MX169298B - Procedimiento para recuperar azufre de los gases que lo contienen - Google Patents
Procedimiento para recuperar azufre de los gases que lo contienenInfo
- Publication number
- MX169298B MX169298B MX006060A MX606087A MX169298B MX 169298 B MX169298 B MX 169298B MX 006060 A MX006060 A MX 006060A MX 606087 A MX606087 A MX 606087A MX 169298 B MX169298 B MX 169298B
- Authority
- MX
- Mexico
- Prior art keywords
- gas
- oxidation
- stage
- hydrogen sulfide
- catalytic
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/85—Chromium, molybdenum or tungsten
- B01J23/86—Chromium
- B01J23/862—Iron and chromium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/02—Preparation of sulfur; Purification
- C01B17/04—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides
- C01B17/0404—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides by processes comprising a dry catalytic conversion of hydrogen sulfide-containing gases, e.g. the Claus process
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/02—Preparation of sulfur; Purification
- C01B17/04—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides
- C01B17/0404—Preparation of sulfur; Purification from gaseous sulfur compounds including gaseous sulfides by processes comprising a dry catalytic conversion of hydrogen sulfide-containing gases, e.g. the Claus process
- C01B17/0452—Process control; Start-up or cooling-down procedures of the Claus process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Automation & Control Theory (AREA)
- Materials Engineering (AREA)
- Treating Waste Gases (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Catalysts (AREA)
- Sampling And Sample Adjustment (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Gas Separation By Absorption (AREA)
- Glass Compositions (AREA)
- Industrial Gases (AREA)
Abstract
La presente invención se refiere a un procedimiento para recuperación de azufre de un gas que contiene sulfuro de hidrógeno, que consiste de oxidar el sulfuro de hidrógeno con oxígeno, y luego hacer reaccionar el gas producido de esta oxidación además usando por lo menos dos etapas catalíticas, de conformidad con la ecuación: 2H2S + SO2 2H2O + 3/n Sn, caracterizado en que la concentración del H2S en el gas que sale de la última etapa catalítica se controla, para tener un valor que varía entre 0.8 y 3 por ciento en volumen, reduciendo la cantidad del aire de combustión u oxidación que se hace pasar hacia la etapa de oxidación y/o ocasionando que una porción del gas del material de alimentación que contiene sulfuro de hidrógeno se desvíe de la etapa de oxidación y se añada al agas que fluye hacia una etapa catalítica.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL8600960A NL8600960A (nl) | 1986-04-16 | 1986-04-16 | Werkwijze voor het winnen van zwavel uit zwavelhoudende gassen. |
Publications (1)
Publication Number | Publication Date |
---|---|
MX169298B true MX169298B (es) | 1993-06-29 |
Family
ID=19847883
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX006060A MX169298B (es) | 1986-04-16 | 1987-04-14 | Procedimiento para recuperar azufre de los gases que lo contienen |
Country Status (21)
Country | Link |
---|---|
US (1) | US4988494A (es) |
EP (1) | EP0242006B1 (es) |
JP (1) | JPS62297202A (es) |
CN (1) | CN1015536B (es) |
AT (1) | ATE78794T1 (es) |
AU (1) | AU583982B2 (es) |
BR (1) | BR8701855A (es) |
CA (1) | CA1323173C (es) |
DE (1) | DE3780682T2 (es) |
DK (1) | DK168700B1 (es) |
ES (1) | ES2033800T3 (es) |
FI (1) | FI81073C (es) |
GR (1) | GR3005393T3 (es) |
IN (1) | IN169395B (es) |
MX (1) | MX169298B (es) |
NL (1) | NL8600960A (es) |
NO (1) | NO173134C (es) |
PT (1) | PT84677B (es) |
SU (1) | SU1709900A3 (es) |
UA (1) | UA5550A1 (es) |
YU (1) | YU45819B (es) |
Families Citing this family (50)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2023009A1 (en) * | 1989-09-19 | 1991-03-20 | Kenneth R. Stamper | Sulfur recovery process |
CA2027764A1 (en) * | 1989-12-29 | 1991-06-30 | Richard D. Skinner | Sulfur recovery process |
GB9025846D0 (en) * | 1990-11-28 | 1991-01-09 | Boc Group Plc | Treatment of gas |
US5304361A (en) * | 1992-06-26 | 1994-04-19 | Union Carbide Chemicals & Plastics Technology Corporation | Removal of hydrogen sulfide |
US5266274A (en) * | 1992-10-13 | 1993-11-30 | Tpa, Inc. | Oxygen control system for a sulfur recovery unit |
EP0631978B1 (en) * | 1993-06-28 | 1996-05-08 | Shell Internationale Researchmaatschappij B.V. | Removing hydrogen sulphide from a gas stream |
US5897850A (en) * | 1993-11-30 | 1999-04-27 | Comprimo B.V. | Process for removing elemental sulfur from a gas stream |
DE4409203A1 (de) * | 1994-03-17 | 1995-09-21 | Linde Ag | Verfahren zur Gewinnung von elementarem Schwefel aus einem H¶2¶S enthaltenden Gasgemisch |
US5556606A (en) * | 1994-10-07 | 1996-09-17 | Khanmamedov; Tofik K. | Method and apparatus for controlling the hydrogen sulfide concentration in the acid gas feedstock of a sulfur recovery unit |
DE69412839T2 (de) * | 1994-12-23 | 1999-03-18 | Shell Internationale Research Maatschappij B.V., Den Haag/S'gravenhage | Entfernung von Schwefelwasserstoff aus einem Gasstrom |
US5965100A (en) * | 1995-04-25 | 1999-10-12 | Khanmamedov; Tofik K. | Process for recovery of sulfur from an acid gas stream |
FR2740704B1 (fr) * | 1995-11-03 | 1997-12-26 | Elf Aquitaine | Procede d'elimination quasi totale des composes soufres h2s, so2, cos et/ou cs2 contenus dans un gaz residuaire d'usine a soufre, avec recuperation desdits composes sous la forme de soufre |
FR2768512B1 (fr) * | 1997-09-18 | 1999-12-17 | Inst Francais Du Petrole | Methode de preparation de l'h2s pour une analyse isotopique |
EP1115472B1 (en) | 1998-08-25 | 2003-07-30 | Gastec N.V. | A process for the recovery of sulphur from a hydrogen sulphide, containing gas |
US6214311B1 (en) * | 1998-09-21 | 2001-04-10 | Kam-Wang Vincent Kwong | Process for direct reduction of sulfur compounds to elemental sulfur in combination with the claus process |
EP1171381B1 (en) | 1999-04-07 | 2002-12-11 | The Boc Group, Inc. | Treatment of combustible gas streams containing hydrogen sulphide |
US6800269B2 (en) | 1999-07-30 | 2004-10-05 | Conocophillips Company | Short contact time catalytic sulfur recovery system for removing H2S from a waste gas stream |
US6946111B2 (en) | 1999-07-30 | 2005-09-20 | Conocophilips Company | Short contact time catalytic partial oxidation process for recovering sulfur from an H2S containing gas stream |
US6403051B1 (en) * | 1999-07-30 | 2002-06-11 | Conoco Inc. | Recovery of sulfur from H2S and concurrent production of H2 using short contact time CPOX |
US6579510B2 (en) | 1999-07-30 | 2003-06-17 | Alfred E. Keller | SPOX-enhanced process for production of synthesis gas |
US7122170B2 (en) * | 2000-07-25 | 2006-10-17 | Conocophillips Company | Catalysts for SPOC™ enhanced synthesis gas production |
EP1186571A1 (en) * | 2000-09-12 | 2002-03-13 | Gastec N.V. | Process for the selective oxidation of hydrogen sulphide to elemental sulphur |
EP1295848A1 (en) * | 2000-09-12 | 2003-03-26 | Gastec N.V. | Process for the selective oxidation of hydrogen sulphide to elemental sulphur |
US7326397B2 (en) * | 2000-12-18 | 2008-02-05 | Conocophillips Company | Catalytic partial oxidation process for recovering sulfur from an H2S-containing gas stream |
US7357908B2 (en) * | 2000-12-18 | 2008-04-15 | Conocophillips Company | Apparatus and catalytic partial oxidation process for recovering sulfur from an H2S-containing gas stream |
WO2005042130A1 (en) * | 2003-10-31 | 2005-05-12 | Metal Alloy Reclaimers, Inc Ii | Process for reduction of inorganic contaminants from waste streams |
CA2455011C (en) | 2004-01-09 | 2011-04-05 | Suncor Energy Inc. | Bituminous froth inline steam injection processing |
US7108842B2 (en) * | 2004-01-15 | 2006-09-19 | Conocophillips Company | Process for the catalytic partial oxidation of H2S using staged addition of oxygen |
EP1555241A1 (en) * | 2004-01-16 | 2005-07-20 | Jacobs Nederland B.V. | Recovery of sulfur from a hydrogen sulfide containing gas |
CN1321882C (zh) * | 2005-06-15 | 2007-06-20 | 石家庄开发区精致化工技术有限公司 | 一种连续硫回收装置 |
FR2897860B1 (fr) * | 2006-02-27 | 2008-05-30 | Total Sa | Procede d'optimisation de la marche des unites claus. |
US7226572B1 (en) | 2006-03-03 | 2007-06-05 | Conocophillips Company | Compact sulfur recovery plant and process |
US7501111B2 (en) | 2006-08-25 | 2009-03-10 | Conoco Phillips Company | Increased capacity sulfur recovery plant and process for recovering elemental sulfur |
EP1902769A1 (en) * | 2006-09-22 | 2008-03-26 | Jacobs Nederland B.V. | Process for the recovery of sulfur from sulfur containing gases |
PL2160665T3 (pl) * | 2007-06-21 | 2013-09-30 | Fluor Tech Corp | Systemy sterowania zwrotnego dopływem powietrza i sposoby dla jednostek odzyskiwania siarki |
CN101418246B (zh) * | 2008-12-05 | 2013-04-03 | 华陆工程科技有限责任公司 | 一种低温甲醇洗集成克劳斯硫回收系统和工艺 |
WO2010107502A1 (en) * | 2009-03-19 | 2010-09-23 | Crystatech, Inc. | System and method for sour gas well testing |
AU2010270695B2 (en) * | 2009-07-06 | 2016-02-25 | Cruickshank, Cecilia A. | Media for removal of contaminants from fluid streams and method of making and using same |
DE102010013052A1 (de) * | 2010-03-22 | 2011-09-22 | Uhde Gmbh | Vorrichtung und Verfahren zur Kondensation, Abscheidung und Lagerung von flüssigem Schwefel in einer Claus-Anlage |
CN101791517B (zh) * | 2010-04-08 | 2012-05-23 | 北京至清时光环保工程技术有限公司 | 一种从含有硫化氢的酸性气体中回收硫的方法 |
CN104302388A (zh) | 2012-04-23 | 2015-01-21 | 雷普索尔有限公司 | 用于选择性氧化硫化合物的催化剂 |
RU2562481C2 (ru) * | 2014-01-29 | 2015-09-10 | Игорь Анатольевич Мнушкин | Способ и установка получения элементной серы с доочисткой хвостового газа |
RU2694750C2 (ru) * | 2014-12-24 | 2019-07-16 | Прозернат | Удаление сероводорода и регенерация серы из газового потока прямым каталитическим окислением и реакцией клауса |
US10195565B2 (en) | 2014-12-24 | 2019-02-05 | Prosernat | Removal of hydrogen sulfide and sulfur recovery from a gas stream by catalytic direct oxidation and claus reaction |
RU2758897C2 (ru) * | 2016-11-10 | 2021-11-02 | Общество с ограниченной ответственностью научно-исследовательский и проектный институт "ПЕГАЗ" | Установка для получения серы |
WO2018096178A1 (en) * | 2016-11-28 | 2018-05-31 | Haldor Topsøe A/S | Method for production of sulfur and sulfuric acid |
WO2019022603A1 (en) | 2017-07-26 | 2019-01-31 | Wte-Tech B.V. | PROCESS FOR TREATING A SOFT COMPOUND COMPRISING A GAS CHARGE |
WO2020254578A1 (en) | 2019-06-20 | 2020-12-24 | Haldor Topsøe A/S | Method and catalyst for selective oxidation of hydrogen sulfide to elemental sulfur in a reducing gas |
US11530131B1 (en) | 2021-11-16 | 2022-12-20 | Saudi Arabian Oil Company | Methods and systems of sub-dew point sulfur recovery with interstage membrane units |
CN117339385A (zh) * | 2023-12-04 | 2024-01-05 | 上海先普气体技术有限公司 | 原料气处理系统和原料气处理方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE71983C (de) * | H. LlLGE, Lehrer, in Hermsdorf, Reg.-Bez. Breslau | Flurthürschlofs mit zwei Fallen | ||
DE1567774A1 (de) * | 1966-09-07 | 1970-08-20 | Pintsch Bamag Ag | Verfahren zur Entschwefelung des Endgases aus Clausanlagen |
FR1603452A (es) * | 1968-02-02 | 1971-04-19 | ||
USRE28864E (en) * | 1970-12-18 | 1976-06-15 | Societe Anonyme Dite: Societe Nationale Des Petroles D'aquitaine | Process and apparatus for automated regulation of sulphur production units |
NL176160C (nl) * | 1973-10-10 | 1985-03-01 | Comprimo Bv | Werkwijze voor het verbranden van een ammoniak en waterstofsulfide bevattend mengsel van gassen. |
FR2277877A1 (fr) * | 1974-07-11 | 1976-02-06 | Aquitaine Petrole | Procede de desulfuration des gaz contenant de l'hydrogene sulfure |
NL7603622A (en) * | 1976-04-07 | 1977-10-11 | Arend Jan | Lowering the sulphur cpd. content of claus installation effluent - by burning hydrogen sulphide and absorbing sulphur dioxide and hydrogen sulphide in a cooling liq. to form sulphur |
US4311683A (en) * | 1976-06-28 | 1982-01-19 | Union Oil Company Of California | Process for removal of hydrogen sulfide from gas streams |
US4243647A (en) * | 1976-06-28 | 1981-01-06 | Union Oil Company Of California | Process for removal of hydrogen sulfide from gas streams |
US4123507A (en) * | 1976-11-02 | 1978-10-31 | Union Oil Company Of California | Process for removing sulfur and NOx components from a gas stream |
US4100266A (en) * | 1977-09-29 | 1978-07-11 | Phillips Petroleum Company | Control system for a sulfur process |
US4279882A (en) * | 1979-04-27 | 1981-07-21 | Ralph M. Parsons Company | Process for sulfur production |
DE3143400A1 (de) * | 1981-11-02 | 1983-06-01 | Mobil Oil Corp., 10017 New York, N.Y. | Verfahren zur verringerung des schwefelgehaltes in gasstroemen unter gewinnung von elementarem schwefel |
DE3280104D1 (de) * | 1982-02-02 | 1990-03-15 | Union Oil Co | Katalysator und verfahren zum oxydieren von schwefelwasserstoff. |
FR2540092B1 (fr) * | 1983-01-31 | 1986-02-21 | Elf Aquitaine | Procede catalytique de production de soufre a partir d'un gaz renfermant h2s |
DE3311372C2 (de) * | 1983-03-29 | 1986-07-10 | Carl Still Gmbh & Co Kg, 4350 Recklinghausen | Verfahren zur Gewinnung von Schwefel nach dem Claus-Verfahren aus Kokereigas |
SU1214583A1 (ru) * | 1983-05-26 | 1986-02-28 | Азербайджанский Институт Нефти И Химии Им.М.Азизбекова | Способ очистки газа от сероводорода |
NL8600959A (nl) * | 1986-04-16 | 1987-11-16 | Veg Gasinstituut Nv | Katalysator voor de selectieve oxydatie van zwavelhoudende verbindingen, in het bizonder zwavelwaterstof tot elementaire zwavel; werkwijze voor de bereiding van de katalysator alsmede werkwijze voor de selectieve oxydatie van zwavelhoudende verbindingen, in het bizonder zwavelwaterstof tot elementaire zwavel. |
-
1986
- 1986-04-16 NL NL8600960A patent/NL8600960A/nl not_active Application Discontinuation
-
1987
- 1987-04-09 CA CA000534313A patent/CA1323173C/en not_active Expired - Lifetime
- 1987-04-10 DK DK183087A patent/DK168700B1/da not_active IP Right Cessation
- 1987-04-13 FI FI871614A patent/FI81073C/fi not_active IP Right Cessation
- 1987-04-13 NO NO871561A patent/NO173134C/no not_active IP Right Cessation
- 1987-04-13 IN IN273/MAS/87A patent/IN169395B/en unknown
- 1987-04-13 US US07/037,954 patent/US4988494A/en not_active Expired - Lifetime
- 1987-04-14 AU AU71497/87A patent/AU583982B2/en not_active Ceased
- 1987-04-14 MX MX006060A patent/MX169298B/es unknown
- 1987-04-14 PT PT84677A patent/PT84677B/pt unknown
- 1987-04-15 YU YU68387A patent/YU45819B/sh unknown
- 1987-04-15 BR BR8701855A patent/BR8701855A/pt not_active IP Right Cessation
- 1987-04-15 DE DE8787200713T patent/DE3780682T2/de not_active Expired - Lifetime
- 1987-04-15 ES ES198787200713T patent/ES2033800T3/es not_active Expired - Lifetime
- 1987-04-15 EP EP87200713A patent/EP0242006B1/en not_active Expired - Lifetime
- 1987-04-15 AT AT87200713T patent/ATE78794T1/de not_active IP Right Cessation
- 1987-04-16 SU SU4202432A patent/SU1709900A3/ru active
- 1987-04-16 CN CN87103563A patent/CN1015536B/zh not_active Expired
- 1987-04-16 JP JP62094241A patent/JPS62297202A/ja active Granted
- 1987-04-16 UA UA4202432A patent/UA5550A1/uk unknown
-
1992
- 1992-08-10 GR GR920400979T patent/GR3005393T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
PT84677B (pt) | 1989-12-29 |
AU583982B2 (en) | 1989-05-11 |
US4988494A (en) | 1991-01-29 |
FI871614A0 (fi) | 1987-04-13 |
FI871614A (fi) | 1987-10-17 |
JPH0551522B2 (es) | 1993-08-02 |
DK168700B1 (da) | 1994-05-24 |
NO871561L (no) | 1987-10-19 |
DE3780682D1 (de) | 1992-09-03 |
BR8701855A (pt) | 1988-01-26 |
NO871561D0 (no) | 1987-04-13 |
ATE78794T1 (de) | 1992-08-15 |
FI81073C (fi) | 1990-09-10 |
IN169395B (es) | 1991-10-12 |
NO173134B (no) | 1993-07-26 |
UA5550A1 (uk) | 1994-12-28 |
ES2033800T3 (es) | 1993-04-01 |
SU1709900A3 (ru) | 1992-01-30 |
JPS62297202A (ja) | 1987-12-24 |
EP0242006A1 (en) | 1987-10-21 |
CN87103563A (zh) | 1988-01-06 |
YU68387A (en) | 1988-10-31 |
DE3780682T2 (de) | 1992-12-10 |
EP0242006B1 (en) | 1992-07-29 |
DK183087D0 (da) | 1987-04-10 |
PT84677A (en) | 1987-05-01 |
CN1015536B (zh) | 1992-02-19 |
GR3005393T3 (es) | 1993-05-24 |
YU45819B (sh) | 1992-07-20 |
NL8600960A (nl) | 1987-11-16 |
CA1323173C (en) | 1993-10-19 |
FI81073B (fi) | 1990-05-31 |
DK183087A (da) | 1987-10-17 |
AU7149787A (en) | 1987-10-22 |
NO173134C (no) | 1993-11-03 |
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