KR930011076B1 - 점착성 그리이스 조성물 - Google Patents

점착성 그리이스 조성물 Download PDF

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KR930011076B1
KR930011076B1 KR1019880002702A KR880002702A KR930011076B1 KR 930011076 B1 KR930011076 B1 KR 930011076B1 KR 1019880002702 A KR1019880002702 A KR 1019880002702A KR 880002702 A KR880002702 A KR 880002702A KR 930011076 B1 KR930011076 B1 KR 930011076B1
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South Korea
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grease
component
oil
adhesive
grease composition
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KR1019880002702A
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KR880011314A (ko
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시게루 모리
다까유끼 다까하시
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신에쓰 가가꾸 고오교 가부시끼가이샤
고사까 유따로
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Publication of KR880011314A publication Critical patent/KR880011314A/ko
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Abstract

내용 없음.

Description

점착성 그리이스 조성물
제1도는 본 발명 그리이스의 온도에 대한 토오크 값(g/cm)을 폴리부텐계 그리이스 및 실리콘계 그리이스의 토오크 값과 비교한, 온도 특성을 나타내는 그래프.
본 발명은 점착성 그리이스 조성물에 관한 것이다.
점착성 그리이스는 점착력을 갖는 윤활제로서 자동차, 항공기, 가열로 콘베이어, 송풍기, 가전 제품, 사무용 기기, 정밀기기, 계측기기 등의 윤활 부분에 널리 사용되고 있으며, 저온 내지는 고온의 격심한 조건하에서도 안정된 윤활성을 유지하여야 함이 요구된다.
종래의, 점착성 그리이스로서는 다음과 같은 것이 알려져 있다.
우선, 윤활성이 양호한 폴리부텐계 점착성 그리이스가 있다. 이러한 폴리부텐계 점착성 그리이스에는 통상의 그리이스에 폴리부텐을 첨가하여 점착력을 부여한 것, 또는 폴리부텐을 베이스로 하고 증조제를 첨가하여 그리이스 상으로 한 것이 있지만, 윤활성이 좋은 반면 온도 토오크 값 특성(이하, 온도 특성이라 약칭함)이 나쁘다는 결점이 있다.
또한, 온도 특성이 우수한 실리콘계의 점착성 그리이스(일본국 특허 공고(소)제53-776호 및 동 제60-45,240호 참조)가 있지만, 이 실리콘계 점착성 그리이스는 윤활성이 매우 나쁘다는 결점이 있다.
또한, 폴리부텐의 특성과 실리콘의 특성을 점착성 그리이스(일본국 특허 공고(소)제56-16,195호 참조)도 있지만, 이 점착성 그리이스는 폴리부텐계 점착성 그리이스에 비해 윤활성이 떨어진다는 결점이 있다.
본 발명은 상기한 종래 기술의 결점을 해결하고자 하는 것이다. 즉, 윤활성 면에서 우수한 폴리부텐계류의 윤활성을 가지면서 동시에 특성이 폴리부텐계 보다도 우수한 고성능의 점착성 그리이스를 제공하고자 하는 것이다.
본 발명의 점착성 그리이스 조성물은 제1성분으로서 하기식
Figure kpo00001
(식 중,R은 알킬이고,x,y 및 p는 x/y=0.5-2.0,(x+y)p=50-150을 만족시키는 양의 정수임)으로 나타내어지는 에틸렌과 α-올레핀과의 랜덤 공중합체(코올리고머) 100중량부와, 제2성분으로서 증조제 5 내지 100중량부를 함유하는 것을 특징으로 하는 그리이스 조성물이다. 본 발명에 있어서, 제1성분인 베이스 오일로서의 코올리고머는, 예를 들어 루칸트 (HC-20,HC-50,HC-100,HC-150,HC-600,HC-2000등)[미쓰이 세끼유 가가꾸 고오교(주) 제품]이 사용되고 있으며, 루칸트 HC-600 또는 루칸트 HC-2000이 적합하다.
제2성분인 증조제로서는 그리이스의 증조제로서 일반적으로 사용되는 증조제이면 좋고, 예를 들어 알루미늄, 납, 망간, 리튬, 플루토늄, 칼슘, 바륨, 스트론튬, 구리, 수은, 비스무트, 크롬, 철, 니켈 등의 금속 비누류, 실리카, 알루미나, 산화철, 산화납, 점토, 그라파이트, 카본 등의 무기질 물질, 또는 아릴우레아, 프탈로시아닌, 인단트렌, 폴리사불화에틸렌 등을 사용할 수 있다. 상기한 것 중에서 금속 비누로서는 리듐스테아레이트, 리튬히드록시 스테아레이트가 적합하고, 무기질 물질로서는 실리카가 본 발명용의 증조제로서 적합하다. 또한, 실리카는 그 표면이 알콕시실란, 클로로실란, 말단에 히드록시를 함유하는 오르가노폴리실록산, 유기아민화합물 또는 유기 붕소 화합물 등으로 처리된 것이어도 좋다. 또한 임의 성분으로서 제1성분 100중량부에 대하여 100중량부를 초과하지 않는 양의 오일을 첨가하여도 좋고, 이 임의 성분의 첨가 오일로서는, 예를 들면 실리콘 오일, α-올레핀 올리고머 또는 디에스테르유 등이 사용된다. 이 중에서 실리콘 오일로서는 디메틸실리콘 오일, 메틸페닐실리콘 오일, α-올레핀 변성 실리콘 오일, 플루오로실리콘 오일 등이 있고, 각각 KF96, KF50과 KF54, KF412와 KF7235B, KL-100등[신에쓰 가가꾸고오교(주) 제품]을 들 수 있다. 이 임의 성분과 제1 및 제2성분과의 상용성 (相溶性)으로 보아, 실리콘 오일중에서도 α-올레핀 변성 실리콘 오일이 적합하다. 또한, α-올레핀 올리고머로서는 PAOL[라이온(주) 제품]등의 올리고머를 들 수 있고, 디에스테르 오일로서는 디옥틸세바케이트(DOS), 디옥틸아젤레이트(DOZ), 디옥틸아디페이트(DOA) 등의 오일을 들 수 있다.
상기 임의 성분으로서의 실리콘 오일 α-올레핀 올리고머 및 디에스테르유는 본 발명의 점착성 그리이스 조성물의 점착력의 강도를 조절하기 위해서 적절하게 첨가되는 것으로서, 상기한 정도의 양을 제1 및 제2성분에 대하여 첨가하면 좋다. 또한, 필요에 따라서 산화 방지제 등의 첨가제를 첨가해도 좋다.
본 발명의 그리이스 조성물은 성분 원료를 단순히 혼합하거나, 열처리 혼합 또는 감압 열처리 혼합 등을 행함으로써 충분히 혼합한 후, 3개의 로울, 콜로이드 밀 등으로 더욱 잘 혼련하여 그리이스화함으로써 제조된다.
본 발명의 점착성 그리이스 조성물에 있어서의 제1성분인 코올리고머는, 광유에 비해 다음과 같은 점에서 우수하다. 즉, 이 코올리고머는 온도 특성 및 열산화 안정성이 우수한 무색 투명한 액체이고, 유동점이 낮으며, 인화점(250 내지 300℃) 및 발화점(395 내지 415℃)이 높고, 화학적으로 안정하고, 금속 부식성이 거의 없다.
또한, 제2성분인 증조제는, 제1성분의 코올리고머 중에 들어가 그물눈 구조를 형성하고, 외부로 여분의 오일 또는 그리이스가 유출하는 것을 방지한다. 제1성분 100중량부에 대하여 이 제2성분의 양이 5중량부보다도 적을 경우에는 상기 그물눈 구조가 충분히 형성되지 않고, 조도(稠度)가 너무 커져 점착성이 충분하지 않은 그리이스가 되어버린다. 또한, 제2성분의 양이 제1성분 100중량부에 대하여 100중량부보다 커지면, 조도가 극도로 작아지고, 너무 굳어져서 그리이스로서 사용할 수 없게 되어버린다.
이하, 실시예에 의하여 본 발명을 설명한다.
[실시예]
[실시예 1-10]
루트칸 HC-600 또는 HC-2000을 베이스 오일로 하고, 이 베이스 오일 성분, 여러 가지 증조제 및 첨가 오일 성분으로 되는 경우의 본 발명의 그리이스 조성물(실시예 1-10) 및 그 특성을 표 1에 나타내었다. 각 그리이스 조성물은 성분 원료를 플래니터리(planetary) 믹서로 예비 혼합하고, 이어서 3개의 로울에 의하여 혼련하여 제조하였다. 증조제가 표면 처리 실리카(이하, 단지 처리 실리카라고 약기함)인 경우(실시예 1-3,7,9 및 10)에는 이 처리 실리카가 베이스 오일에 잘 풀려서 서로 충분히 혼합되도록 3개의 로울에 의한 혼련을 수 회 수행하였다. 혼련 후, 얻어진 본 발명의 그리이스 조성물을 베어링에 도포하고, 각종 측정 시험을 행하였다(표 1참조).
[표 1]
Figure kpo00002
[비교예 11 및 12]
실리콘계 또는 폴리부텐계의 그리이스에 대해 실시예 1-10과 같은 방법으로 시험을 행한 결과를 표 2에 나타냈다.
[표 2]
Figure kpo00003
Figure kpo00004
이하, 각종 시험의 실시 방법에 대해서 설명한다.
[조도의 측정]
JIS K 2220의 측정법에 준해서 조도를 측정하였다.
[토오크의 값의 측정]
4ø×8mm의 축(알루미늄제)과 그 베어링(아연제)에 그리이스를 도포하여 최초의 토오크 값을 초기 토오크 값으로 하고, 360도 회전 1왕복/초를 1사이클로 하여 50 사이클 후, 150 사이클 후 및 300 사이클 후의 토오크 값을 각각 측정하였다.
단, 토오크 값 측정시의 축 회전수는 10r. p. m이다.
[회전 수명 시험]
4ø×8mm의 축(알루미늄제)과 그 베어링(아연제)에 그리이스를 도포하고, 360도 회전 1왕복/초를 1사이클로 하고, 1000사이클/시간의 스피드로 눌어 붙을 때까지의 사이클 수에 대하여 측정하였다.
[온도 특성 시험]
4ø×8mm의 축(알루미늄제)과 그 베어링(아연제)에 그리이스를 도포하고 , 주변 온도를 변화시켜 토오크 값을 측정하였다(토오크 값 측정시의 축 회전수는 10r.p.m.임). 제1도에 그 결과를 나타내었다.
이상 실시예 및 비교예로부터 명백한 바와 같이, 본 발명의 점착성 그리이스 조성물은 폴리부텐계 그리이스와 동등한 윤활성을 가지면서 온도 특성이 폴리부텐계 그리이스 보다 더 우수하므로 본 발명의 점착성 그리이스 조성물에 의하여 고성능의 점착성 그리이스를 제공하는 것이 가능하게 되었다.

Claims (1)

  1. 하기 식으로 나타내어지는 중합체 100중량부와, 증조제 5 내지 100중량부로 되는 것을 특징으로 하는 점착성 그리이스 조성물.
    Figure kpo00005
    식중, R은 알킬기이고, x, y 및 p는 x/y=0.5-2.0, (x+y)p=50-150을 만족시키는 양의 정수이다.
KR1019880002702A 1987-03-17 1988-03-15 점착성 그리이스 조성물 KR930011076B1 (ko)

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GB1524116A (en) * 1974-12-19 1978-09-06 World Inventions Ltd Container for foodstuffs or the like
JPS5616195A (en) * 1979-07-17 1981-02-16 Brother Ind Ltd Wind regulating device and volume switching device for lead organ
US4294713A (en) * 1980-03-31 1981-10-13 Olin Corporation Grease compositions containing selected shielded polysilicate compounds
JPS57123205A (en) * 1981-01-13 1982-07-31 Mitsui Petrochem Ind Ltd Production of low-molecular weight copolymer
JPS59223797A (ja) * 1983-06-03 1984-12-15 Matsushita Electric Ind Co Ltd 摩擦材潤滑膜安定化組成物
JPS6045240A (ja) * 1983-08-23 1985-03-11 Fujitsu Ltd アルカリ現像ネガ型レジスト組成物
JPS6044593A (ja) * 1983-08-23 1985-03-09 Idemitsu Kosan Co Ltd 汎用グリ−ス組成物

Also Published As

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US4840739A (en) 1989-06-20
JPS63227697A (ja) 1988-09-21
JPH0534394B2 (ko) 1993-05-21
KR880011314A (ko) 1988-10-27

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