MX2009005152A - Sistemas catalizadores y procesos de polimerizacion. - Google Patents
Sistemas catalizadores y procesos de polimerizacion.Info
- Publication number
- MX2009005152A MX2009005152A MX2009005152A MX2009005152A MX2009005152A MX 2009005152 A MX2009005152 A MX 2009005152A MX 2009005152 A MX2009005152 A MX 2009005152A MX 2009005152 A MX2009005152 A MX 2009005152A MX 2009005152 A MX2009005152 A MX 2009005152A
- Authority
- MX
- Mexico
- Prior art keywords
- catalyst systems
- polymerization processes
- catalyst system
- catalyst
- systems
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/65904—Component covered by group C08F4/64 containing a transition metal-carbon bond in combination with another component of C08F4/64
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/6592—Component covered by group C08F4/64 containing a transition metal-carbon bond containing at least one cyclopentadienyl ring, condensed or not, e.g. an indenyl or a fluorenyl ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/69—Chromium, molybdenum, tungsten or compounds thereof
- C08F4/69008—Chromium, molybdenum, tungsten or compounds thereof the metallic compound containing a multidentate ligand, i.e. a ligand capable of donating two or more pairs of electrons to form a coordinate or ionic bond
- C08F4/69017—Bidentate ligand
- C08F4/69103—Monoanionic ligand
- C08F4/6912—NO
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2500/00—Characteristics or properties of obtained polyolefins; Use thereof
- C08F2500/01—High molecular weight, e.g. >800,000 Da.
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2500/00—Characteristics or properties of obtained polyolefins; Use thereof
- C08F2500/02—Low molecular weight, e.g. <100,000 Da.
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2500/00—Characteristics or properties of obtained polyolefins; Use thereof
- C08F2500/05—Bimodal or multimodal molecular weight distribution
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/65912—Component covered by group C08F4/64 containing a transition metal-carbon bond in combination with an organoaluminium compound
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
- C08F4/62—Refractory metals or compounds thereof
- C08F4/64—Titanium, zirconium, hafnium or compounds thereof
- C08F4/659—Component covered by group C08F4/64 containing a transition metal-carbon bond
- C08F4/65916—Component covered by group C08F4/64 containing a transition metal-carbon bond supported on a carrier, e.g. silica, MgCl2, polymer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S526/943—Polymerization with metallocene catalysts
Abstract
Un método para polimerizar olefinas con sistemas catalizadores, tales como, por ejemplo, un sistema catalizador multimodal, donde el sistema catalizador se almacena a una temperatura controlada para minimizar la pérdida de productividad del sistema catalizador.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US85882406P | 2006-11-14 | 2006-11-14 | |
PCT/US2007/023749 WO2008060512A1 (en) | 2006-11-14 | 2007-11-13 | Catalyst systems and polymerization processes |
Publications (2)
Publication Number | Publication Date |
---|---|
MX2009005152A true MX2009005152A (es) | 2009-07-24 |
MX345881B MX345881B (es) | 2016-03-07 |
Family
ID=38283117
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2009005152A MX345881B (es) | 2006-11-14 | 2007-11-13 | Sistemas catalizadores y procesos de polimerizacion. |
Country Status (14)
Country | Link |
---|---|
US (2) | US8088871B2 (es) |
EP (1) | EP2081968B1 (es) |
JP (1) | JP5676106B2 (es) |
KR (1) | KR101540820B1 (es) |
CN (1) | CN101541838B (es) |
AU (1) | AU2007319883B2 (es) |
BR (2) | BRPI0718849B1 (es) |
CA (1) | CA2668880C (es) |
ES (1) | ES2549693T3 (es) |
MX (1) | MX345881B (es) |
MY (1) | MY157264A (es) |
RU (1) | RU2452740C2 (es) |
WO (1) | WO2008060512A1 (es) |
ZA (1) | ZA200902461B (es) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8088871B2 (en) | 2006-11-14 | 2012-01-03 | Univation Technologies, Llc | Catalyst systems and polymerization processes |
US8835577B2 (en) | 2007-11-15 | 2014-09-16 | Univation Technologies, Llc | Catalyst systems having a tailored hydrogen response |
CN102414228B (zh) | 2009-05-14 | 2014-05-07 | 尤尼威蒂恩技术有限责任公司 | 具有特制的氢响应的混合金属催化剂体系 |
US8821800B2 (en) | 2012-10-18 | 2014-09-02 | Chevron Phillips Chemical Company Lp | System and method for catalyst preparation |
WO2014109832A1 (en) | 2013-01-14 | 2014-07-17 | Univation Technologies, Llc | Methods for preparing catalyst systems with increased productivity |
WO2015123171A2 (en) | 2014-02-11 | 2015-08-20 | Univation Technologies, Llc | Producing polyolefin products |
CN110330580A (zh) * | 2014-02-11 | 2019-10-15 | 尤尼威蒂恩技术有限责任公司 | 制造聚烯烃产物 |
JP6561655B2 (ja) * | 2014-08-08 | 2019-08-21 | 日本ポリプロ株式会社 | オレフィン重合体の製造方法 |
WO2017065274A1 (ja) * | 2015-10-14 | 2017-04-20 | 住友電気工業株式会社 | 光ファイバ素線 |
EP3778666B1 (en) * | 2016-11-08 | 2023-12-13 | Univation Technologies, LLC | Polyethylene composition |
WO2018147931A1 (en) | 2017-02-07 | 2018-08-16 | Exxonmobil Chemical Patents Inc. | Processes for reducing the loss of catalyst activity of a ziegler-natta catalyst |
US10030086B1 (en) | 2017-07-21 | 2018-07-24 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
US10697889B2 (en) | 2017-07-21 | 2020-06-30 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
US10507445B2 (en) | 2018-03-29 | 2019-12-17 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
US10679734B2 (en) | 2018-03-29 | 2020-06-09 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
Family Cites Families (43)
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SU859379A1 (ru) * | 1979-12-17 | 1981-08-30 | Предприятие П/Я М-5681 | Способ получени полипропилена |
US4522982A (en) * | 1983-06-06 | 1985-06-11 | Exxon Research & Engineering Co. | Isotactic-stereoblock polymers of alpha-olefins and process for producing the same |
IT1215820B (it) * | 1988-02-08 | 1990-02-22 | Fata Europ Group | Sistema per immagazzinare in modo automatizzato containers termici. |
IT1228916B (it) * | 1989-02-28 | 1991-07-09 | Himont Inc | Polimeri a struttura sindiotattica delle alfa olefine |
JP2951763B2 (ja) * | 1991-08-27 | 1999-09-20 | 三井化学株式会社 | メタロセン化合物溶液及びその保存方法 |
RU2048660C1 (ru) | 1992-02-19 | 1995-11-20 | Александр Васильевич Евсеев | Резервуар для охлаждения и хранения жидкости |
US5393851A (en) * | 1992-05-26 | 1995-02-28 | Fina Technology, Inc. | Process for using metallocene catalyst in a continuous reactor system |
BE1006880A3 (fr) * | 1993-03-01 | 1995-01-17 | Solvay | Precurseur solide d'un systeme catalytique pour la polymerisation d'olefines, procede pour sa preparation, systeme catalytique comprenant ce precurseur solide et procede de polymerisation d'olefines en presence de ce systeme catalytique. |
US6440745B1 (en) | 1994-10-18 | 2002-08-27 | Symyx Technologies | Combinatorial synthesis and screening of organometallic compounds and catalysts |
WO1996026967A1 (en) * | 1995-03-01 | 1996-09-06 | Minnesota Mining And Manufacturing Company | Tris(pentafluorophenyl)borate complexes and catalysts derived therefrom |
JP3472941B2 (ja) * | 1995-03-08 | 2003-12-02 | 三井化学株式会社 | オレフィン重合用触媒の保存方法、オレフィン重合用触媒溶液、オレフィン重合用触媒およびオレフィンの重合方法 |
JP3483013B2 (ja) * | 1995-04-28 | 2004-01-06 | 出光石油化学株式会社 | 重合用均一系触媒の保存方法 |
JP2000506212A (ja) * | 1996-03-04 | 2000-05-23 | エクソン・ケミカル・パテンツ・インク | 安定なメタロセン触媒系 |
ES2156389T3 (es) * | 1996-07-04 | 2001-06-16 | Basf Ag | Procedimiento para la obtencion de catalizadores de metales de transicion soportados. |
WO1999002571A1 (fr) * | 1997-07-09 | 1999-01-21 | Maruzen Petrochemical Co., Ltd. | Composants catalytiques destines a la polymerisation d'olefines, catalyseurs de polymerisation, et procede de polymerisation d'olefines a l'aide de ces derniers |
JP2002053607A (ja) * | 1997-07-09 | 2002-02-19 | Maruzen Petrochem Co Ltd | オレフィン類重合用触媒成分、重合用触媒およびこれを用いたオレフィン類の重合方法 |
US6265512B1 (en) * | 1997-10-23 | 2001-07-24 | 3M Innovative Company | Elastic polypropylenes and catalysts for their manufacture |
US6149882A (en) | 1998-06-09 | 2000-11-21 | Symyx Technologies, Inc. | Parallel fixed bed reactor and fluid contacting apparatus |
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DE60014376T2 (de) * | 1999-02-22 | 2005-02-24 | Eastman Chemical Co., Kingsport | Katalysatoren, die n-pyrrolylsubstituierte stickstoffdonoren enthalten |
US6274684B1 (en) | 1999-10-22 | 2001-08-14 | Univation Technologies, Llc | Catalyst composition, method of polymerization, and polymer therefrom |
BR0015241B1 (pt) * | 1999-10-22 | 2010-10-05 | processo para polimerização de olefina(s) na presença de uma sistema catalisador, sistemas catalisadores e uso de um composto catalisador. | |
US6271323B1 (en) * | 1999-10-28 | 2001-08-07 | Univation Technologies, Llc | Mixed catalyst compounds, catalyst systems and their use in a polymerization process |
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KR20060018849A (ko) * | 2003-05-12 | 2006-03-02 | 유니온 카바이드 케미칼즈 앤드 플라스틱스 테크날러지 코포레이션 | 기상 중합에서 중합체 미세물질의 제어 방법 |
US7087687B2 (en) * | 2003-08-21 | 2006-08-08 | Rohm And Haas Company | Catalytic composition and its preparation and use for preparing polymers from ethylenically unsaturated monomers |
US7288596B2 (en) * | 2003-12-22 | 2007-10-30 | Univation Technologies, Llc | Polyethylene compositions having improved tear properties |
US20050182210A1 (en) * | 2004-02-17 | 2005-08-18 | Natarajan Muruganandam | De-foaming spray dried catalyst slurries |
JP2005290098A (ja) * | 2004-03-31 | 2005-10-20 | Sumitomo Chemical Co Ltd | メタロセン系遷移金属化合物の溶液の製造方法および保存方法 |
RU41300U1 (ru) | 2004-06-09 | 2004-10-20 | Беляев Анатолий Иванович | Контейнер для транспортирования и хранения скоропортящегося груза |
US7193017B2 (en) * | 2004-08-13 | 2007-03-20 | Univation Technologies, Llc | High strength biomodal polyethylene compositions |
US7312279B2 (en) * | 2005-02-07 | 2007-12-25 | Univation Technologies, Llc | Polyethylene blend compositions |
US8088871B2 (en) | 2006-11-14 | 2012-01-03 | Univation Technologies, Llc | Catalyst systems and polymerization processes |
-
2007
- 2007-11-13 US US12/514,547 patent/US8088871B2/en active Active
- 2007-11-13 RU RU2009122450/04A patent/RU2452740C2/ru active
- 2007-11-13 EP EP07840022.3A patent/EP2081968B1/en active Active
- 2007-11-13 MX MX2009005152A patent/MX345881B/es active IP Right Grant
- 2007-11-13 KR KR1020097012143A patent/KR101540820B1/ko active IP Right Grant
- 2007-11-13 AU AU2007319883A patent/AU2007319883B2/en active Active
- 2007-11-13 WO PCT/US2007/023749 patent/WO2008060512A1/en active Search and Examination
- 2007-11-13 CN CN2007800421969A patent/CN101541838B/zh active Active
- 2007-11-13 BR BRPI0718849A patent/BRPI0718849B1/pt active IP Right Grant
- 2007-11-13 CA CA2668880A patent/CA2668880C/en active Active
- 2007-11-13 JP JP2009537174A patent/JP5676106B2/ja active Active
- 2007-11-13 ES ES07840022.3T patent/ES2549693T3/es active Active
- 2007-11-13 MY MYPI20091926A patent/MY157264A/en unknown
- 2007-11-13 BR BR122018006662-8A patent/BR122018006662B1/pt active IP Right Grant
-
2009
- 2009-04-08 ZA ZA200902461A patent/ZA200902461B/xx unknown
-
2011
- 2011-11-22 US US13/302,622 patent/US8563458B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
CA2668880A1 (en) | 2008-05-22 |
MY157264A (en) | 2016-05-31 |
ZA200902461B (en) | 2010-04-28 |
BRPI0718849A2 (pt) | 2014-02-25 |
RU2452740C2 (ru) | 2012-06-10 |
RU2009122450A (ru) | 2010-12-20 |
BRPI0718849A8 (pt) | 2017-12-26 |
US20100063227A1 (en) | 2010-03-11 |
CN101541838B (zh) | 2013-10-30 |
WO2008060512A1 (en) | 2008-05-22 |
ES2549693T3 (es) | 2015-10-30 |
EP2081968A1 (en) | 2009-07-29 |
BRPI0718849B1 (pt) | 2018-11-27 |
US8563458B2 (en) | 2013-10-22 |
KR20090094276A (ko) | 2009-09-04 |
BR122018006662B1 (pt) | 2019-07-09 |
CN101541838A (zh) | 2009-09-23 |
EP2081968A4 (en) | 2011-07-27 |
EP2081968B1 (en) | 2015-09-16 |
US20120065054A1 (en) | 2012-03-15 |
KR101540820B1 (ko) | 2015-07-30 |
AU2007319883B2 (en) | 2012-12-13 |
AU2007319883A1 (en) | 2008-05-22 |
CA2668880C (en) | 2016-04-26 |
US8088871B2 (en) | 2012-01-03 |
MX345881B (es) | 2016-03-07 |
JP2010509484A (ja) | 2010-03-25 |
JP5676106B2 (ja) | 2015-02-25 |
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