KR970065513A - N-메틸-n'-니트로구아니딘의 제조 방법 - Google Patents

N-메틸-n'-니트로구아니딘의 제조 방법 Download PDF

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Publication number
KR970065513A
KR970065513A KR1019970009842A KR19970009842A KR970065513A KR 970065513 A KR970065513 A KR 970065513A KR 1019970009842 A KR1019970009842 A KR 1019970009842A KR 19970009842 A KR19970009842 A KR 19970009842A KR 970065513 A KR970065513 A KR 970065513A
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South Korea
Prior art keywords
nitroguanidine
methyl
preparing
formula
reacting
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KR1019970009842A
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English (en)
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KR100434991B1 (ko
Inventor
갈렌캄프 베른트
로에 로타르
Original Assignee
클라우스 로이터, 귄터 슈마허
바이엘 악티엔게젤샤프트
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Application filed by 클라우스 로이터, 귄터 슈마허, 바이엘 악티엔게젤샤프트 filed Critical 클라우스 로이터, 귄터 슈마허
Publication of KR970065513A publication Critical patent/KR970065513A/ko
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Publication of KR100434991B1 publication Critical patent/KR100434991B1/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C279/00—Derivatives of guanidine, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
    • C07C279/30—Derivatives of guanidine, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of guanidine groups bound to nitro or nitroso groups
    • C07C279/32—N-nitroguanidines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C279/00—Derivatives of guanidine, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
    • C07C279/30—Derivatives of guanidine, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups having nitrogen atoms of guanidine groups bound to nitro or nitroso groups
    • C07C279/32—N-nitroguanidines
    • C07C279/36—Substituted N-nitroguanidines

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

본 발명은 0 내지 40℃에서 니트로구아니딘을 메틸아민 수용액과 반응시키는 신규한 N-메틸-N′-니트로구아니딘의 제조방법에 관한 것이다.

Description

N-메틸-N'-니트로구아니딘의 제조 방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (1)

  1. 0℃ 내지 40℃ 사이의 온도에서 구조식 (Ⅱ)의 니트로구아니딘을 메틸아민수용액과 반응시킴을 특징으로 하는 구조식 (Ⅰ)의 N-메틸-N′-니트로구아니딘의 제조 방법:
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019970009842A 1996-03-25 1997-03-21 N-메틸-n'-니트로구아니딘의 제조 방법 KR100434991B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19611654A DE19611654A1 (de) 1996-03-25 1996-03-25 Verfahren zur Herstellung von N-Methyl-N'-nitroguanidin
DE19611654.6 1996-03-25

Publications (2)

Publication Number Publication Date
KR970065513A true KR970065513A (ko) 1997-10-13
KR100434991B1 KR100434991B1 (ko) 2004-09-08

Family

ID=7789289

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019970009842A KR100434991B1 (ko) 1996-03-25 1997-03-21 N-메틸-n'-니트로구아니딘의 제조 방법

Country Status (9)

Country Link
US (1) US5783734A (ko)
EP (1) EP0798293B1 (ko)
JP (1) JP3927274B2 (ko)
KR (1) KR100434991B1 (ko)
CN (1) CN1065526C (ko)
DE (2) DE19611654A1 (ko)
ES (1) ES2150714T3 (ko)
HK (1) HK1002070A1 (ko)
TW (1) TW362094B (ko)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19712411A1 (de) 1997-03-25 1998-10-01 Bayer Ag Verfahren zur Herstellung von 1,3-disubstituierten 2-Nitroguanidinen
CN1207279C (zh) * 1998-11-25 2005-06-22 狄纳米特诺贝尔爆炸材料和系统技术股份有限公司 制备n－烷基－n′－硝基胍的方法
DE19939609A1 (de) * 1999-08-20 2001-02-22 Nigu Chemie Gmbh Verfahren zur Herstellung von 1-Methyl-3-nitroguanidin
DE10000891A1 (de) * 2000-01-12 2001-07-19 Bayer Ag Verfahren zur Herstellung von N-Methyl-N'-nitroguanidin
DE10003834A1 (de) * 2000-01-28 2001-08-02 Nigu Chemie Gmbh Verfahren zur Herstellung von 1-Methyl-3-nitroguanidin
CN101565392A (zh) * 2008-04-21 2009-10-28 南通天泽化工有限公司 一种甲基硝基胍及其制备方法
CN103172545A (zh) * 2013-04-02 2013-06-26 常州大学 一种微通道反应器制备硝基胍的方法
CN103641746B (zh) * 2013-11-22 2016-03-30 青岛文创科技有限公司 一种n-甲基-n’硝基胍的合成工艺
CN106986790A (zh) * 2017-05-25 2017-07-28 宁夏贝利特生物科技有限公司 用生产硝基胍后的稀硫酸生产n‑甲基‑n′‑硝基胍的方法
CN107382789A (zh) * 2017-06-29 2017-11-24 南通天泽化工有限公司 一种甲基硝基胍的制备方法
CN107698466A (zh) * 2017-11-09 2018-02-16 宁夏贝利特生物科技有限公司 一种n‑甲基‑n′‑硝基胍的制备方法
CN109053498A (zh) * 2018-09-27 2018-12-21 南通天泽化工有限公司 一种1-甲基-1,2-二硝基胍的制备方法
CN110128300A (zh) * 2019-05-10 2019-08-16 宁夏贝利特生物科技有限公司 一种制备1-甲基-3-硝基胍的方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2559085A (en) * 1948-10-22 1951-07-03 Honorary Advisory Council Sci Preparation of n-substituted-n'-nitroguanidines

Also Published As

Publication number Publication date
JP3927274B2 (ja) 2007-06-06
EP0798293A1 (de) 1997-10-01
JPH09255651A (ja) 1997-09-30
CN1065526C (zh) 2001-05-09
ES2150714T3 (es) 2000-12-01
TW362094B (en) 1999-06-21
EP0798293B1 (de) 2000-08-09
KR100434991B1 (ko) 2004-09-08
CN1163888A (zh) 1997-11-05
US5783734A (en) 1998-07-21
DE19611654A1 (de) 1997-10-02
DE59702117D1 (de) 2000-09-14
HK1002070A1 (en) 1998-07-31

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