KR910008019A - 폴리이미드/지방족 폴리에스테르 공중합체 - Google Patents

폴리이미드/지방족 폴리에스테르 공중합체 Download PDF

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KR910008019A
KR910008019A KR1019900016342A KR900016342A KR910008019A KR 910008019 A KR910008019 A KR 910008019A KR 1019900016342 A KR1019900016342 A KR 1019900016342A KR 900016342 A KR900016342 A KR 900016342A KR 910008019 A KR910008019 A KR 910008019A
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bis
aminophenoxy
diamine
mda
dianhydride
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KR1019900016342A
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KR100186775B1 (ko
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윈스톤 호 윈-소우
사르토리 구이도
알랜 탈러 워렌
크레이그 달림플 데이비드
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앤 허쉬코비츠 제이콥슨
엑손 리써치 앤드 엔지니어링 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
    • B01D61/362—Pervaporation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
    • B01D61/362—Pervaporation
    • B01D61/3621—Pervaporation comprising multiple pervaporation steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/48—Polyesters
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/76—Macromolecular material not specifically provided for in a single one of groups B01D71/08 - B01D71/74
    • B01D71/80—Block polymers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/144—Purification; Separation; Use of additives using membranes, e.g. selective permeation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
    • C08G73/06—Polycondensates having nitrogen-containing heterocyclic rings in the main chain of the macromolecule
    • C08G73/10—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
    • C08G73/16—Polyester-imides

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Analytical Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)

Abstract

내용 없음

Description

폴리이미드/지방족 폴리에스테르 공중합체
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 2개의 염소를 가진 폴리우레아/우레탄 경성 분절(segment) 및 분자량 2000의 폴리에틸렌 아디페이트(PEA 2000) 연성 분절을 함유하는 공중합체의 합성 및 조성을 도시한다.
제2도는 폴리우레탄의 연성 분절이 수착성(sorption) 즉, 선택성 및 투과성을 조절함을 도시한다.
제3도는 다른 경성 분절들을 가진 세가지의 폴리우레탄을 도시한다.

Claims (15)

  1. 탄소수 8 내지 20의 이무수물과 탄소수 2내지 30의 디아민으로부터 유도된 폴리이미드 경성 분절(hard segment), 및 폴리아디페이트, 폴리석시네이트, 폴리말로네이트, 폴리옥살레이트 또는 폴리글루타레이트인 올리고머성 지방족 폴리에스테르 연성 분절을 포함하는 공중합체 조성물을 포함한 박막을 통해 방향족 탄화수소를 선택적으로 투과시킴을 포함하는, 방향족 및 비방향족 화합물의 혼합물인 공급물로부터 방향족 화합물을 분리하는 방법.
  2. 제1항에 있어서, 상기 이무수물이 방향족 화합물인 방법.
  3. 제1항에 있어서, 상기 디아민이 페닐렌 디아민, 메틸렌 디아닐린(MDA), 메틸렌-디-o-클로로아닐린(MOCA), 메틸렌비스(디클로로아닐린)(테트라클로로 MDA), 메틸렌디사이클로헥실아민(H12-MDA), 메틸렌디클로로 사이클로헥실아민(H12-MOCA), 메틸렌 비스(디클로로 사이클로헥실아민)(테트라클로로 H12-MDA), 4,4'-(헥시플루오로이소프로필리덴)-비스아닐린(6F 디아민), 3,3'-디아미노페닐 설폰(3.3'DAPSON), 4,4'-디아미노페닐 설폰(4.4' DAPSON), 4.4' -디메틸-3.3'- 디아미노페닐 설폰(4.4' -디메틸-3,3'-DAPSON), 2,4-디아미노 큐멘, 메틸 비스(디-o-톨루이딘), 옥시디아닐린(ODA), 비스아닐린 A, 비스아닐린 M, 비스아닐린 P, 티오디아닐린, 2,2-비스[4-(4-아미노페녹시)페닐]프로판(BAPP), 비스[4-(4-아미노페녹시)페닐]설폰(BAPS), 4,4'-비스(4-아미노페녹시)비페닐(BAPB), 1,4-비스(4-아미노페녹시)벤젠(TPE-Q), 및 1,3-비스(4-아미노페녹시)벤젠(TPE-R)로 이루어진 그룹중에서 선택되는 방법.
  4. 제2항에 있어서, 상기 방향족 화합물이 파이로델리트산 이무수물, 3,3',4,4'-벤조패논 테트라카복실산 이무수물, 4,4'-(헥사플루오로이소프로필리덴)-비스(프탈산무수물), 4,4'-옥시디프탈산 무수물, 디페닐설폰-3,3', 4,4'-테트라카복실산 이무수물 및 3,3', 4,4'-비페닐테트라카복실산 이무수물로 이루어진 그룹중에서 선택되는 방법.
  5. 제1항에 있어서, 상기 폴리에스테르가 폴리에틸렌 아디페이트인 방법.
  6. 제1항에 있어서, 상기 폴리에스테르가 폴리에틸렌 석시네이트인 방법.
  7. 제1항에 있어서, 상기 디아민이 메틸렌 디-o-클로로아닐린인 방법.
  8. 130℃이상의 유리 전이 온도를 갖는 경성 분절 및 경성 분절의 Tg보다 낮은 Tg를 갖는 연성 분절을 포함하는 물질의 공중합체 조성물.
  9. 제8항에 있어서, 탄소수 8 내지 20의 이무수물과 탄소수 2 내지 30의 디아민으로부터 유도된 폴리이미드 경성 분절, 및 폴리아디페이트, 폴리석시네이트, 폴리말로네이트, 폴리옥살레이트 또는 폴리글루타레이트인 올리고머성 지방족 폴리에스테르 연성 분절을 포함하는 공중합체 조성물.
  10. 제9항에 있어서, 상기 이무수물이 방향족 화합물이 조성물.
  11. 제9항에 있어서, 상기 디아민이 페닐렌 디아민, 메틸렌 디아닐린(MDA), 메틸렌-디-o-클로로아닐린(MOCA), 메틸렌비스(디클로로아닐린)(테트라클로로 MDA), 메틸렌디사이클로헥실아민(H12-MDA), 메틸렌디클로로 사이클로헥실아민(H12-MOCA), 메틸렌 비스(디클로로 사이클로헥실아민)(테트라클로로 H12-MDA), 4,4'-(헥사플루오로이소프로필리덴)-비스 아닐린(6F 디아민), 3,3'-디아미노페닐 설폰(3,3' DAPSON), 4,4'-디아미노페닐 설폰(4,4' DAPSON), 4,4'-디메틸-3,3'-디아미노페닐 설폰(4,4'-디메틸-3,3'-DAPSON), 2,4-디아미노 큐멘, 메틸 비스(디-o-톨루이딘), 옥시디아닐린(ODA), 비스 아닐린 A, 비스아닐린 M, 비스아닐린 P, 티오디아닐린, 2,2-비스[4-(4-아미노페녹시)페닐]프로판(BAPP), 비스[4-(4-아미노페녹시)페닐]설폰(BAPS), 4,4'-비스(4-아미노페녹시)비페닐(BAPB), 1,4-비스(4-아미노페녹시)벤젠(TPE-Q), 및 1,3-비스(4-아미노페녹시)벤젠(TPE-R)로 이루어진 그룹중에서 선택되는 조성물.
  12. 제10항에 있어서, 상기 방향족 화합물이 파이로멜리트산 이무수물, 3,3'4,4'-벤조패논 테트라카복실산 이무수물, 4,4'-(헥사플루오로이소프로필리덴)-비스(프탈산무수물), 4,4'-옥시디프탈산 무수물, 디페닐설폰-3,3', 4,4'-테트라카복실산 이무수물 및 3,3', 4,4'-비페닐테트라카복실산 이무수물로 이루어진 그룹중에서 선택되는 조성물.
  13. 제9항에 있어서, 상기 폴리에스테르가 폴리에틸렌 아디페이트인 조성물.
  14. 제9항에 있어서, 상기 폴리에스테르가 폴리에틸렌 석시네이트인 조성물.
  15. 제1항에 있어서, 상기 디아민이 메틸렌 디-o-클로로아닐린인 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019900016342A 1989-10-16 1990-10-15 폴리이미드/지방족 폴리에스테르 공중합체 조성물을 사용하여 방향족 및 비방향족 화합물의 혼합물로부터 방향족 화합물을 분리하는 방법 KR100186775B1 (ko)

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KR1019980034636A KR100195664B1 (en) 1989-10-16 1998-08-26 Polyimide/aliphatic polyester copolymers

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US07/422,385 US4944880A (en) 1989-10-16 1989-10-16 Polyimide/aliphatic polyester copolymers
US422,385 1989-10-16

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KR100186775B1 KR100186775B1 (ko) 1999-05-15

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US (1) US4944880A (ko)
EP (1) EP0424041B1 (ko)
JP (1) JPH03207434A (ko)
KR (1) KR100186775B1 (ko)
CA (1) CA2026788C (ko)
DE (1) DE69026022T2 (ko)
ES (1) ES2084666T3 (ko)
MY (1) MY107151A (ko)

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JPH03207434A (ja) 1991-09-10
EP0424041A3 (en) 1991-08-21
DE69026022D1 (de) 1996-04-25
US4944880A (en) 1990-07-31
MY107151A (en) 1995-09-30
CA2026788C (en) 2001-01-30
KR100186775B1 (ko) 1999-05-15
ES2084666T3 (es) 1996-05-16
EP0424041B1 (en) 1996-03-20
CA2026788A1 (en) 1991-04-17
DE69026022T2 (de) 1996-09-05
EP0424041A2 (en) 1991-04-24

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