MX2016001853A - Procedimiento para preparar poliéter-carbonato polioles. - Google Patents
Procedimiento para preparar poliéter-carbonato polioles.Info
- Publication number
- MX2016001853A MX2016001853A MX2016001853A MX2016001853A MX2016001853A MX 2016001853 A MX2016001853 A MX 2016001853A MX 2016001853 A MX2016001853 A MX 2016001853A MX 2016001853 A MX2016001853 A MX 2016001853A MX 2016001853 A MX2016001853 A MX 2016001853A
- Authority
- MX
- Mexico
- Prior art keywords
- carbonate polyols
- polyether carbonate
- polyether polyol
- preparing polyether
- polyol ligand
- Prior art date
Links
- 239000004721 Polyphenylene oxide Substances 0.000 title abstract 5
- 229920000570 polyether Polymers 0.000 title abstract 5
- 229920005862 polyol Polymers 0.000 title abstract 5
- -1 carbonate polyols Chemical class 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000003054 catalyst Substances 0.000 abstract 3
- 239000003446 ligand Substances 0.000 abstract 3
- 150000003077 polyols Chemical class 0.000 abstract 3
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 239000008139 complexing agent Substances 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000002002 slurry Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 230000002194 synthesizing effect Effects 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/32—General preparatory processes using carbon dioxide
- C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
- B01J27/26—Cyanides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/06—Washing
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Toxicology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Health & Medical Sciences (AREA)
- Polyesters Or Polycarbonates (AREA)
- Polyethers (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
La presente invención se refiere a un procedimiento para la preparación de poliéter-carbonato polioles en presencia de un catalizador de cianuro bimetálico que puede obtenerse mediante un procedimiento que comprende (a) sintetizar un catalizador de cianuro bimetálico sólido en presencia de un agente de complejación orgánico y un ligando poliéter poliol; y (b) lavar en primer lugar el catalizador obtenido en la etapa a) con una disolución acuosa que comprende el 90-100% en peso de agua y 0-10% en peso de un ligando poliéter poliol, para formar una suspensión, en el que la disolución acuosa no contiene ningún agente de complejación orgánico distinto del ligando poliéter poliol.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP13382327.8A EP2837648A1 (en) | 2013-08-12 | 2013-08-12 | Process for preparing polyether carbonate polyols |
PCT/EP2014/067158 WO2015022290A1 (en) | 2013-08-12 | 2014-08-11 | Process for preparing polyether carbonate polyols |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2016001853A true MX2016001853A (es) | 2016-08-03 |
Family
ID=49029046
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2016001853A MX2016001853A (es) | 2013-08-12 | 2014-08-11 | Procedimiento para preparar poliéter-carbonato polioles. |
Country Status (13)
Country | Link |
---|---|
US (1) | US10385164B2 (es) |
EP (2) | EP2837648A1 (es) |
JP (1) | JP6328241B2 (es) |
KR (1) | KR20160042967A (es) |
CN (1) | CN105531299B (es) |
BR (1) | BR112016002894A2 (es) |
CA (1) | CA2921138A1 (es) |
ES (1) | ES2762553T3 (es) |
MX (1) | MX2016001853A (es) |
PT (1) | PT3033374T (es) |
RU (1) | RU2659782C2 (es) |
SA (1) | SA516370566B1 (es) |
WO (1) | WO2015022290A1 (es) |
Families Citing this family (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2016166165A1 (en) | 2015-04-13 | 2016-10-20 | Repsol, S.A. | New formulations for polyurethane applications |
CN107849233B (zh) * | 2015-06-15 | 2020-01-17 | 阿卜杜拉国王科技大学 | 制备聚碳酸酯的方法以及用于控制聚合物组成的方法 |
EP3106221A1 (en) * | 2015-06-15 | 2016-12-21 | Universität Hamburg | Process for preparing double metal cyanide catalysts and their use in polymerization reactions |
ES2936086T3 (es) | 2015-08-03 | 2023-03-14 | Repsol Sa | Composición adhesiva que comprende poliéter carbonato polioles |
WO2017021448A1 (en) | 2015-08-04 | 2017-02-09 | Repsol, S.A. | New formulations for pressure sensitive adhesives |
GB201515350D0 (en) | 2015-08-28 | 2015-10-14 | Econic Technologies Ltd | Method for preparing polyols |
US10119223B2 (en) * | 2016-07-15 | 2018-11-06 | Covestro Llc | Carpet and synthetic turf backings prepared from a polyether carbonate polyol |
BR112019007848A2 (pt) * | 2016-10-18 | 2019-07-16 | Repsol Sa | polímeros inovadores de alto peso molecular a partir de matérias-primas residuais |
KR101867721B1 (ko) | 2016-12-16 | 2018-06-14 | 주식회사 포스코 | 폴리에테르 카보네이트 폴리올 제조공정에서의 프로필렌 카보네이트의 분리방법 |
GB201703324D0 (en) | 2017-03-01 | 2017-04-12 | Econic Tech Ltd | Method for preparing polyether carbonates |
GB201717459D0 (en) | 2017-10-24 | 2017-12-06 | Econic Tech Limited | Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates |
GB201717441D0 (en) | 2017-10-24 | 2017-12-06 | Econic Tech Ltd | A polymerisation process |
JP2021508753A (ja) * | 2017-12-28 | 2021-03-11 | コベストロ、ドイチュラント、アクチエンゲゼルシャフトCovestro Deutschland Ag | 水性分散液 |
GB201814526D0 (en) | 2018-09-06 | 2018-10-24 | Econic Tech Ltd | Methods for forming polycarbonate ether polyols and high molecular weight polyether carbonates |
GB201906210D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Limited | A polyol block copolymer, compositions and processes therefor |
GB201906214D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Ltd | A polyol block copolymer, compositions and processes therefor |
EP4017901A1 (de) * | 2019-08-19 | 2022-06-29 | Covestro Deutschland AG | Verfahren zur herstellung von polyethercarbonatalkoholen |
GB202003002D0 (en) | 2020-03-02 | 2020-04-15 | Crane Ltd | Method of preparation of a polyol block copolymer |
GB202003003D0 (en) | 2020-03-02 | 2020-04-15 | Econic Tech Ltd | A polyol block copolymer |
GB202017531D0 (en) | 2020-11-05 | 2020-12-23 | Econic Tech Limited | (poly)ol block copolymer |
CN114805817B (zh) * | 2021-01-28 | 2023-07-11 | 万华化学集团股份有限公司 | 一种双金属催化剂及其制备方法和在制备聚醚多元醇中的应用 |
CN113493563A (zh) * | 2021-07-14 | 2021-10-12 | 扬州工业职业技术学院 | 一种聚醚多元醇及其制备方法、应用 |
WO2023013510A1 (ja) * | 2021-08-06 | 2023-02-09 | Agc株式会社 | ポリウレタン樹脂及びその製造方法 |
WO2023017276A1 (en) | 2021-08-11 | 2023-02-16 | Econic Technologies Ltd | Method for preparing surfactants by copolymerisation of epoxides and co2 using a mixture of a macrocyclic bimetal catalyst and a double metal cyanide catalyst |
GB202115335D0 (en) | 2021-10-25 | 2021-12-08 | Econic Tech Ltd | Surface-active agent |
CN114836115A (zh) * | 2022-04-06 | 2022-08-02 | 上海予通管道工程技术有限公司 | 非开挖管道内衬修复用聚脲涂料及其制备方法 |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3427256A (en) | 1963-02-14 | 1969-02-11 | Gen Tire & Rubber Co | Double metal cyanide complex compounds |
US3427334A (en) | 1963-02-14 | 1969-02-11 | Gen Tire & Rubber Co | Double metal cyanides complexed with an alcohol aldehyde or ketone to increase catalytic activity |
GB1063525A (en) | 1963-02-14 | 1967-03-30 | Gen Tire & Rubber Co | Organic cyclic oxide polymers, their preparation and tires prepared therefrom |
US3941849A (en) | 1972-07-07 | 1976-03-02 | The General Tire & Rubber Company | Polyethers and method for making the same |
JP3194255B2 (ja) * | 1990-11-27 | 2001-07-30 | 旭硝子株式会社 | 複合金属シアン化物錯体の保存方法およびポリエーテルの製造方法 |
US5158922A (en) | 1992-02-04 | 1992-10-27 | Arco Chemical Technology, L.P. | Process for preparing metal cyanide complex catalyst |
US5627120A (en) | 1996-04-19 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
DE60127192T2 (de) | 2000-06-27 | 2007-11-22 | Saudi Basic Industries Corp. | Katalysatoren für die Herstellung von Olefinen durch oxidative Dehydrierung |
US6762278B2 (en) * | 2002-02-04 | 2004-07-13 | Basf Corporation | Process for the copolymerization of alkylene oxides and carbon dioxide using suspensions of multi-metal cyanide compounds |
US7671228B2 (en) * | 2005-03-29 | 2010-03-02 | Basf Corporation | Method of forming a polyethercarbonate polyol using a CO2-philic compound or substituent |
US7977501B2 (en) | 2006-07-24 | 2011-07-12 | Bayer Materialscience Llc | Polyether carbonate polyols made via double metal cyanide (DMC) catalysis |
KR101455878B1 (ko) * | 2006-11-15 | 2014-11-03 | 바스프 에스이 | 연질 폴리우레탄 발포체의 제조 방법 |
CN101623656A (zh) * | 2009-07-31 | 2010-01-13 | 广州市达志化工科技有限公司 | 一种双金属氰化物催化剂及其制备方法和用途 |
WO2011089120A1 (de) | 2010-01-20 | 2011-07-28 | Bayer Materialscience Ag | Verfahren zur aktivierung von doppelmetallcyanidkatalysatoren zur herstellung von polyethercarbonatpolyolen |
DE102010008410A1 (de) * | 2010-02-18 | 2011-08-18 | Bayer MaterialScience AG, 51373 | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
WO2011144523A1 (de) * | 2010-05-18 | 2011-11-24 | Bayer Materialscience Ag | Verfahren zur herstellung von polyethercarbonatpolyolen |
DE102010040517A1 (de) * | 2010-09-09 | 2012-03-15 | Bayer Materialscience Aktiengesellschaft | Verfahren zur Herstellung von Polyetherpolyolen |
EP2441788A1 (de) * | 2010-10-14 | 2012-04-18 | Bayer MaterialScience AG | Verfahren zur Herstellung von Polyetherpolyolen |
SA116370919B1 (ar) | 2011-05-17 | 2017-05-08 | ريبسول، اس. ايه. | عملية لتحضير مُحفِّز من مُعقَّد سيانيدي مزدوج المعدن |
EP2548908A1 (de) * | 2011-07-18 | 2013-01-23 | Bayer MaterialScience AG | Verfahren zur Herstellung von Polyetherpolyolen |
-
2013
- 2013-08-12 EP EP13382327.8A patent/EP2837648A1/en not_active Withdrawn
-
2014
- 2014-08-11 BR BR112016002894A patent/BR112016002894A2/pt active Search and Examination
- 2014-08-11 ES ES14750468T patent/ES2762553T3/es active Active
- 2014-08-11 MX MX2016001853A patent/MX2016001853A/es active IP Right Grant
- 2014-08-11 CN CN201480050222.2A patent/CN105531299B/zh active Active
- 2014-08-11 RU RU2016108497A patent/RU2659782C2/ru active
- 2014-08-11 PT PT147504682T patent/PT3033374T/pt unknown
- 2014-08-11 JP JP2016533901A patent/JP6328241B2/ja not_active Expired - Fee Related
- 2014-08-11 KR KR1020167006178A patent/KR20160042967A/ko active IP Right Grant
- 2014-08-11 CA CA2921138A patent/CA2921138A1/en not_active Abandoned
- 2014-08-11 WO PCT/EP2014/067158 patent/WO2015022290A1/en active Application Filing
- 2014-08-11 US US14/911,669 patent/US10385164B2/en active Active
- 2014-08-11 EP EP14750468.2A patent/EP3033374B1/en active Active
-
2016
- 2016-02-11 SA SA516370566A patent/SA516370566B1/ar unknown
Also Published As
Publication number | Publication date |
---|---|
RU2659782C2 (ru) | 2018-07-04 |
EP2837648A1 (en) | 2015-02-18 |
US10385164B2 (en) | 2019-08-20 |
BR112016002894A2 (pt) | 2017-08-01 |
CA2921138A1 (en) | 2015-02-19 |
RU2016108497A (ru) | 2017-09-19 |
PT3033374T (pt) | 2020-01-20 |
JP6328241B2 (ja) | 2018-05-23 |
KR20160042967A (ko) | 2016-04-20 |
CN105531299B (zh) | 2017-11-10 |
ES2762553T3 (es) | 2020-05-25 |
WO2015022290A1 (en) | 2015-02-19 |
CN105531299A (zh) | 2016-04-27 |
EP3033374A1 (en) | 2016-06-22 |
US20160194441A1 (en) | 2016-07-07 |
SA516370566B1 (ar) | 2019-11-10 |
EP3033374B1 (en) | 2019-11-13 |
JP2016527385A (ja) | 2016-09-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant or registration |