KR910009573B1 - 실리카의 제조방법 - Google Patents

실리카의 제조방법 Download PDF

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Publication number
KR910009573B1
KR910009573B1 KR1019850004952A KR850004952A KR910009573B1 KR 910009573 B1 KR910009573 B1 KR 910009573B1 KR 1019850004952 A KR1019850004952 A KR 1019850004952A KR 850004952 A KR850004952 A KR 850004952A KR 910009573 B1 KR910009573 B1 KR 910009573B1
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KR
South Korea
Prior art keywords
silica
minutes
colloid
volume
reaction
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Expired
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KR1019850004952A
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English (en)
Korean (ko)
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KR860001008A (ko
Inventor
슈발리에 이보니끄
Original Assignee
롱-쁠랑 쉬미드 바쓰
헨리 마틴
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Publication of KR860001008A publication Critical patent/KR860001008A/ko
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Publication of KR910009573B1 publication Critical patent/KR910009573B1/ko
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/19—Oil-absorption capacity, e.g. DBP values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/90—Other properties not specified above

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Silicon Compounds (AREA)
  • Lubricants (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Fats And Perfumes (AREA)
KR1019850004952A 1984-07-11 1985-07-11 실리카의 제조방법 Expired KR910009573B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR8411004A FR2567505B1 (fr) 1984-07-11 1984-07-11 Silice a prise d'huile elevee et a structure primaire controlee et procede pour son obtention
FR8411004 1984-07-11
FR84.11004 1984-07-11

Publications (2)

Publication Number Publication Date
KR860001008A KR860001008A (ko) 1986-02-22
KR910009573B1 true KR910009573B1 (ko) 1991-11-21

Family

ID=9306012

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019850004952A Expired KR910009573B1 (ko) 1984-07-11 1985-07-11 실리카의 제조방법

Country Status (8)

Country Link
US (3) US4708859A (https=)
EP (1) EP0170579B1 (https=)
JP (1) JPS61117113A (https=)
KR (1) KR910009573B1 (https=)
AT (1) ATE40669T1 (https=)
CA (1) CA1285116C (https=)
DE (1) DE3568155D1 (https=)
FR (1) FR2567505B1 (https=)

Families Citing this family (53)

* Cited by examiner, † Cited by third party
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FR2589871B1 (fr) * 1985-09-13 1987-12-11 Rhone Poulenc Chim Base Charge renforcante pour elastomere a base de silice
GB8713263D0 (en) * 1987-06-05 1987-07-08 Unilever Plc Spheroidal silica
US5614177A (en) * 1987-11-04 1997-03-25 Rhone-Poulenc Chimie Dentifrice-compatible silica particulates
US5286478A (en) * 1987-11-04 1994-02-15 Rhone-Poulenc Chimie Dentifrice-compatible silica particulates
FR2631620B1 (fr) * 1988-05-19 1990-07-27 Rhone Poulenc Chimie Nouvelle silice precipitee absorbante et composition a base de cette s ilice
FR2632185B1 (fr) * 1988-06-01 1992-05-22 Rhone Poulenc Chimie Silice pour compositions dentifrices compatible notamment avec le zinc
FR2649089B1 (fr) * 1989-07-03 1991-12-13 Rhone Poulenc Chimie Silice a porosite controlee et son procede d'obtention
US5225177A (en) * 1990-01-19 1993-07-06 J. M. Huber Corporation Dentifrice abrasives and compositions
US5094829A (en) * 1990-06-21 1992-03-10 Ppg Industries, Inc. Reinforced precipitated silica
FR2678259B1 (fr) * 1991-06-26 1993-11-05 Rhone Poulenc Chimie Nouvelles silices precipitees sous forme de granules ou de poudres, procedes de synthese et utilisation au renforcement des elastomeres.
US6001322A (en) * 1993-09-29 1999-12-14 Rhone-Poulenc Chimie Precipitated silicas
US6169135B1 (en) 1993-09-29 2001-01-02 Rhone Poulenc Chimie Precipitated silica
EP0670813B1 (fr) * 1993-09-29 2003-03-12 Rhodia Chimie Silice precipitee
FR2710630B1 (fr) * 1993-09-29 1995-12-29 Rhone Poulenc Chimie Nouvelles silices précipitées, leur procédé de préparation et leur utilisation au renforcement des élastomères.
WO1995017459A1 (en) * 1993-12-20 1995-06-29 Ppg Industries, Inc. Tire tread composition comprising highly reinforcing silica
WO1995017458A1 (en) * 1993-12-20 1995-06-29 Ppg Industries, Inc. Tire tread composition comprising highly reinforcing silica
FR2714369B1 (fr) * 1993-12-29 1996-01-26 Rhone Poulenc Chimie Silices abrasives pour compositions dentifrices.
FR2732331B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant du zinc et leur utilisation au renforcement des elastomeres
JP2908253B2 (ja) * 1994-09-26 1999-06-21 日本化学工業株式会社 水和珪酸とその製造方法
US5846506A (en) * 1994-10-07 1998-12-08 Degussa Aktiengesellschaft Precipitated silicas
US5571494A (en) * 1995-01-20 1996-11-05 J. M. Huber Corporation Temperature-activated polysilicic acids
FR2732330B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant du zinc et leur utilisation au renforcement des elastomeres
IL117915A (en) * 1995-04-19 2001-05-20 Ppg Ind Ohio Inc Amorphous precipitated silica having large liquid carrying capacity
US5911963A (en) * 1995-05-12 1999-06-15 Ppg Industries Ohio, Inc. Amorphous precipitated silica having a low proportion of small pores
DE19527278A1 (de) * 1995-07-26 1997-01-30 Degussa Fällungskieselsäure
US5804293A (en) * 1995-12-08 1998-09-08 Ppg Industries, Inc. Coating composition for recording paper
EP0902758B1 (en) * 1996-05-31 2001-06-06 PPG Industries Ohio, Inc. Amorphous precipitated silica
KR100342941B1 (ko) * 1996-05-31 2002-08-22 피피지 인더스트리즈 오하이오 인코포레이티드 무정형의침전된실리카
FR2750692B1 (fr) * 1996-07-05 1998-10-16 Rhone Poulenc Chimie Nouvelle silice abrasive, utilisable dans les dentifrices, son procede de preparation et compositions dentifrices la contenant
FR2762611B1 (fr) * 1997-04-29 1999-06-11 Atochem Elf Sa Silice poreuse modifiee, son procede de fabrication et son utilisation dans les peintures et comme vecteur de pigments et colorants
US5891949A (en) * 1997-05-02 1999-04-06 J.M. Huber Corporation Natural rubber compound
US5929156A (en) * 1997-05-02 1999-07-27 J.M. Huber Corporation Silica product for use in elastomers
FR2763581B1 (fr) * 1997-05-26 1999-07-23 Rhodia Chimie Sa Silice precipitee utilisable comme charge renforcante pour elastomeres
US6607648B1 (en) * 1998-11-10 2003-08-19 Integrity Technologies Llc Method and apparatus for generating aqueous silica network particles
US6573032B1 (en) * 1999-04-22 2003-06-03 J. M. Huber Corporation Very high structure, highly absorptive hybrid silica and method for making same
US6624233B2 (en) 1999-05-31 2003-09-23 Pirelli Pneumatici S.P.A. Low rolling resistance tire for vehicles
BR0011098A (pt) * 1999-05-31 2002-03-26 Pirelli Pneu com baixa resistência ao rolamento para veìculos, banda de rodagem com baixa resistência ao rolamento para pneus de veìculo, e, método para redução da resistência ao rolamento de um pneu
CA2292819A1 (en) * 1999-12-22 2001-06-22 Bayer Inc. Process for the production of a precipitated silica slurry with a controlled aggregate particle size distribution
US7700062B2 (en) * 2000-10-13 2010-04-20 University Of Cincinnati Methods for synthesizing precipitated silica and use thereof
EP1284277B1 (de) * 2001-08-08 2004-10-20 Degussa Aktiengesellschaft Mit Siliziumdioxid umhüllte Metalloxidpartikel
US20030096900A1 (en) * 2001-11-16 2003-05-22 Holden Brian David Organic plant derived precipitated silica aggregates, elastomers reinforced therewith and articles such as tires with component thereof
FR2833937B1 (fr) * 2001-12-26 2004-11-12 Rhodia Chimie Sa Silices a faible reprise en eau
EP1495502A4 (en) * 2002-02-07 2006-12-13 Kvg Technologies Inc GELIFIED ELECTROLYTE LEAD BATTERY BATTERY, FORMED BY FILTRATION OF ABSORBENT SEPARATORS, ITS ELECTROLYTES, AND ITS ABSORBENT SEPARATORS
JP2005053728A (ja) * 2003-08-01 2005-03-03 Dsl Japan Co Ltd 高吸油性および高い構造性を有する非晶質シリカ粒子
IN2007DE00954A (https=) * 2007-05-03 2016-05-06
FR2928363B1 (fr) * 2008-03-10 2012-08-31 Rhodia Operations Nouveau procede de preparation de silices precipitees, silices precipitees a morphologie, granulometrie et porosite particulieres et leurs utilisations, notamment pour le renforcement de polymeres
US8790608B2 (en) * 2008-09-12 2014-07-29 Nalco Company Siliceous materials having tunable porosity and surface morphology and methods of synthesizing same
CN102164853B (zh) * 2008-09-26 2014-12-31 扶桑化学工业株式会社 含有具有弯曲结构和/或分支结构的二氧化硅二次颗粒的胶体二氧化硅及其制造方法
US8609068B2 (en) 2010-02-24 2013-12-17 J.M. Huber Corporation Continuous silica production process and silica product prepared from same
JP5495880B2 (ja) * 2010-03-25 2014-05-21 扶桑化学工業株式会社 コロイダルシリカの二次粒子径調整方法
US20130109072A1 (en) * 2010-06-09 2013-05-02 National Institute Of Advanced Industrial Science And Technology Support for protein immobilization, immobilized protein, and methods for producing the same
US9028605B2 (en) 2011-02-25 2015-05-12 J.M. Huber Corporation Coating compositions comprising spheroid silica or silicate
JP2025542087A (ja) 2022-11-08 2025-12-25 エボニック オペレーションズ ゲーエムベーハー 沈降シリカおよびその方法

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US2466842A (en) * 1945-11-15 1949-04-12 Davison Chemical Corp Method for making silica hydrosol
US2577485A (en) * 1950-09-08 1951-12-04 Du Pont Process of making stable silica sols and resulting composition
GB710015A (en) * 1950-12-02 1954-06-02 Degussa An improved process for the production of finely divided silica
CH341802A (de) * 1955-02-03 1959-10-31 Basf Ag Verfahren zur kontinuierlichen Herstellung kieselsäurehaltiger Hydrogele
US2956957A (en) * 1956-04-02 1960-10-18 Grace W R & Co Method for producing clear, homogeneous silica hydrosols
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FR2353486A1 (fr) * 1976-06-04 1977-12-30 Rhone Poulenc Ind Nouvelle silice de synthese amorphe, procede pour son obtention et application de ladite silice dans les vulcanisats
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Also Published As

Publication number Publication date
US4708859A (en) 1987-11-24
DE3568155D1 (en) 1989-03-16
JPH0130764B2 (https=) 1989-06-21
US4874594A (en) 1989-10-17
US4842838A (en) 1989-06-27
EP0170579B1 (fr) 1989-02-08
FR2567505A1 (fr) 1986-01-17
ATE40669T1 (de) 1989-02-15
EP0170579A1 (fr) 1986-02-05
FR2567505B1 (fr) 1986-11-21
CA1285116C (en) 1991-06-25
KR860001008A (ko) 1986-02-22
JPS61117113A (ja) 1986-06-04

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Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20011122

P22-X000 Classification modified

St.27 status event code: A-4-4-P10-P22-nap-X000