JPH08143883A - 耐熱性グリース組成物 - Google Patents

耐熱性グリース組成物

Info

Publication number
JPH08143883A
JPH08143883A JP6308121A JP30812194A JPH08143883A JP H08143883 A JPH08143883 A JP H08143883A JP 6308121 A JP6308121 A JP 6308121A JP 30812194 A JP30812194 A JP 30812194A JP H08143883 A JPH08143883 A JP H08143883A
Authority
JP
Japan
Prior art keywords
grease
heat
grease composition
formula
compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP6308121A
Other languages
English (en)
Inventor
Shishiyou Chin
志昌 沈
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DuPont Toray Specialty Materials KK
Original Assignee
Dow Corning Asia Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Asia Ltd filed Critical Dow Corning Asia Ltd
Priority to JP6308121A priority Critical patent/JPH08143883A/ja
Priority to EP95308254A priority patent/EP0717099A1/en
Publication of JPH08143883A publication Critical patent/JPH08143883A/ja
Priority to US08/837,663 priority patent/US5908815A/en
Pending legal-status Critical Current

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    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • C08L83/08—Polysiloxanes containing silicon bound to organic groups containing atoms other than carbon, hydrogen and oxygen
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    • C10M107/50—Lubricating compositions characterised by the base-material being a macromolecular compound containing silicon
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Abstract

(57)【要約】 （修正有） 【目的】 フッ素系グリースの高温条件での劣化現象を
防止して、１．耐熱性に優れること、２．耐熱性が長期
的に安定であること、の特性を有するグリース組成物の
提供。 【構成】 フルオロシリコーンオイル（イ）、フッ素樹
脂系増ちょう剤（ロ）と 変性ウンデカン混合物 変性ブタン Ｃｕフタロシアニン Ｃａスルフォネート等で表される添加剤（ハ）の少なく
とも１種以上を含有することを特徴とする耐熱性グリー
ス組成物。

Description

【発明の詳細な説明】
【０００１】
【技術分野】本発明は、フルオロシリコーンオイルを基
油とし、フッ素系樹脂を増ちょう剤とする耐熱性フッ素
系グリース組成物に関する。
【０００２】
【従来技術】フルオロシリコーンオイルを基油とし、フ
ッ素系樹脂を増ちょう剤とするグリースは、耐熱性が良
いグリースとして公知である。例えば、ＵＳ３，３１
４，８８９やＵＳ３，６４２，６２６などに開示されて
おり、前記米国特許明細書には、広い温度範囲で使用可
能で、高荷重下にて使用できるグリース組成物を開示し
ており、特に基油としてフロロシリコーンオイルが使用
されている。さらに、特開昭６１−１１３６９４号に
は、耐熱性に優れたグリースの処方として、フロロポリ
エーテルを基油とし、フッ素樹脂を含む組成物が開示さ
れている。しかし、このようなフッ素系グリースであっ
ても、著しい高温条件下では時間の経過とともに、性状
が不安定になるという問題があった。
【０００３】
【目的】本発明は、フッ素系グリースの高温条件での劣
化現象を防止して、以下の特性を有するグリース組成物
の提供を目的とする。 １．耐熱性に優れること ２．耐熱性が長期的に安定であること 具体的には、前記フッ素系グリースからの基油の蒸発抑
止および／またはグリースのゲル化ないしは硬化を防止
することを目的とする。従って、本発明における耐熱性
とは、グリースからの蒸発と、ゲル化の傾向をもって指
標とした。
【０００４】
【構成】本発明はフロロシリコーンオイル基油（イ）
と、フッ素樹脂系増ちょう剤（ロ）を含有するグリース
組成物において、従来から見られた高温条件下における
経時でのゲル化や経時での蒸発量の増大といった問題を
解決したものであり、特に自動車用ファンクラッチベア
リングに適用して優れた耐熱性を示すグリース組成物に
関する。本発明はフルオロシリコーンオイルを基油と
し、フッ素系樹脂を増ちょう剤として含有するフッ素系
グリースにおいて、該グリースに特定の酸化剤を含有さ
せることにより、前記の目的を達成した。
【０００５】すなわち、本発明者らはフロロシリコーン
オイル基油とフッ素樹脂系増ちょう剤を含有するフッ素
系グリースの高温条件下での使用によるゲル化の防止と
基油の蒸発量の低減化に優れた効果のある添加剤として
多くの添加剤の中から前式（ａ）〜（ｇ）で表わされる
添加剤よりなる群から選ばれる少なくとも１種以上を使
用することを見い出したことにもとづき、本発明を完成
した。具体的には、上記（ａ）〜（ｇ）から選ばれる１
種以上を含んだ本発明のグリース組成物は、（ａ）〜
（ｇ）以外の添加剤を配合したグリース組成物に較べて
特にグリースの高温条件下での使用によるゲル化の防止
と基油の蒸発量の低減化にすぐれた耐熱性、優れた効果
を示すという知見に基づき、本発明は完成されたもので
ある。
【０００６】本発明のフッ素系グリースの（イ）成分で
ある基油を構成するフロロシリコーンオイルとは、フッ
素化アルキル基あるいはパーフロロアルキル基を有する
オルガノポリシロキサンであれば、格別限定されるもの
ではない。本発明のフロロシリコーンオイルの粘度とし
ては、グリース化できる範囲であれば、格別限定される
ものではない。通常は１００ｃＳｔ〜１００，０００ｃ
Ｓｔのものが選択されるが、好適には１００ｃＳｔ〜５
０，０００ｃＳｔのものが選択される。また、ファンク
ラッチベアリング用としては、３００ｃＳｔ〜５，００
０ｃＳｔが望ましい。また、本発明のフロロシリコーン
オイルの使用可能な温度範囲は、−５０〜４００℃、好
ましくは−３０〜３００℃の範囲のものである。本発明
に使用されるフロロシリコーンオイルの具体例として、
下式（１）のものを示すが、これらに限定されるもので
はない。さらにこれらフロロシリコーンに、本発明の所
期の目的を防げない限り、他の公知のグリース基油、例
えばパーフルオロポリエーテル、フロロシリコン、メチ
ルフェニルシリコン、ジメチルシリコン等のシリコン、
エステル、ポリエーテル、合成炭化水素油、鉱物油、植
物油を添加、混合してもよい。
【０００７】
【化６】 Ｒ′：炭素原子数１〜３の炭化水素基 Ｒ″：メチル基、エチル基、ビニル基、フェニル基又は
−ＣＨ2ＣＨ2Ｒ基 （Ｒ：炭素原子数１〜１０のパーフルオロアルキル基で
あり、Ｒ″のうち少なくとも５０％は−ＣＨ2ＣＨ2Ｒ基
である。また、ｎは前記の粘度範囲を与える範囲の数で
ある。） 前式（１）で示されるフロロシリコーン化合物のうち、
特に以下のものが望ましい。
【０００８】下式（２）で表わされるトリフロロプロピ
ルメチルポリシロキサン
【化７】 (ｍ：粘度範囲１００ｃＳｔ〜１００，０００ｃＳｔを
与える範囲の数である。)
【０００９】下式（３）で表わされるパーフロロアルキ
ルメチルポリシロキサン
【化８】 （ａおよびｂ：粘度範囲１００ｃＳｔ〜１００，０００
ｃＳｔを与える範囲で、互いに任意に選択される数であ
る。）
【００１０】
【化９】 （ｎ：粘度範囲１００ｃＳｔ〜１００，０００ｃＳｔを
与える範囲の数である。）
【化１０】 （ｍおよびｎ：粘度範囲１００ｃＳｔ〜１００，０００
ｃＳｔを与える範囲で、互いに任意に選択される数であ
る。）
【化１１】 （ｍおよびｎ：前記に同じ。）
【００１１】
【化１２】 （ｎ：前記に同じ。）
【化１３】 （ｎ：前記に同じ。）
【化１４】 （ｍおよびｎ：上記に同じ。）
【００１２】本発明の耐熱性グリース組成物の（ロ）成
分である増ちょう剤としては、フッ素樹脂系のものであ
れば、格別その種類は限定されないが、例えばポリテト
ラフルオロエチレン（ＰＴＦＥ）、三フッ化エチレン樹
脂等が挙げられる。さらに前記フッ素樹脂系増ちょう剤
に、本発明の目的を妨げない限り、他の公知の増ちょう
剤、例えばＬｉ−石鹸、シリカ、Ｃａ−石鹸、Ａｌ−石
鹸、Ｃａ−ｃｏｍｐｌｅｘ、Ａｌ−ｃｏｍｐｌｅｘ、Ｌ
ｉ−ｃｏｍｐｌｅｘ、ウレア、ベントン等を加えてもよ
い。本発明の耐熱性グリース組成物におけるフルオロシ
リコーンオイルとフッ素樹脂系増ちょう剤との配合比率
は、該グリースを適用する用途に応じて適したちょう度
あるいはその使用温度に合った組み合わせとなるもので
あればよく、格別限定されるものではないが、通常は、
ＪＩＳ Ｋ２２２０のちょう度番号１番〜３番の範囲が
選択される。また、ファンクラッチベアリング用には、
ちょう度番号２番の範囲が望ましい。本発明の耐熱性グ
リース組成物の（ハ）成分としては、下式（ａ）、
（ｂ）、（ｃ）、（ｄ）、（ｅ）、（ｆ）および（ｇ）
で表わされる化合物よりなる群から選ばれた少なくとも
１種の化合物、または２種以上の混合物を用いることが
できる。
【００１３】
【化１５】 ３，９−ビス〔１，１−ジメチル−２−｛β−（３−ｔ
−ブチル−４−ハイドロキシ−５−メチルフェニル）プ
ロピオニルオキシ｝エチル〕−２，４，８，１０−テト
ラオキサスピロ〔５，５〕ウンデカン
【００１４】
【化１６】 （Ｒ：炭素原子数１２のアルキル基）
【００１５】
【化１７】 １，１，３−トリス（２−メチル−４−ヒドロキシ−５
−ｔ−ブチルフエニル）ブタン
【００１６】
【化１８】 銅フタロシアニン（Ｃｕ−Ｐｈｔｈａｌｏｃｙａｎｉｎ
ｅ）
【００１７】
【化１９】Ｒ−ＳＯ3Ｃａ （ｅ） （Ｒ：アルキル基） カルシウムスルフォネイト（Ｃａ−Ｓｕｌｆｏｎａｔ
ｅ） アセチルアセトン銅塩 （ｆ） 次のと 両末端が４−（フェニルアミノ）フェノキシ・ジメチ
ルシリル基で封鎖されてなるジメチルポリシロキサン ポリジメチルシロキサンとジルコニウムカルボキシレ
ートの混合物（但し該混合物中のジルコニウム金属の含
有量は、０．１〜１０重量％）を不活性雰囲気下でジル
コニウムカルボキシレートを分解できる温度で加熱して
得られたもの。（ｇ） 前記両者の重量比は、０．５：１〜１：０．５が好まし
い。この重量比の範囲外では充分な耐熱性が得にくい。
また、両者は、混合物の形で使用してもよいし、あるい
は両者の１方を先に使用し、残りの１方を後に使用して
もよい。前記両末端４−（フェニルアミノ）フェノール
封鎖ジメチルポリシロキサンの粘度は、５０〜３００ｃ
Ｓｔが好ましい。前記粘度の範囲外では分散性が充分で
ない。
【００１８】前式（ａ）、（ｂ）、（ｃ）、（ｄ）、
（ｅ）、（ｆ）および（ｇ）で表わされる化合物よりな
る群から選ばれる１種又は２種以上の添加剤の配合量は
フルオロシリコーンオイルとフッ素樹脂系増ちょう剤の
合計量に対して０．５〜１０重量％配合されることが必
要である。０．５重量％未満では、充分な耐熱性効果を
発揮できない。また１０重量％以上ではグリースの性状
自体に影響を与えるものである。本発明の耐熱性グリー
ス組成物は、通常のグリース製造方法で使用される任意
の製造方法を採用することができる。具体的には、たと
えば基油、増ちょう剤および添加剤をニーダー等で充分
に混合した後、ロールを２回通す工程があげられる。本
発明の耐熱性グリース組成物には、上記のフルオロシリ
コーンオイル（イ）、フッ素樹脂系増ちょう剤（ロ）、
前式（ａ）、（ｂ）、（ｃ）、（ｄ）、（ｅ）、（ｆ）
および（ｇ）で表わされる添加剤（ハ）の他に、通常、
グリースに配合される各種添加剤を添加することができ
る。この様な例として、以下のものが挙げられる。 固体潤滑剤（ＭｏＳ2、グラファイトなど） 極圧添加剤（ジチオリン酸亜鉛、ジチオカルバミン酸亜
鉛、フォスフェート、アルキルサルファイドなど） 次に本発明のグリース組成物を実施例として、前記の添
加剤を含有しない耐熱性グリースを比較例として、下記
実験１試験方法および実験２試験方法で評価し、その結
果を、下表１〜１１に示した。本発明のグリース組成物
は、試料（グリース組成物）を２００℃で貯蔵した場
合、貯蔵時間が２６４時間の段階で蒸発損が１６％以
下、グリース性状を維持していることの再条件を満た
しているものである。
【００１９】実験１試験方法 １）グリース（１０ｇ）をシャーレ（直径：５１ｍｍ、
高さ：１６ｍｍ）上に平になるように塗布し秤量する。 ２）オーブンで温度：２００℃でエージングする。 ３）所定時間経過後オーブンからとり出し、放冷後秤量
する。
【００２０】実験２試験方法 １）グリースの初期ちょう度は、不混和状態のもの１０
ｇを１／２ちょう度試験器を用いて測定した。（不混和
ちょう度） 測定方法は「ＪＩＳ Ｋ２２２０−１９８
４参考１１．グリースの１／４及び１／２ちょう度試験
方法」に準じて行った。 ２）グリースのエージングは実験１の方法で行った。 ３）エージング後の測定は、１／４ちょう度試験器を用
いて不混和ちょう度を測定した。以下に前記の実験１試
験方法および実験２試験方法で使用した配合成分につい
て説明する。
【００２１】１．成分１−１（Ｓｉ・ＯＩＬ５００）お
よび１−２（Ｓｉ・ＯＩＬ３００）とも下式（１０）で
表わされる。両末端がトリメチルシリル基で封鎖されて
おり、主鎖はトリフルオロプロピルメチルシロキサンで
構成されてなる基本構造の点では同じであるが、前者の
成分１−１は粘度が５００ｃＳｔであり、後者の成分１
−２は粘度が３００ｃＳｔのものである。
【化２０】 （式中、ｎは成分１−１の場合には、粘度が５００ｃＳ
ｔの範囲のものであり、成分１−２の場合には、粘度が
３００ｃＳｔの範囲のものである。） ２．成分２：ＰＴＦＥ（ポリテトラフルオロエチレン） ３．成分３：変性ウンデカン混合物〔前式（ａ）と
（ｂ）の化合物の１：１混合物〕 ４．成分４：変性ブタン〔前式（ｃ）の化合物〕
【００２２】５．成分５：Ｃｕフタロシアニン〔前式
（ｄ）の化合物〕 ６．成分６：Ｃａスルフォネート〔前式（ｅ）の化合
物〕 ７．成分７：ＭｇＯ ８．成分８：Ｃａステアリン酸〔カルシウムステアリン
酸塩〕 ９．成分９：ＡｃＡｃＣａ〔アセチルアセトンカルシウ
ム塩〕 １０．成分１０：ＣａＳＡＮＳＡ〔セバシン酸モノステ
アリルアミドカルシウム塩〕 １１．成分１１：ＺｎＳＡＮＳＡ〔セバシン酸モノステ
アリルアミド亜鉛塩〕
【００２３】１２．成分１２：次の式で表わされる化合
物（粘度１００ｃＳｔ）
【化２１】 （式中ｘは粘度１００ｃＳｔを与える値） 両末端が４−（フェニルアミノ）フェノールで封鎖され
たジメチルポリシロキサン １３．成分１３：ポリジメチルシロキサンとジルコニウ
ムオクタネイトの混合物（重量比３：１）を窒素雰囲気
下３５０℃で２４時間加熱したもの １４．成分１４：成分１２と成分１３の１：１混合物 １５．成分１５：フェロセンＦｅ〔Ｆｅ（Ｃ5Ｈ5）2〕
（メタロセンＦｅとも言う） １６．成分１６：ＡｃＡｃＣｕ〔アセチルアセトン銅
塩〕 １７．成分１７：Ｃａ（ＯＨ）2 １８．成分１８：ＰＴＦＥパウダー（商品名 セフラル
ルーブ、セントラルガラス社製） １９．成分１９：ＰＴＦＥパウダー（商品名 フルオン
１７１Ｊ、旭硝子社製）
【００２４】実験１（蒸発テスト）のグリースの組成
【表１】
【００２５】実験１（蒸発テスト）の結果 〔蒸発損（％）／貯蔵時間（Ｈｒｓ）〕
【表２】 ＊貯蔵温度：２００℃ 試料：１０ｇ ＊実施例１〜４は、貯蔵時間２６４時間以降においてもグリース性状を維持
【００２６】実験１（蒸発テスト）のグリースの組成
（比較例）
【表３】
【００２７】実験１（蒸発テスト）の結果（比較例） 〔蒸発損（％）／貯蔵時間（Ｈｒｓ）〕
【表４】 貯蔵温度：２００℃ 試料：１０ｇ ＊〜 グリース性状を失ったため測定を終了した。
【００２８】実験１−２（エージングテスト）のグリー
スの組成およびテスト結果（実施例）
【表５】
【００２９】実験１−２（エージングテスト）のグリー
スの組成およびテスト結果（比較例）
【表６】
【００３０】実験２（蒸発テスト）のグリースの組成
（実施例）
【表７】
【００３１】実験２（蒸発テスト）の結果 〔蒸発損（％）／貯蔵時間（Ｈｒｓ）〕
【表８】 ＊貯蔵温度：２００℃ 試料：１０ｇ ＊実施例９〜１４は、貯蔵時間２６４時間以降においてもグリース性状を維持
【００３２】実験２（蒸発テスト）のグリース組成（比
較例）
【表９】
【００３３】実験２（蒸発テスト）の結果（比較例） 〔蒸発損（％）／貯蔵時間（Ｈｒｓ）〕
【表１０】 貯蔵温度：２００℃ 試料：１０ｇ ＊比較例１３、１４、１５、１６、１７については貯蔵時間２６４時間にて グリース性状を喪失した。
【００３４】実験２−２（エージングテスト）のグリー
ス組成（実施例）
【表１１】
【００３５】本発明の具体的実施態様を、以下、記載す
る。 １．フルオロシリコーンオイル（イ）、フッ素樹脂系増
ちょう剤（ロ）と次式（ａ）、（ｂ）、（ｃ）、
（ｄ）、（ｅ）、（ｆ）および（ｇ）で表わされる添加
剤（ハ）の少なくとも１種以上を含有することを特徴と
する耐熱性グリース組成物。 ２．前記１の耐熱性グリース組成物において、フロロシ
リコーンオイルの粘度が、１００〜１００，０００ｃＳ
ｔの範囲のものである耐熱性グリース組成物。 ３．前記１または２の耐熱性グリース組成物において、
フロロシリコーンオイルが、他の公知のグリース基油を
含有するものである耐熱性グリース組成物。 ４．前記１、２または３の耐熱性グリース組成物におい
て、フロロシリコーンオイルが、前式（１）で表わされ
るものである耐熱性グリース組成物。 ５．前記５の耐熱性グリース組成物において、前式
（１）で表わされるフロロシリコーンオイルが、前式
（２）、（３）、（４）、（５）、（６）、（７）、
（８）および（９）よりなる群から選ばれたものである
耐熱性グリース組成物。 ６．前記１、２、３、４または５の耐熱性グリース組成
物において、増ちょう剤がポリテトラフルオロエチレン
および／または三フッ化エチレン樹脂である耐熱性グリ
ース組成物。 ７．前記６の耐熱性グリース組成物において、増ちょう
剤が他の公知の増ちょう剤を含有するものである耐熱性
グリース組成物。 ８．前記１、２、３、４、５、６または７のグリース組
成物において、添加剤（ハ）として、前式（ａ）、
（ｂ）、（ｃ）、（ｄ）、（ｅ）、（ｆ）および（ｇ）
で表わされる化合物よりなる群から選ばれた少なくとも
１種の化合物を含有するものである耐熱性グリース組成
物。 ９．前記１、２、３、４、５、６、７または８の耐熱性
グリース組成物よりなることを特徴とするファンクラッ
チベアリング用耐熱性グリース組成物。
【００３６】
【効果】本発明によると、高温条件下における経時での
ゲル化や経時での基油の蒸発量の増大といった問題を解
決した耐熱性グリース、特に自動車用ファンクラッチベ
アリングに適用して優れた耐熱性を示すグリース組成物
が提供された。
───────────────────────────────────────────────────── フロントページの続き (51)Int.Cl.6 識別記号 庁内整理番号 ＦＩ 技術表示箇所 Ｃ１０Ｍ 129:74 129:10 139:00 135:10 139:06 139:02 139:04） Ｃ１０Ｎ 20:00 Ａ 20:02 50:10

Claims (1)

    【特許請求の範囲】
  1. 【請求項１】 フルオロシリコーンオイル（イ）、フッ
    素樹脂系増ちょう剤（ロ）と下記（ａ）、（ｂ）、
    （ｃ）、（ｄ）、（ｅ）、（ｆ）および（ｇ）で表わさ
    れる添加剤（ハ）の少なくとも１種以上を含有すること
    を特徴とする耐熱性グリース組成物。 【化１】 ３，９−ビス〔１，１−ジメチル−２−｛β−（３−ｔ
    −ブチル−４−ハイドロキシ−５−メチルフェニル）プ
    ロピオニルオキシ｝エチル〕−２，４，８，１０−テト
    ラオキサスピロ〔５，５〕ウンデカン 【化２】 （Ｒ：炭素原子数１２のアルキル基） 【化３】 １，１，３−トリス（２−メチル−４−ヒドロキシ−５
    −ｔ−ブチルフエニル）ブタン 【化４】 銅フタロシアニン（Ｃｕ−Ｐｈｔｈａｌｏｃｙａｎｉｎ
    ｅ） 【化５】Ｒ−ＳＯ3Ｃａ （ｅ） （Ｒ：アルキル基） カルシウムスルフォネイト（Ｃａ−Ｓｕｌｆｏｎａｔ
    ｅ） アセチルアセトン銅塩（ｆ） 次のと 両末端が４−（フェニルアミノ）フェノキシ・ジメチ
    ルシリル基で封鎖されてなるジメチルポリシロキサンお
    よびポリジメチルシロキサンとジルコニウムカルボキ
    シレートの混合物（但し該混合物中のジルコニウム金属
    の含有量は、０．１〜１０重量％）を不活性雰囲気下で
    ジルコニウムカルボキシレートを分解できる温度で加熱
    して得られたもの。（ｇ）
JP6308121A 1994-11-17 1994-11-17 耐熱性グリース組成物 Pending JPH08143883A (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP6308121A JPH08143883A (ja) 1994-11-17 1994-11-17 耐熱性グリース組成物
EP95308254A EP0717099A1 (en) 1994-11-17 1995-11-17 Heat resistant grease
US08/837,663 US5908815A (en) 1994-11-17 1997-04-22 Heat resistant grease

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP6308121A JPH08143883A (ja) 1994-11-17 1994-11-17 耐熱性グリース組成物

Publications (1)

Publication Number Publication Date
JPH08143883A true JPH08143883A (ja) 1996-06-04

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ID=17977138

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Application Number Title Priority Date Filing Date
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Country Link
US (1) US5908815A (ja)
EP (1) EP0717099A1 (ja)
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JP2000303088A (ja) * 1999-04-16 2000-10-31 Koyo Seiko Co Ltd 潤滑剤組成物とそれを用いた転がり軸受
JP2001354986A (ja) * 2000-06-12 2001-12-25 Nok Kuluver Kk 潤滑グリース組成物
JP2002194379A (ja) * 2000-12-27 2002-07-10 Ge Toshiba Silicones Co Ltd 放熱グリース
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JP2015151516A (ja) * 2014-02-18 2015-08-24 協同油脂株式会社 シリコーングリース組成物
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JP2001354986A (ja) * 2000-06-12 2001-12-25 Nok Kuluver Kk 潤滑グリース組成物
JP4505954B2 (ja) * 2000-06-12 2010-07-21 Ｎｏｋクリューバー株式会社 潤滑グリース組成物
JP2002194379A (ja) * 2000-12-27 2002-07-10 Ge Toshiba Silicones Co Ltd 放熱グリース
US8182155B2 (en) 2005-09-02 2012-05-22 Ntn Corporation Lubricating grease and lubricating grease-enclosed roller bearing
US9868877B2 (en) 2009-06-30 2018-01-16 Daikin Industries, Ltd. Composition and method for producing the same, and powder coating material, pellet, resin formed article, and electric wire
JP2011213894A (ja) * 2010-03-31 2011-10-27 Daikin Industries Ltd 組成物、ペレット、樹脂成形品及び電線、並びに、組成物の製造方法
JP2014141544A (ja) * 2013-01-22 2014-08-07 Adeka Corp 潤滑油用酸化防止剤組成物及びそれを含有する潤滑油組成物
JP2015151516A (ja) * 2014-02-18 2015-08-24 協同油脂株式会社 シリコーングリース組成物
WO2015125805A1 (ja) * 2014-02-18 2015-08-27 協同油脂株式会社 シリコーングリース組成物
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