KR910002957A - 폴리아릴렌술피드의 제조방법과 분말상 폴리아릴렌술피드의 회수사용방법 - Google Patents

폴리아릴렌술피드의 제조방법과 분말상 폴리아릴렌술피드의 회수사용방법 Download PDF

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KR910002957A
KR910002957A KR1019900010764A KR900010764A KR910002957A KR 910002957 A KR910002957 A KR 910002957A KR 1019900010764 A KR1019900010764 A KR 1019900010764A KR 900010764 A KR900010764 A KR 900010764A KR 910002957 A KR910002957 A KR 910002957A
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polyarylene sulfide
producing
phase separation
powdered
sulfur source
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KR1019900010764A
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미노루 센가
아끼라 미요시
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홍고오 므쯔미
이데미쯔세끼유가가꾸 가부시기가이샤
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Publication of KR910002957A publication Critical patent/KR910002957A/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/0209—Polyarylenethioethers derived from monomers containing one aromatic ring
    • C08G75/0213—Polyarylenethioethers derived from monomers containing one aromatic ring containing elements other than carbon, hydrogen or sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0254—Preparatory processes using metal sulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0259—Preparatory processes metal hydrogensulfides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/025—Preparatory processes
    • C08G75/0272—Preparatory processes using other sulfur sources
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/0277—Post-polymerisation treatment
    • C08G75/0281—Recovery or purification
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/02—Polythioethers
    • C08G75/0204—Polyarylenethioethers
    • C08G75/0286—Chemical after-treatment

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)

Abstract

내용 없음.

Description

폴리아릴렌술피드의 제조방법과 분말상 폴리아릴렌술피드의 회수사용방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (9)

  1. 유기극성 용매속에서 유황원과 디할로방향족화합물을 증축합반응시켜서 폴리아릴렌술피드를 얻는 제조방법에 있어서, 분말상 폴리아릴렌술피드의 존재하에 증축합반응하는 것을 특징으로하는 폴리아릴렌술피드의 제조방법.
  2. 제1항에 있어서, 상기 분말상 폴리아릴렌술피드는 그 입도가 0.2mm이하인 것을 특징으로하는 폴리아릴렌술피드의 제조방법.
  3. 제1항에 있어서, 상기 분말상 폴리아릴렌술피드는, 24~200매시의 체를 통과하는 분말인 것을 특징으로 하는 폴리아릴렌술피드의 제조방법.
  4. 제1항에 있어서, 상기 분말상 폴리아릴렌술피드의 첨가량이, 디할로방향족화합물에 대해서 1~50중량%인 것을 특징으로 하는 폴리아릴렌술피드의 제조방법.
  5. 제1항에 있어서, 증축합반응을 상분리제의 존재하에 행하는것을 특징으로하는 폴리아릴렌술피드의 제조방법.
  6. 제5항에 있어서, 상기 상분리제가 물,할로겐화리튬, 및 알칼리금속의 아세트산염으로 이루어진 군으로부터 선택되는 적어도 1종인 것을 특징으로 하는 폴리아릴렌술피드의 제조방법.
  7. 제6항에 있어서, 상기 유황원과 상기 상분리제인 물 이외의 상분리제와의 사용비율로서, 상기 유황원의 유황원자 1몰에 대해서, 상기 상분리제가 0.05~2.0몰인 것을 특징으로하는 폴리아릴렌술피드의 제조방법.
  8. 제5항에 있어서, 상기 상분리제가 증축합전에 반응계에 첨가되는 것을 특징으로하는 폴리아릴렌술피드의 제조방법.
  9. 유기극성 용매속에서 유황원과 디할로방향족화합물을 증축합반응시켜서 폴리아릴렌술피드를 얻는 제조방법에 있어서, 증축합반응에 의해 얻게된 폴리아릴렌술피드를 입상폴리아릴렌술피드의 분말상 폴리아릴렌술피드로 분리하고, 얻게되는 분말상 폴리아릴렌술피드를, 유기극성용매속에서, 유황원 및 디할로방향족화합물을 가진 혼합물에 첨가해서, 분말상 폴리아릴렌 술피드의 존재하에 유기극성용매속에서 유황원과 디할로방향족화합물을 증축합반응시키는 것을 특징으로 하는 분말상 폴리아릴렌술피드의 회수사용방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019900010764A 1989-07-17 1990-07-16 폴리아릴렌술피드의 제조방법과 분말상 폴리아릴렌술피드의 회수사용방법 KR910002957A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP1-184375 1989-07-17
JP1184375A JPH0672185B2 (ja) 1989-07-17 1989-07-17 ポリアリーレンスルフィドの製造方法

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KR910002957A true KR910002957A (ko) 1991-02-26

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KR1019900010764A KR910002957A (ko) 1989-07-17 1990-07-16 폴리아릴렌술피드의 제조방법과 분말상 폴리아릴렌술피드의 회수사용방법

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EP (1) EP0409105B1 (ko)
JP (1) JPH0672185B2 (ko)
KR (1) KR910002957A (ko)
CA (1) CA2021393A1 (ko)
DE (1) DE69031672T2 (ko)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2997725B2 (ja) * 1990-09-28 2000-01-11 出光石油化学株式会社 塩化リチウムの回収法
KR100189767B1 (ko) * 1991-06-24 1999-06-01 린다 에스 잘리 폴리(아릴렌설파이드)중합체 제조 방법
US5210128A (en) * 1991-07-24 1993-05-11 Phillips Petroleum Company Poly(arylene sulfide) compositions, composites, and methods of production
CA2111404A1 (en) * 1992-12-31 1994-07-01 Jon F. Geibel Process for preparing poly(arylene sulfide) polymers using high molecular weight poly(arylene sulfide) polymer as a reactant
JP2002265603A (ja) * 2001-03-12 2002-09-18 Idemitsu Petrochem Co Ltd ポリアリーレンスルフィドの製造方法
JP2002293938A (ja) * 2001-03-30 2002-10-09 Petroleum Energy Center ポリアリーレンスルフィドの連続製造方法
JP2002293939A (ja) * 2001-03-30 2002-10-09 Petroleum Energy Center ポリアリーレンスルフィドの製造方法
CN102105513B (zh) * 2008-07-31 2012-11-28 株式会社吴羽 粒状聚芳撑硫醚的制造方法
EP3088443A4 (en) * 2013-12-25 2017-08-02 Toray Industries, Inc. Polyphenylene sulphide block copolymer, method for manufacturing same, and method for manufacturing polyphenylene sulphide porous body

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4415729A (en) * 1982-06-04 1983-11-15 Phillips Petroleum Company Recovering granular poly(arylene sulfide) particles from a poly(arylene sulfide) reaction mixture
US4405767A (en) * 1982-06-22 1983-09-20 Phillips Petroleum Company Treatment of poly(arylene sulfide)
JPS617332A (ja) * 1984-06-20 1986-01-14 Kureha Chem Ind Co Ltd 高分子量ポリアリ−レンスルフイドの製造法
JPS62195022A (ja) * 1986-02-21 1987-08-27 Dainippon Ink & Chem Inc 高分子量アリ−レンスルフイドポリマ−の製造法
EP0257228A1 (en) * 1986-07-25 1988-03-02 Tohpren Co., Ltd. Polyphenylene sulfide resin composition
JPH07106595B2 (ja) * 1987-04-24 1995-11-15 呉羽化学工業株式会社 熱成形ポリアリ−レンスルフイド容器及びその製造法

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JPH0350237A (ja) 1991-03-04
DE69031672T2 (de) 1998-06-04
EP0409105B1 (en) 1997-11-05
EP0409105A2 (en) 1991-01-23
EP0409105A3 (en) 1991-11-21
CA2021393A1 (en) 1991-01-18
DE69031672D1 (de) 1997-12-11
JPH0672185B2 (ja) 1994-09-14

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