KR940009799B1 - 저압 다이 캐스팅용 분말상 주형 탈형제 - Google Patents

저압 다이 캐스팅용 분말상 주형 탈형제 Download PDF

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KR940009799B1
KR940009799B1 KR1019910008264A KR910008264A KR940009799B1 KR 940009799 B1 KR940009799 B1 KR 940009799B1 KR 1019910008264 A KR1019910008264 A KR 1019910008264A KR 910008264 A KR910008264 A KR 910008264A KR 940009799 B1 KR940009799 B1 KR 940009799B1
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South Korea
Prior art keywords
low pressure
die casting
pressure die
mold release
compound
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KR1019910008264A
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English (en)
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다까시 하나노
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하나노 쇼오지 가부시기가이샤
하나노 히로시
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    • C10M111/04—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential at least one of them being a macromolecular organic compound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22C—FOUNDRY MOULDING
    • B22C3/00—Selection of compositions for coating the surfaces of moulds, cores, or patterns
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    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/05—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon
    • C10M2229/054—Siloxanes with specific structure containing atoms other than silicon, hydrogen, oxygen or carbon containing phosphorus
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    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
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Abstract

내용 없음.

Description

저압 다이 캐스팅용 분말상 주형 탈형제
본 발명은 저압 다이 캐스팅(die casting) 작업시 주형(molding die)의 내면에다 분무하여 사용하는 주형 탈형제(mold releasing agent)에 관한 것이다.
저압 다이 캐스팅법은 고정밀도의 주조 부품을 이 방법에 의하여 연속적으로 다량 제조할 수 있기 때문에 자동차 및 전기 설비용 각종 부품제조시에 널리 활용되고 있다. 또한 이러한 저압 다이 캐스팅법에 있어서 주형 탈형제를 사용하여 주형이 용융금속과 직접 접촉하지 못하게 함으로써 소부현상(seizure)을 방지함과 이울러 제품을 주형으로 부터 보다 쉽게 탈형할 수 있도록 한다.
저압 다이 캐스팅용 주형 탈형제는 수용성(水溶性) 주형 탈형제와 수불용성(水不溶性) 주형 탈형제의 두 가지로 주로 구분되고 있는 것이 일반적이다. 이들 탈형제 중에서 수불용성 주형 탈형제는 매연과 인화성으로 인한 위험이 크기 때문에 안전성의 관점에서 여러 가지 문제점을 내포하고 있으므로 수용성 주형 탈형제가 빈번히 사용되고 있다.
수용성 주형 탈형제는 일반적으로 물, 광유 등과 같은 주형 탈형 기재에 계면활성제 또는 극압(extreme pressure) 부여제의 용도로 실리콘 오일, 합성 또는 천연 왁스, 유지, 지방산 에스테르 등을 첨가해서 된 것이다.
부수적으로 근년에 와서 저압 다이 캐스팅 기술의 발전과 더불어 작업성이 보다 양호하고 고품질의 제품을 제조할 수 있는 주형 탈형제에 대한 수요가 점차 커지고 있다. 그러나 수용성 주형 탈형제를 사용하여 이러한 요구를 충족시킨다는 것은 불가능해지고 있다. 즉 수용성 주형 탈형제는 그 수용성으로 인해 주형의 온도 조절이 어렵고 잔존 수분으로 인해 제품내부에 결함이 발생할 가능성이 크다는 등 여러 가지 문제점을 내포하고 있다. 더욱이 수질오염을 방지하기 위해 폐수 처리를 해야 하므로 공장 시설 투자에 필요한 각종 경비의 증가 요인이 되고 있다는 문제점도 가지고 있다. 따라서 새로운 유형의 주형 탈형제에 대한 요청이 강하게 대두되고 있다.
본 발명은 위에 나온 상황을 고려하여 구체적인 연구와 체계적인 실험에 입각하여 완성된 것이다.
본 발명의 목적은 작업성이 보다 양호하고 주변 환경을 악화시킴이 없이 고품질의 주조제품을 제조할 수 있는 저압 다이 캐스팅용 주형 탈형제를 제공함에 있다. 즉 더 구체적으로는 제품의 소부현상과 내부결함 발생을 확실하게 방지하여 제품을 주형으로 부터 탈형할 수 있는 능력을 향상시키고 사용 후에 주형 내부와 제품 표면으로 부터 쉽사리 제거되며 주조 도중 가스 발생과 주조 후의 수질오염을 전혀 일으키지 않는 주형 탈형제를 제공함에 있다.
본 발명은 저압 다이 캐스팅 작업시에 주형의 내면에다 분무하여 사용하는 저압 다이 캐스팅용 주형 탈형제에 있어서 고체형태로 윤활제로 사용되는 분말상 또는 과립상 무기화합물과 주형 탈형 기재(基材)에 접착성을 부여하는 분말상 또는 과립상 유기화합물로 구성되며 유기화합물이 코우팅된 분말상 또는 과립상 주형 탈형 기재로 된 혼합물을 함유하는 저압 다이 캐스팅용 분말상 주형 탈형제에 관한 것이다.
본 발명의 가장 현저한 특징은 주형 탈형 기재가 분말상 또는 과립상이라는 것이다.
무기화합물에 대하여 유기화합물의 함량을 0.1∼45wt.% 범위에서 선택하는 것이 효과적인데, 그 이유는 무기화합물의 금속 주형 내부에 대한 접착효과는 그 함량이 0.1wt.% 이하인 경우에는 충분히 나타나지 않고, 또한 그 함량이 45wt.% 이상인 경우에는 축적이 되어 금속 주형 내부로 부터 주형 탈형제를 제거할 때 곤란을 겪게 되는데, 즉 주형 탈형 효율이 감소하거나 제품의 칫수 정확도가 나빠지기 때문인 것이다.
본 발명에 사용되는 주형 탈형 기재에는 아무런 제한이 없으나 단, 이들은 윤활제용으로 사용되는 고체 무기화합물로 된 것이면 좋은데, 일반적으로 질화 붕소, 운모, 금속 산화물, 질화 규소, 황 화합물, 플루오르화합물, 활석, 붕소 화합물 및 인 화합물을 사용하는 것이 바람직하다.
그러나 종래부터 주형 탈형제로 사용되어온 이황화 몰리브덴, 흑연 등과 같은 기타 공지의 고체 윤활제도 사용할 수 있다. 이들 무기화합물은 분말상 또는 과립상의 것인데 이들 중 한 가지만을 사용하거나 두 가지 이상을 조합하여 사용한다.
더욱이 본 발명에 사용되는 유기화합물에는 아무런 특별한 제한이 없으나 단, 위에 나온 무기화합물에 대하여 접착성과 결합성을 부여하는 특성을 가진 것이 좋으며, 일반적으로 금속비누 또는 고분자 화합물을 사용하는 것이 바람직하다.
금속비누용으로는 나트륨, 칼슘, 바륨, 리튬, 칼륨, 마그네슘 또는 아연과 결합한 카르복실산 구조의 것을 사용하고, 고분자 화합물 용으로는 폴리에틸렌, 폴리프로필렌, 에폭시 수지, 규소 수지, 페놀 수지, 아크릴레이트 수지, 알키드 수지 또는 폴리스티렌을 사용하는 것이 바람직하다.
이들 유기화합물을 분말상 또는 과립상 주형 탈형 기재와 혼합하거나 가열용융된 상태로 하여 혼합한다.
따라서 본 발명의 주형 탈형제에 있어서 주형 탈형 기재와 유기화합물을 모두 분말 또는 과립형태로 하던지 분말상 또는 과립상 주형 탈형 기재를 유기화합물로 코우팅한다. 부수적으로 위에 나온 유기화합물 중 한 가지만을 사용하거나 두 가지 이상을 조합해서 사용한다. 금속비누와 고분자 화합물을 조합해서 사용해도 좋다.
본 발명에 의한 저압 다이 캐스팅용 분말상 주형 탈형제에 있어서 주형 탈형 기재는 최소한 분말상 또는 과립상이기 때문에 주형 탈형제가 부착하는 금속 주형 내면의 일부에 있는 주형 탈형 기재의 분말 또는 과립의 입자직경 만큼 적어도 금속 주형 내면과 제품이 확실히 간격을 두고 떨어져 있게 된다. 따라서 주형 탈형제는 금속 주형 내면 전체에 균일하게 부착하기 때문에 제품과 금속 주형 내면과 직접 접촉하여 생기는 소부현상을 확실히 피할 수 있다. 더욱이 본 발명에 의한 주형 탈형제는 유기화합물과 무기화합물로 되어 있고 수분을 함유하지 않기 때문에 제품내면에는 잔존 수분으로 인한 결함이 전혀 생기지 않는다. 따라서 제품품질을 향상시킬 수 있다.
또한 본 발명에 의한 주형 탈형제에 있어서 주형 탈형 기재는 최소한 분말 또는 과립형태이고 수분을 함유하지 않기 때문에 금속 주형 내면과 제품 사이에 작용하는 장력은 약하다. 따라서 금속 주형으로 부터 제품을 탈형하기가 쉬워지고, 더욱이 주형 탈형제를 금속 주형 내면과 제품 표면으로 부터 쉽사리 제거할 수 있다.
또한 본 발명의 주형 탈형제에 있어서 주형 탈형 기재는 최소한 분말 또는 과립형태이므로 기재가 저압 다이 캐스팅 도중 열을 받는다 하더라도 반응하기가 어렵고 가스를 거의 발생하지 않는다.
그리고 본 발명의 탈형제는 주조후에 수용성 주형 탈형제의 경우에는 나타나는 것과 같은 수질오염을 일으키지 않는다.
따라서 환경오염을 피할 수 있고 폐수 처리 경비가 필요없기 때문에 유지비를 절감할 수 있다.
본 발명에 있어서 무기화합물과 유기화합물로 구성된 주형 탈형 기재의 혼합물을 함유하는 저압 다이 캐스팅 주형 탈형제는 최소한 기재가 분말상 또는 과립상인 것을 사용하여 탈형제로 제조한 것이다.
따라서 저압 다이 캐스팅법으로 제조된 알루미늄 합금과 아연 합금 등의 주물에 있어서 소부현상과 내부결함을 확실히 제거할 수 있고, 주물의 품질을 향상시킬 수 있으며, 다이 캐스팅법에 의한 주조작업시 그 작업성이 양호하고, 본 발명의 탈형제를 사용하기 전후에 있어서의 환경오염을 완전히 피할 수 있다.
특히 무기화합물에 대한 유기화합물의 함량범위를 0.1∼45wt.%로 함으로써 제조된 주물의 품질을 향상시킬 수 있다. 더욱이 무기화합물로서는 질화 붕소, 운모, 금속 산화물, 질화 규소, 황 화합물, 플루오르화합물, 활석, 붕소 화합물 또는 인 화합물을 사용하고, 유기화합물로서는 나트륨, 칼슘, 바륨, 리튬, 칼륨, 마그네슘 또는 아연이 결합된 카르복실산 화합물로 된 금속비누 또는 폴리에틸렌, 폴리프로필렌, 에폭시 수지, 규소 수지, 페놀 수지, 아크릴레이트 수지, 알키드 수지 또는 폴리스티렌 등과 같은 고분자 화합물을 사용하면 위에 나온 효과를 훨씬 더 많이 향상시킬 수 있다. 각기 해당되는 다이 캐스팅 작업에 가장 적절히 사용할 수 있는 주형 탈형제는 위에 나온 무기화합물과 유기화합물을 각각 두 가지 이상을 조합하여 사용해서 제조할 수 있다.
본 발명을 실시예로 설명하는데 본 발명은 이들 실시예에 한정되는 것은 아니다.
[실시예]
다음에 나오는 주형 탈형제 (A)∼(F)를 제조한 후 저압 다이 캐스팅법에 따라 이들 주형 탈형제를 사용하여 주조시험을 하여 표에 나와 있는 각 시험항목을 비교검토하였다.
두 가지 혼합물, 즉 유기화합물과 무기화합물을 분말 또는 과립형태로 하여 혼합한 혼합물과 유기화합물과 무기화합물을 가열용융된 상태로 하여 혼합한 혼합물을 제조하여 본 발명의 실시예(A)∼(C)로 하였다.
이들 두 가지 혼합물을 검토하여 얻은 결과는 두 가지 혼합물에 있어서 동일하였다. 부수적으로 주형 탈형제 (A)∼(E)에 사용된 화합물은 시판품이다.
(A) 실시예 1 : 질화 붕소(평균 입자크기 : 1∼5마이크론) 95부와 스테아르산 칼슘 5부로 된 혼합물
(B) 실시예 2 : 질화 붕소 20부, 운모 75부 및 폴리에틸렌 5부로 된 혼합물
(C) 실시예 3 : 질화 붕소 50부, 질화 규소 45부, 스테아르산 바륨 3부 및 폴리프로필렌 2부로 된 혼합물
(D) 질화 붕소 단독(비교 실시예 1)
(E) 주성분으로서 왁스와 실리콘 오일을 1 : 80의 비율로 함유한 수용성 주형 탈형제(비교 실시예 2).
[표 1]
X : 완전히 없음, - : 측정 불가
* : 작음, ○ : 중간, ◎ : 큼

Claims (6)

  1. 저압 다이 캐스팅 작업시에 주형의 내면에다 분무하여 사용하는 저압 다이 캐스팅용 주형 탈형제에 있어서 고체형태로 윤활제로 사용되는 분말상 또는 과립상 무기화합물과 주형 탈형 기재(基材)에 접착성을 부여하는 분말상 또는 과립상 유기화합물로 구성되며 유기화합물로 코우팅된 분말상 또는 과립상 탈형 탈형 기재로 된 혼합물을 함유하는 저압 다이 캐스팅용 분말상 주형 탈형제.
  2. 제 1 항에 있어서, 무기화합물에 대하여 유기화합물을 0.1∼45wt.%의 함량으로 함유하는 저압 다이 캐스팅용 분말상 주형 탈형제.
  3. 제 1 항에 있어서, 무기화합물로는 질화 붕소, 질화 규소, 운모, 금속 산화물, 황 화합물, 플루오르화물, 활석, 붕소 화합물 및 인 화합물 중 한 가지 이상을 함유하는 저압 다이 캐스팅용 분말상 주형 탈형제.
  4. 제 1 항에 있어서, 유기화합물로는 금속비누 및/또는 고분자 화합물 중 한 가지 이상을 함유하는 저압 다이 캐스팅용 분말상 주형 탈형제.
  5. 제 4 항에 있어서, 금속비누가 나트륨, 칼슘, 바륨, 리튬, 칼륨, 마그네슘 또는 아연과 결합한 카르복실산 그룹을 함유하는 것인 저압 다이 캐스팅용 분말상 주형 탈형제.
  6. 제 4 항에 있어서, 고분자 화합물이 폴리에틸렌, 폴리프로필렌, 에폭시 수지, 규소 수지, 페놀 수지, 아크릴레이트 수지, 알키드 수지 또는 폴리스티렌인 저압 다이 캐스팅용 분말상 주형 탈형제.
KR1019910008264A 1991-03-06 1991-05-22 저압 다이 캐스팅용 분말상 주형 탈형제 KR940009799B1 (ko)

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Application Number Priority Date Filing Date Title
JP02-67976 1991-03-06
JP3067976A JPH0759346B2 (ja) 1991-03-06 1991-03-06 低圧鋳造用粉末離型剤

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KR940009799B1 true KR940009799B1 (ko) 1994-10-17

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JP (1) JPH0759346B2 (ko)
KR (1) KR940009799B1 (ko)
CA (1) CA2041503A1 (ko)
DE (1) DE4116260A1 (ko)
GB (1) GB2253408A (ko)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000033457A (ja) 1998-07-21 2000-02-02 Denso Corp 潤滑離型剤
CN101898227A (zh) * 2010-07-28 2010-12-01 启东尤希路化学工业有限公司 环境友好型镁合金脱模剂
CN114540101B (zh) * 2022-01-24 2023-03-14 华中光电技术研究所（中国船舶重工集团公司第七一七研究所） 高精度树脂砂轮加工用脱模剂及其使用方法

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Publication number Priority date Publication date Assignee Title
GB120255A (en) * 1917-10-31 1918-10-31 Thomas William Staine Hutchins Improvements relating to the Manufacture of Carbon Blocks.
GB318740A (en) * 1928-08-27 1929-09-12 Lajos Dorogi Improvements in or relating to templates for the manufacture of articles from sheet rubber
GB334857A (en) * 1929-06-05 1930-09-05 Kelly Graphite Mills Inc Improvements in or relating to parting compounds for foundry moulds
GB676408A (en) * 1950-11-20 1952-07-23 Buttress & Mcclellan Inc Method of constructing concrete building elements
US2937406A (en) * 1959-03-20 1960-05-24 Goodyear Tire & Rubber Fluid pressure core
GB1193645A (en) * 1966-08-05 1970-06-03 Francis Guy Sydenham English Improvements in or relating to Wet-Table Coatings.
US3615071A (en) * 1969-04-16 1971-10-26 Dow Corning Flexible mold
GB1362881A (en) * 1971-06-22 1974-08-07 Scott Bader Co Gel coats for moulds
DE2328337C3 (de) * 1973-06-04 1978-01-19 Wacker Chemie Gmbh Verfahren zum herstellen von formkoerpern und ueberzuegen aus baustoffen auf grundlage von anorganischen bindemitteln
GB2003923B (en) * 1977-09-07 1982-03-10 Foseco Int Metal working lubricants
JPH069730B2 (ja) * 1989-01-13 1994-02-09 花野商事株式会社 ダイカスト用粉末離型剤

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Publication number Publication date
CA2041503A1 (en) 1992-09-07
DE4116260A1 (de) 1992-09-10
GB2253408A (en) 1992-09-09
GB9111497D0 (en) 1991-07-17
JPH0759346B2 (ja) 1995-06-28
JPH04279244A (ja) 1992-10-05

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