
ES2898659T3 (es) 2022-03-08
WO2015140062A1 (de) 2015-09-24
CN106132496B (zh) 2020-03-13
US10294182B2 (en) 2019-05-21
PL3119489T3 (pl) 2022-01-17
EP3919148B1 (de) 2024-05-08
US20170240494A1 (en) 2017-08-24
EP3119489A1 (de) 2017-01-25
EP3919148A1 (de) 2021-12-08
CN106132496A (zh) 2016-11-16
EP3119489B1 (de) 2021-08-25
JP6702880B2 (ja) 2020-06-03
JP2017512781A (ja) 2017-05-25

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