MX173526B - Procedimiento para la preparacion de las sales no toxicas del 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-on-2,2-dioxido - Google Patents
Procedimiento para la preparacion de las sales no toxicas del 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-on-2,2-dioxidoInfo
- Publication number
- MX173526B MX173526B MX003636A MX363686A MX173526B MX 173526 B MX173526 B MX 173526B MX 003636 A MX003636 A MX 003636A MX 363686 A MX363686 A MX 363686A MX 173526 B MX173526 B MX 173526B
- Authority
- MX
- Mexico
- Prior art keywords
- dihydro
- methyl
- water
- dioxide
- salts
- Prior art date
Links
- 150000003839 salts Chemical class 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 3
- 231100000252 nontoxic Toxicity 0.000 title abstract 3
- 230000003000 nontoxic effect Effects 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
- 239000012074 organic phase Substances 0.000 abstract 3
- YGCFIWIQZPHFLU-UHFFFAOYSA-N acesulfame Chemical compound CC1=CC(=O)NS(=O)(=O)O1 YGCFIWIQZPHFLU-UHFFFAOYSA-N 0.000 abstract 2
- GCPWJFKTWGFEHH-UHFFFAOYSA-N acetoacetamide Chemical class CC(=O)CC(N)=O GCPWJFKTWGFEHH-UHFFFAOYSA-N 0.000 abstract 2
- 238000000605 extraction Methods 0.000 abstract 2
- 238000006386 neutralization reaction Methods 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 238000006798 ring closing metathesis reaction Methods 0.000 abstract 2
- QXBGLCSYJYZBFK-UHFFFAOYSA-N 3-oxobutanoylsulfamic acid Chemical compound CC(=O)CC(=O)NS(O)(=O)=O QXBGLCSYJYZBFK-UHFFFAOYSA-N 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 229910001867 inorganic solvent Inorganic materials 0.000 abstract 1
- 239000003049 inorganic solvent Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- 238000007363 ring formation reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D291/00—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms
- C07D291/02—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms not condensed with other rings
- C07D291/06—Six-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Seasonings (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19853531358 DE3531358A1 (de) | 1985-09-03 | 1985-09-03 | Verfahren zur herstellung der nicht-toxischen salze des 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxids |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX173526B true MX173526B (es) | 1994-03-14 |
Family
ID=6279975
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX003636A MX173526B (es) | 1985-09-03 | 1986-09-03 | Procedimiento para la preparacion de las sales no toxicas del 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-on-2,2-dioxido |
Country Status (23)
| Country | Link |
|---|---|
| US (1) | US4804755A (Direct) |
| EP (1) | EP0218076B1 (Direct) |
| JP (1) | JPS6256481A (Direct) |
| KR (1) | KR940008749B1 (Direct) |
| CN (1) | CN1008736B (Direct) |
| AR (1) | AR248016A1 (Direct) |
| AT (1) | ATE49201T1 (Direct) |
| AU (1) | AU587855B2 (Direct) |
| BR (1) | BR8604201A (Direct) |
| CA (1) | CA1283913C (Direct) |
| CS (1) | CS262439B2 (Direct) |
| DD (1) | DD249272A5 (Direct) |
| DE (2) | DE3531358A1 (Direct) |
| DK (1) | DK168045B1 (Direct) |
| ES (1) | ES2000617A6 (Direct) |
| FI (1) | FI83077C (Direct) |
| HU (1) | HU200758B (Direct) |
| IE (1) | IE59132B1 (Direct) |
| IL (1) | IL79894A (Direct) |
| MX (1) | MX173526B (Direct) |
| NO (1) | NO163856C (Direct) |
| SU (1) | SU1582988A3 (Direct) |
| ZA (1) | ZA866647B (Direct) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3429039A1 (de) * | 1984-08-07 | 1986-02-20 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen |
| DE3531359A1 (de) * | 1985-09-03 | 1987-03-12 | Hoechst Ag | Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid sowie zu dessen reinigung |
| TW223067B (Direct) * | 1992-03-17 | 1994-05-01 | Hoechst Ag | |
| DE10253773B3 (de) * | 2002-11-19 | 2004-06-24 | Nutrinova Nutrition Specialties & Food Ingredients Gmbh | Verwendung von Acesulfamsäure zur pH-Wert-Absenkung |
| JP2005263779A (ja) * | 2004-02-17 | 2005-09-29 | Daicel Chem Ind Ltd | ３，４−ジヒドロ−１，２，３−オキサチアジン−４−オン−２，２−ジオキサイド化合物又はその塩の製造法 |
| JP2008037778A (ja) * | 2006-08-03 | 2008-02-21 | Daicel Chem Ind Ltd | ３，４−ジヒドロ−１，２，３−オキサチアジン−４−オン−２，２−ジオキサイド化合物又はその塩の製造法 |
| JP2008037777A (ja) * | 2006-08-03 | 2008-02-21 | Daicel Chem Ind Ltd | ３，４−ジヒドロ−１，２，３−オキサチアジン−４−オン−２，２−ジオキサイド化合物のカリウム塩の製造方法 |
| US9024016B2 (en) | 2012-06-08 | 2015-05-05 | Nutrinova Nutrition Specialists & Food Ingredients GmbH | Process for producing acesulfame potassium |
| JP6912582B2 (ja) | 2016-09-21 | 2021-08-04 | セラニーズ・インターナショナル・コーポレーション | アセスルファムカリウム組成物及びその製造方法 |
| EP3623363A1 (en) | 2016-09-21 | 2020-03-18 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| CN119192099A (zh) | 2016-09-21 | 2024-12-27 | 国际人造丝公司 | 乙酰舒泛钾组合物和用于生产其的方法 |
| SI3319949T1 (sl) * | 2016-09-21 | 2020-11-30 | Celanese International Corporation, | Sestavki kalijevega acesulfama in postopki za njihovo izdelavo |
| CN109369572A (zh) * | 2018-10-25 | 2019-02-22 | 苏州浩波科技股份有限公司 | 一种安赛蜜的纯化工艺 |
| CN109593071A (zh) * | 2018-12-10 | 2019-04-09 | 安徽金禾实业股份有限公司 | 一种连续可控的安赛蜜重结晶离心装置及方法 |
| CN112424176A (zh) * | 2020-09-21 | 2021-02-26 | 安徽金禾实业股份有限公司 | 安赛蜜的精制方法 |
| CN116568674A (zh) * | 2021-12-31 | 2023-08-08 | 安徽金禾实业股份有限公司 | 一种对含有乙酰磺胺酸的水解反应产物的处理方法和装置 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2327804C3 (de) * | 1973-06-01 | 1980-08-14 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von 3,4-Dihydro-l,23-oxathiazin-4-onen |
| DE2434548C2 (de) * | 1974-07-18 | 1982-11-18 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Herstellung von Fluoridarmem 6-Methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid-kalium |
| DE2453063A1 (de) * | 1974-11-08 | 1976-05-13 | Hoechst Ag | Verfahren zur herstellung von acetoacetamid-n-sulfofluorid |
| DE3410439A1 (de) * | 1984-03-22 | 1985-09-26 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen sowie der dabei als zwischenprodukt(e) auftretenden acetoacetamind-n-sulfonsaeure(salze) |
| DE3410440A1 (de) * | 1984-03-22 | 1985-09-26 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid und dessen nichttoxischen salzen |
| DE3531359A1 (de) * | 1985-09-03 | 1987-03-12 | Hoechst Ag | Verfahren zur herstellung von 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-on-2,2-dioxid sowie zu dessen reinigung |
-
1985
- 1985-09-03 DE DE19853531358 patent/DE3531358A1/de not_active Withdrawn
-
1986
- 1986-08-27 AT AT86111841T patent/ATE49201T1/de not_active IP Right Cessation
- 1986-08-27 EP EP86111841A patent/EP0218076B1/de not_active Expired - Lifetime
- 1986-08-27 DE DE8686111841T patent/DE3667972D1/de not_active Expired - Lifetime
- 1986-08-29 CA CA000517246A patent/CA1283913C/en not_active Expired - Lifetime
- 1986-08-29 US US06/902,427 patent/US4804755A/en not_active Expired - Lifetime
- 1986-09-01 HU HU863764A patent/HU200758B/hu not_active IP Right Cessation
- 1986-09-01 ES ES8601536A patent/ES2000617A6/es not_active Expired
- 1986-09-01 IL IL79894A patent/IL79894A/xx not_active IP Right Cessation
- 1986-09-01 CS CS866323A patent/CS262439B2/cs not_active IP Right Cessation
- 1986-09-01 DD DD86294054A patent/DD249272A5/de not_active IP Right Cessation
- 1986-09-01 FI FI863523A patent/FI83077C/fi not_active IP Right Cessation
- 1986-09-01 SU SU864028038A patent/SU1582988A3/ru active
- 1986-09-02 ZA ZA866647A patent/ZA866647B/xx unknown
- 1986-09-02 AU AU62173/86A patent/AU587855B2/en not_active Expired
- 1986-09-02 BR BR8604201A patent/BR8604201A/pt not_active IP Right Cessation
- 1986-09-02 IE IE234486A patent/IE59132B1/en not_active IP Right Cessation
- 1986-09-02 NO NO863504A patent/NO163856C/no not_active IP Right Cessation
- 1986-09-02 CN CN86105877A patent/CN1008736B/zh not_active Expired
- 1986-09-02 JP JP61205245A patent/JPS6256481A/ja active Granted
- 1986-09-02 DK DK418186A patent/DK168045B1/da not_active IP Right Cessation
- 1986-09-03 MX MX003636A patent/MX173526B/es unknown
- 1986-09-03 KR KR1019860007363A patent/KR940008749B1/ko not_active Expired - Lifetime
- 1986-09-11 AR AR86305109A patent/AR248016A1/es active
Also Published As
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| MX173526B (es) | Procedimiento para la preparacion de las sales no toxicas del 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-on-2,2-dioxido | |
| MX173525B (es) | Mejoras en un procedimiento para la preparacion de 6-metil-3,4-dihidro-1,2,3-oxatiazin-4-ona-2,2-dioxido por cierre de anillo de un derivado de acetoacetamida | |
| IL74676A (en) | Process for the preparation of 6-methyl-3-,4-dihydro-1,2,3-oxathiazin-4-one 2,2-dioxide and its non-toxic salts,and the acetoacetamide-n-sulfonic acid(salts)which occur as intermediate(s)in this process | |
| ATE16598T1 (de) | Verfahren zur herstellung von sulfonierten arylphosphinen. | |
| DK247387D0 (da) | Fremgangsmaade til indvinding af en aminosyre fra en vanding oploesning | |
| TR21939A (tr) | Islak usullue fosforik asidin aritilmasina mahsus usul | |
| ES8301971A1 (es) | Un proceso para la preparacion de derivados de n-alquilimi- dazoles sustituidos | |
| ES2172914T3 (es) | Procedimiento de tratamiento de soluciones acuosas que comprenden acidos y compuestos nitrados. | |
| MX172704B (es) | Procedimiento para la purificacion de acidos parafinicos sulfonicos | |
| BE900170A (fr) | Procede de purification de l'acide phosphorique par extraction par solvant. | |
| ATE53383T1 (de) | Reinigung von aromatischen kohlenwasserstoffthioaminen. | |
| ES495482A0 (es) | Procedimiento para la recuperacion de acidos carboxilicos a partir de mezclas que contienen esteres de glicoles deriva- dos de estos acidos | |
| GB1519913A (en) | Purification of naphthalene | |
| DK229088A (da) | Fremgangsmaade til fremstilling af propanon-1,3-disulfonsyre | |
| AR034596A1 (es) | Procedimiento para la preparacion de n-fosfonometilglicina | |
| SE7708777L (sv) | Raffineringsforfarande for sackarin-natrium | |
| FR2409252A1 (fr) | Procede de purification de l'acide p-tolylique obtenu par oxydation du p-xylene | |
| GB899386A (en) | d-2-phenyl-3-methyltetrahydro-1,4-oxazine and a method of manufacturing same | |
| DE3761976D1 (de) | Verfahren zur abtrennung von schwefelsaeure aus waesserigen loesungen, die sie zusammen mit alkansulfonsaeuren enthalten. | |
| IT1165139B (it) | Metodo per il recupero di acido omega-ammino-dodecanoico da acque di cristallizzazione | |
| JPS5675450A (en) | Preparation of 2,3-dimethoxy-5-methyl-1,4-benzoquinone | |
| UA8331A1 (uk) | Спосіб одержання 6-метіл-3, 4-дигідро-1, 2, 3,оксатиазин-4-он-2, 2-диоксиду | |
| JPS5785359A (en) | Preparation of chlorobenzenesulfochloride (chlorobenzenesulfonyl chloride) |