KR960037785A - 히드록실 작용기 및 카르복실 작용기를 포함하는 라텍스 분산액 및 도포제의 제조를 위한 그의 용도 - Google Patents
히드록실 작용기 및 카르복실 작용기를 포함하는 라텍스 분산액 및 도포제의 제조를 위한 그의 용도 Download PDFInfo
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- KR960037785A KR960037785A KR1019960013304A KR19960013304A KR960037785A KR 960037785 A KR960037785 A KR 960037785A KR 1019960013304 A KR1019960013304 A KR 1019960013304A KR 19960013304 A KR19960013304 A KR 19960013304A KR 960037785 A KR960037785 A KR 960037785A
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- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 title claims abstract 6
- 239000006185 dispersion Substances 0.000 title claims abstract 4
- 239000004816 latex Substances 0.000 title claims 3
- 229920000126 latex Polymers 0.000 title claims 3
- 238000000576 coating method Methods 0.000 title 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 title 1
- 238000002360 preparation method Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 claims abstract 29
- 239000002245 particle Substances 0.000 claims abstract 13
- 239000008346 aqueous phase Substances 0.000 claims abstract 6
- 229920001577 copolymer Polymers 0.000 claims abstract 4
- 230000002378 acidificating effect Effects 0.000 claims abstract 3
- 239000011248 coating agent Substances 0.000 claims abstract 3
- 239000003973 paint Substances 0.000 claims abstract 2
- 239000007787 solid Substances 0.000 claims abstract 2
- 239000002966 varnish Substances 0.000 claims abstract 2
- 125000003158 alcohol group Chemical group 0.000 claims 5
- 125000000524 functional group Chemical group 0.000 claims 5
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims 5
- 239000002253 acid Substances 0.000 claims 4
- 150000002009 diols Chemical class 0.000 claims 3
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 claims 3
- 239000012948 isocyanate Substances 0.000 claims 3
- 150000002513 isocyanates Chemical class 0.000 claims 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 2
- 239000005977 Ethylene Substances 0.000 claims 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 2
- 150000001298 alcohols Chemical class 0.000 claims 2
- 239000000178 monomer Substances 0.000 claims 2
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 claims 1
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical group C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 206010061218 Inflammation Diseases 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 150000001735 carboxylic acids Chemical class 0.000 claims 1
- 238000007334 copolymerization reaction Methods 0.000 claims 1
- 239000003995 emulsifying agent Substances 0.000 claims 1
- 239000000839 emulsion Substances 0.000 claims 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims 1
- 230000004054 inflammatory process Effects 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 239000000049 pigment Substances 0.000 claims 1
- 238000006116 polymerization reaction Methods 0.000 claims 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 claims 1
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- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/062—Copolymers with monomers not covered by C09D133/06
- C09D133/066—Copolymers with monomers not covered by C09D133/06 containing -OH groups
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/12—Esters of monohydric alcohols or phenols
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/62—Polymers of compounds having carbon-to-carbon double bonds
- C08G18/6216—Polymers of alpha-beta ethylenically unsaturated carboxylic acids or of derivatives thereof
- C08G18/625—Polymers of alpha-beta ethylenically unsaturated carboxylic acids; hydrolyzed polymers of esters of these acids
- C08G18/6254—Polymers of alpha-beta ethylenically unsaturated carboxylic acids and of esters of these acids containing hydroxy groups
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/703—Isocyanates or isothiocyanates transformed in a latent form by physical means
- C08G18/705—Dispersions of isocyanates or isothiocyanates in a liquid medium
- C08G18/706—Dispersions of isocyanates or isothiocyanates in a liquid medium the liquid medium being water
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- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/728—Polymerisation products of compounds having carbon-to-carbon unsaturated bonds and having isocyanate or isothiocyanate groups or groups forming isocyanate or isothiocyanate groups
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- C08G18/00—Polymeric products of isocyanates or isothiocyanates
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- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/80—Masked polyisocyanates
- C08G18/8061—Masked polyisocyanates masked with compounds having only one group containing active hydrogen
- C08G18/807—Masked polyisocyanates masked with compounds having only one group containing active hydrogen with nitrogen containing compounds
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- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/81—Unsaturated isocyanates or isothiocyanates
- C08G18/8141—Unsaturated isocyanates or isothiocyanates masked
- C08G18/815—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen
- C08G18/8158—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with unsaturated compounds having only one group containing active hydrogen
- C08G18/8175—Polyisocyanates or polyisothiocyanates masked with unsaturated compounds having active hydrogen with unsaturated compounds having only one group containing active hydrogen with esters of acrylic or alkylacrylic acid having only one group containing active hydrogen
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Abstract
본 발명은 경화 후 도포제를 형성시킬 수 있는 수성상 상태의 분산액에 관한 것이다.
입자가 0.2 내지 1.2밀리당량/고형물g의 입수가능한 산성(유리하게는 카르복실) 작용기 함량을 갖는 것을 특징으로 하는, 1종 이상의 수성상 및 크기가 10 내지 1000mm인 (공)중합체(들)의 입자의 모집단 A를 함유하는 분산액으로 구성된 페인트 및 니스용 조성물.
도포시키기 위한 용도.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (29)
1종 이상의 수성상 및 크기가 10 내지 1000mm인 (공)중합체의 입자의 모집단 A를 함유하는 분산액으로 구성된 페인트 및 니스용 조성물에 있어서, 입자가 0.2 내지 1.2 밀리당량/고형물의 g의 입수가능한 산성(유리하게는 카르복실) 작용기 함량을 갖고, 0.3 내지 1.5 밀리당량/g의 입수 가능한 알코올 작용기 함량을 갖는 것을 특징으로 하는 페인트 및 니스용 조성물.
제1항에 있어서, 라텍스 입자의 함량이 10 내지 80질량%, 유리하게는 10 내지 60질량%인 것을 특징으로 하는 조성물.
제1 또는 2항에 있어서, 모집단 A의 입자의 산성 작용기는 pKa가 2 이상, 바람직하게는 3인 약산성 작용기인 것을 특징으로 하는 조성물.
제1 내지 3항 중 어느 한 항에 있어서, 모집단 A의 분산도 (〔d90-d90〕/d90)는 0 내지 1/4인 것을 특징으로 하는 조성물.
제1 내지 4항 중 어느 한 항에 있어서, 활성화 에틸렌 결합을 포함하는 1종 이상의 유리산 및 활성화 에틸렌 작용기를 포함하는 1종 이상의 유리 알코올 사이의 공중합으로부터 (공)중합체 입자가 생성되는 것을 특징으로 하는 조성물.
제1내지 4항 중 어느 한 항에 있어서, (공)중합체의 평균분자량이 5×104내지 5×106인 것을 특징으로 하는 조성물.
제5 또는 6항에 있어서, 활성화 에틸렌 작용기를 포함하는 유리 알코올이 알파-에틸렌산으로 모노에스테르화된 디올인 것을 특징으로 하는 조성물.
제1 내지 7항 중 어느 한 항에 있어서, 활성화 에틸렌 작용기를 포함하는 유리 알코올로 구성된 단량체로부터 생성된 단위체의 함량이 3 내지 15%, 유리하게는 4 내지 10%인 것을 특징으로 하는 조성물.
제7 내지 8항 중의 어느 한 항에 있어서, 디올이 유리하게는 1,3-프로판디올 및 글리콜로부터 선택된 ω, ω'디올인 것을 특징으로 하는 조성물.
제7 내지 9항 중의 어느 한 항에 있어서, 알파-에틸렌산이 치환될 수 있는 아크릴산인 것을 특징으로 하는 조성물,
제5 내지 10항 중 어느 한 항에 있어서, 유리산이 단일치환될 수 있는 아크릴산이거나 이의 염증의 하나인 것을 특징으로 하는 조성물,
제5 내지 11항 중 어느 한 항에 있어서, 유리 카르복실산으로부터 생성된 단위체의 함량이 2 내지 10%(몰)인 것을 특징으로 하는 조성물.
제1 내지 12항 중 어느 한 항에 있어서, 입자는 에피중합을 거친 입자로부터 생성되는 것을 특징으로 하는 조성물.
제1 내지 13항 중 어느 한 항에 있어서, 유화제 함량이 2% 이하, 유리하게는 1% 이하인 것을 특징으로 하는 조성물,
제1 내지 14항 중 어느 한 항에 있어서, 추가로 이소시아네이트 작용기(들)를 갖는 입자의 모집단 B를 포함하는 것을 특징으로 하는 조성물.
제15항에 있어서, 이소시아네이트 작용기는 보호된 것을 특징으로 하는 조성물.
제15 또는 16항에 있어서, 이소시아네이트 작용기 함량이 0.5 내지 1밀리당량/모집단 B 입자의 g인 것을 특징으로 하는 조성물.
제15 내지 17항 중 어느 한 항에 있어서, 모집단 A 및 모집단 B의 질량비는 알코올 작용기 대 이소시아네이트 작용기의 비가 1/10 내지 10, 유리하게는 0.3 내지 5 정도인 것을 특징으로 하는 조성물.
제15 내지 18항 중 어느 한 항에 있어서, 모집단 B가 수성상을 갖는 에멀션을 구성하는 것을 특징으로 하는 조성물.
제15 내지 19항 중 어느 한 항에 있어서, 모집단 B가 수성상을 갖는 라텍스를 구성하는 것을 특징으로 하는 조성물.
제15 내지 20항 중 어느 한 항에 있어서, 모집단 A 및 모집단 B가 함께 유리 카르복실 작용기, 유리 알코올 작용기 및 보호 이소시아네이트를 동시에 포함하는 입자의 모집단을 구성하는 것을 특징으로 하는 조성물.
제21항에 있어서, 보호된 이소시아네이트 대 알코올 작용기의 비(당량)가 0.1 내지 10인 것을 특징으로 하는 조성물.
제21 또는 22항에 있어서, 알코올 작용기 대 카르복실 작용기의 비(당량)가 0.2 내지 5인 것을 특징으로 하는 조성물.
제21 내지 23항 중 어느 한 항에 있어서, 이소시아네이트 대 카르복실 작용기의 비(당량)가 0.1 내지 10인 것을 특징으로 하는 조성물.
제1 내지 24항 중 어느 한 항에 있어서, 추가로 안료를 포함하는 것을 특징으로 하는 조성물.
제1 내지 25항 중 어느 한 항에 있어서, 수성상의 pH가 4 내지 9인 것을 특징으로 하는 조성물.
도포제를 제조하기 위하여 사용하는 제1 내지 26항에서 청구한 조성물.
제1 내지 26항 중 어느 한 항에서 청구한 조성물을 지지체상에 적용하는 단계를 포함하는 것을 특징으로 하는 도포제의 제조 방법.
제28항에 있어서, 조성물이 1종 이상의 보호된 이소시아네이트 작용기를 포함하고, 120 내지 200℃의 온도에서 경화시키는 단계를 포함하는 것을 특징으로 하는 제조 방법.
※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9505123 | 1995-04-28 | ||
| FR9505123A FR2733506B1 (fr) | 1995-04-28 | 1995-04-28 | Dispersions de latex a fonction hydroxyle et a fonction carboxylique et leur utilisation pour fabrication des revetements |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR960037785A true KR960037785A (ko) | 1996-11-19 |
| KR100481264B1 KR100481264B1 (ko) | 2005-11-14 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019960013304A KR100481264B1 (ko) | 1995-04-28 | 1996-04-27 | 히드록시작용기및카르복시작용기를포함하는라텍스분산액을함유하는조성물,및이조성물을사용한도포제의제조방법 |
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| Country | Link |
|---|---|
| EP (2) | EP0860454B1 (ko) |
| JP (1) | JP2788630B2 (ko) |
| KR (1) | KR100481264B1 (ko) |
| CN (1) | CN1076039C (ko) |
| AT (2) | ATE344303T1 (ko) |
| BR (1) | BR9602082A (ko) |
| CA (1) | CA2175149C (ko) |
| DE (2) | DE69636676T2 (ko) |
| DK (1) | DK0739961T3 (ko) |
| ES (2) | ES2270481T3 (ko) |
| FR (1) | FR2733506B1 (ko) |
| HU (1) | HU215178B (ko) |
| MX (1) | MX9601567A (ko) |
| ZA (1) | ZA963265B (ko) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2760242A1 (fr) * | 1997-02-28 | 1998-09-04 | Rhodia Chimie Sa | Revetement pour exterieur, composition utile pour ces revetements et procede d'obtention de ces revetements |
| ATE278726T1 (de) | 1997-02-28 | 2004-10-15 | Rodhia Chimie | Aussenbeschichtung, geeignete zusammensetzung für solche beschichtungen und verfahren zur herstellung solcher beschichtungen |
| DE19913042C2 (de) | 1999-03-23 | 2001-05-03 | Inventa Ag | Haftvermittler für textile Verstärkungseinlagen, Verfahren zur Herstellung und dessen Verwendung |
| US6875834B2 (en) * | 2001-01-30 | 2005-04-05 | Rohm And Haas Company | Two-component coating composition and method of preparation |
| US20060205870A1 (en) * | 2005-03-11 | 2006-09-14 | Eastman Kodak Company | Multifunctional polymer particles and methods of making the same |
| NZ601697A (en) | 2010-03-15 | 2013-09-27 | Synthomer Deutschland Gmbh | Polymer latex useful for the production of textile floor coverings |
| EP2450389B1 (de) | 2010-11-08 | 2015-03-18 | EMS-Patent AG | Haftvermittler für textile Verstärkungseinlagen und dessen Verwendung |
| EP2730563B1 (de) | 2012-11-13 | 2017-01-11 | Ems-Patent Ag | Verfahren zur Herstellung von MDI-Dimer |
| EP2837643B1 (de) | 2013-08-16 | 2018-10-10 | Ems-Patent Ag | Pulverförmiger, in wasser dispergierbarer haftvermittler |
| BR112016023851A2 (pt) | 2014-04-15 | 2017-08-15 | Basf Se | ?composição de revestimento de duas partes e método para revestir uma superfície? |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4177076A (en) * | 1977-04-15 | 1979-12-04 | Nippon Oil Company, Ltd. | Water or alcohol soluble printing ink composition |
| DE2749691C2 (de) * | 1977-11-07 | 1986-01-30 | Basf Ag, 6700 Ludwigshafen | Wärmehärtbare selbstvernetzende wäßrige Überzugsmittel |
| DE3318147A1 (de) * | 1983-05-18 | 1984-11-22 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von, isocyanuratgruppen und olefinische doppelbindungen aufweisenden verbindungen, die nach diesem verfahren erhaeltlichen verbindungen und ihre verwendung als bindemittel bzw. bindemittelkomponente in ueberzugsmitteln |
| JPH05148313A (ja) * | 1991-09-12 | 1993-06-15 | Dainippon Ink & Chem Inc | 架橋粒子の製法及び塗料 |
-
1995
- 1995-04-28 FR FR9505123A patent/FR2733506B1/fr not_active Expired - Fee Related
-
1996
- 1996-04-17 DE DE69636676T patent/DE69636676T2/de not_active Expired - Lifetime
- 1996-04-17 DE DE69600900T patent/DE69600900T2/de not_active Revoked
- 1996-04-17 ES ES98107203T patent/ES2270481T3/es not_active Expired - Lifetime
- 1996-04-17 AT AT98107203T patent/ATE344303T1/de not_active IP Right Cessation
- 1996-04-17 DK DK96400814T patent/DK0739961T3/da active
- 1996-04-17 ES ES96400814T patent/ES2126985T3/es not_active Expired - Lifetime
- 1996-04-17 EP EP98107203A patent/EP0860454B1/fr not_active Expired - Lifetime
- 1996-04-17 AT AT96400814T patent/ATE173003T1/de not_active IP Right Cessation
- 1996-04-17 EP EP96400814A patent/EP0739961B1/fr not_active Revoked
- 1996-04-24 ZA ZA9603265A patent/ZA963265B/xx unknown
- 1996-04-26 CA CA002175149A patent/CA2175149C/fr not_active Expired - Fee Related
- 1996-04-26 MX MX9601567A patent/MX9601567A/es unknown
- 1996-04-26 BR BR9602082A patent/BR9602082A/pt not_active IP Right Cessation
- 1996-04-26 HU HU9601112A patent/HU215178B/hu not_active IP Right Cessation
- 1996-04-26 CN CN96105653A patent/CN1076039C/zh not_active Expired - Fee Related
- 1996-04-27 KR KR1019960013304A patent/KR100481264B1/ko not_active IP Right Cessation
- 1996-04-30 JP JP8109848A patent/JP2788630B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ATE173003T1 (de) | 1998-11-15 |
| HU215178B (hu) | 1998-10-28 |
| HUP9601112A2 (en) | 1997-05-28 |
| FR2733506A1 (fr) | 1996-10-31 |
| EP0739961A1 (fr) | 1996-10-30 |
| EP0860454A2 (fr) | 1998-08-26 |
| DK0739961T3 (da) | 1999-07-19 |
| BR9602082A (pt) | 1998-04-07 |
| DE69600900T2 (de) | 1999-04-15 |
| CA2175149C (fr) | 2001-06-12 |
| CN1147002A (zh) | 1997-04-09 |
| CN1076039C (zh) | 2001-12-12 |
| DE69636676D1 (de) | 2006-12-14 |
| EP0739961B1 (fr) | 1998-11-04 |
| ATE344303T1 (de) | 2006-11-15 |
| MX9601567A (es) | 1997-06-28 |
| HU9601112D0 (en) | 1996-06-28 |
| DE69600900D1 (de) | 1998-12-10 |
| DE69636676T2 (de) | 2007-09-06 |
| EP0860454A3 (fr) | 1998-09-23 |
| ES2270481T3 (es) | 2007-04-01 |
| JPH08302210A (ja) | 1996-11-19 |
| ZA963265B (en) | 1997-10-24 |
| HUP9601112A3 (en) | 1997-10-28 |
| KR100481264B1 (ko) | 2005-11-14 |
| FR2733506B1 (fr) | 1997-06-06 |
| ES2126985T3 (es) | 1999-04-01 |
| EP0860454B1 (fr) | 2006-11-02 |
| JP2788630B2 (ja) | 1998-08-20 |
| CA2175149A1 (fr) | 1996-10-29 |
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