KR910001027A - 냉수중에서 분산될 수 있는 고활성 세제 입자 - Google Patents
냉수중에서 분산될 수 있는 고활성 세제 입자 Download PDFInfo
- Publication number
- KR910001027A KR910001027A KR1019900008446A KR900008446A KR910001027A KR 910001027 A KR910001027 A KR 910001027A KR 1019900008446 A KR1019900008446 A KR 1019900008446A KR 900008446 A KR900008446 A KR 900008446A KR 910001027 A KR910001027 A KR 910001027A
- Authority
- KR
- South Korea
- Prior art keywords
- weight
- paste
- water
- temperature
- alkyl
- Prior art date
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims 11
- 239000002245 particle Substances 0.000 title claims 8
- 239000003599 detergent Substances 0.000 title claims 6
- 238000000034 method Methods 0.000 claims 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 9
- 150000008051 alkyl sulfates Chemical class 0.000 claims 5
- 239000002202 Polyethylene glycol Substances 0.000 claims 4
- -1 alkyl sulfuric acid Chemical compound 0.000 claims 4
- 238000006386 neutralization reaction Methods 0.000 claims 4
- 229920001223 polyethylene glycol Polymers 0.000 claims 4
- 229910052708 sodium Inorganic materials 0.000 claims 3
- 239000011734 sodium Substances 0.000 claims 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 239000004744 fabric Substances 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims 2
- 239000000463 material Substances 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 229910021653 sulphate ion Inorganic materials 0.000 claims 2
- 238000005406 washing Methods 0.000 claims 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
- 230000029936 alkylation Effects 0.000 claims 1
- 238000005804 alkylation reaction Methods 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 239000002736 nonionic surfactant Substances 0.000 claims 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 1
- 238000004321 preservation Methods 0.000 claims 1
- 239000000344 soap Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
내용 없음.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (16)
- (a) 물 약 14중량% 미만 및 추가 성분 약 20중량% 미만을 함유하는 중화된 (C12내지 C18)알킬 설페이트 페이스트를 제조하고, (b) 페이스트를 약 10 내지 45℃의 온도에서 유지시키면서 페이스트에 기계적으로 작동(이때, 기계적 작동은 입자를 약 4 내지 30℃ 온도의 수중에서 약 10분동안 진탕시킨후 실질적으로 분산되도록 하기에 충분한 양을 적용한다)을 적용시킨 후, (c) 작동된 페이스트로부터 세제 입자를 형성시킴을 특징으로 하여, 냉수중에서 분산될 수 있는 고활성 세제 입자를 제조하는 방법.
- 제1항에 있어서, 기계적 작동이 롤 제분기, 압출기, 비누 플라더 또는 이의 혼합에 의해 수행되는 방법.
- 제2항에 있어서, 페이스트가 약 8내지 12중량%의 물을 함유하는 방법.
- 제3항에 있어서, 추가성분은 분자량이 약 4,000 내지 50,000인 폴리에틸렌 글리콜: 융점이 약 48℃ 이상인 일반식 R(OC2H4)nOH {여기서, R은 (C12내지 C18) 알킬 그룹 또는(C8내지 C16)알킬 페놀 그룹이고, n은 약 9 내지 약 80이다)의 에톡실화 비이온성 계면활성제 : 및 이의 혼합물로 이루어진 그룹중에서 선택되는 방법.
- 제4항에 있어서, 기계적 작동이 입자가 약 5내지 20℃온도의 수중에서 약 10분동안 진탕시킨 후에 실질적으로 분산되기에 충분한 양으로 적용되는 방법.
- 제5항에 있어서, 페이스트 온도가, 기계적 작동을 적용시키면서, 약 15 내지 40℃에서 유지되는 방법.
- 제6항에 있어서, 중화된 (C12내지 C18) 알킬 설페이트 페이스트가 연속 중화 시스템에서 수산화물이 약 62중량% 이상인 수산화 알칼리 금속 용액과, C12내지 C18)알킬 황산을 반응시켜 제조되는 방법.
- 제7항에 있어서, 중화된 알킬 설페이트 페이스트가 14 내지 16개의 탄소원자를 함유하며 언급된 연속 중화 시스템에서 수산화물이 약 70중량%인 수산화나트륨 용액과 (C14내지 C16)알킬 황산을 반응시켜 제조되는 방법.
- 제8항에 있어서, 추가 성분이 분자량 약 7,000 내지 12,000의 폴리에틸렌 글리콜이고 중화중 연속 중화 시스템에 첨가시키는 방법.
- 제1항에 있어서, 중화된 알킬 설패이트 페이스트는 보존 알킬리도가 약 0.2 내지 1.0% Na20이고 활성이 약 70 내지 75중량%인 방법.
- 제10항에 있어서, 기계적 작동이 약 20 내지 27℃의 롤 온도, 약 20, 40 및 60의 롤 회전/분 및 약 0.004 내지 0.008인치(약 0.1mm 내지 0.2mm)의 최종 롤 클리어런스에서 삼롤 제분기에 대해 1내지 3회 통과시켜 수행되며 페이스트 온도는 약 25 내지 35℃인 방법.
- 제10항에 있어서, 기계적 작동이 1mm의 오우프닝인 압출기 판으로 램 피스톤 압출기를 통해 4내지 6회 통과시켜 수행하는 방법.
- 제1항의 방법에 따라서 제조된 세제 입자.
- (a) 나트륨 (C14내지 C16)알킬 설페이트 약 70 내지 75중량% : (b) 물 약 8 내지 12 중량% : (c) 분자량이 약 7,000내지 12,000인 폴리에틸렌 글리콜 약 5 내지 10중량% : (d) 수산화 나트륨 0 내지 약 6중량% : (e) 비반응 물질 0 내지 약 6중량% : 및 (f) 설페이트 0 내지 약 6중량% {여기서, (c),(d),(e)와 (f)의 총 합은 약 20중량%미만이다)를 함유함을 특징으로 하는, 제11항의 방법에 따라서 제조된 세제 입자.
- 제1항의 방법에 따라서 제조되고 (a) 중화된 (C12내지 C18) 알킬 설페이트 약 60 내지 85중량% : (b) 물 약 14중량%미만 : 및 (c) 추가성분 약 20중량%미만을 함유하는 고활성 세제 입자로 약 4내지 30℃의 수온에서 직물을 세탁하는 방법.
- 제9항의 방법에 따라서 제조되고, (a) 나트륨 (C14내지 C16)알킬 설페이트 약 70 내지 75중량% : (b) 물 약 8내지 12중량% : (c) 분자량이 약 7,000 내지 12,000인 폴리에틸렌 글리콜 약 5 내지 10중량% : (d) 수산화나트륨 0 내지 약 6중량% : (e) 비반응 물질 0 내지 약 6중량% : 및 (f) 설페이트 0 내지 약 6중량% {여기서, (c),(d),(e)와 (f)의 총 합은 약 20중량%미만이다)을 함유하는 고활성 세제 입자로 약 10내지 15℃의 수온에서 직물을 세탁하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US364732 | 1989-06-09 | ||
US07/364,732 US5045238A (en) | 1989-06-09 | 1989-06-09 | High active detergent particles which are dispersible in cold water |
Publications (1)
Publication Number | Publication Date |
---|---|
KR910001027A true KR910001027A (ko) | 1991-01-30 |
Family
ID=23435826
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019900008446A KR910001027A (ko) | 1989-06-09 | 1990-06-09 | 냉수중에서 분산될 수 있는 고활성 세제 입자 |
Country Status (19)
Country | Link |
---|---|
US (1) | US5045238A (ko) |
EP (1) | EP0403148B1 (ko) |
JP (1) | JP2935729B2 (ko) |
KR (1) | KR910001027A (ko) |
CN (1) | CN1027453C (ko) |
AU (1) | AU643441B2 (ko) |
BR (1) | BR9002722A (ko) |
CA (1) | CA2017913C (ko) |
DE (1) | DE69028045T2 (ko) |
EG (1) | EG19508A (ko) |
ES (1) | ES2090101T3 (ko) |
FI (1) | FI902876A0 (ko) |
IE (1) | IE902076L (ko) |
MA (1) | MA21870A1 (ko) |
MX (1) | MX170960B (ko) |
NZ (1) | NZ233998A (ko) |
PE (1) | PE35590A1 (ko) |
PT (1) | PT94314A (ko) |
TR (1) | TR24394A (ko) |
Families Citing this family (24)
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CA2017921C (en) * | 1989-06-09 | 1995-05-16 | John Michael Jolicoeur | Formation of detergent granules by deagglomeration of detergent dough |
CA2017922C (en) * | 1989-06-09 | 1995-07-11 | Frank Joseph Mueller | Formation of discrete, high active detergent granules using a continuous neutralization system |
KR0170424B1 (ko) * | 1990-07-05 | 1999-01-15 | 호르스트 헤를레,요한 글라슬 | 세제 및 청정제용 표면 활성제 과립의 제조방법 |
DE4038476A1 (de) * | 1990-12-03 | 1992-06-04 | Henkel Kgaa | Feste waschmittel |
US5451354A (en) * | 1991-04-12 | 1995-09-19 | The Procter & Gamble Co. | Chemical structuring of surfactant pastes to form high active surfactant granules |
EP0508543B1 (en) * | 1991-04-12 | 1997-08-06 | The Procter & Gamble Company | Chemical structuring of surfactant pastes to form high active surfactant granules |
DE4127323A1 (de) * | 1991-08-20 | 1993-02-25 | Henkel Kgaa | Verfahren zur herstellung von tensidgranulaten |
US5219495A (en) * | 1991-12-16 | 1993-06-15 | Lever Brothers Company, Division Of Conopco, Inc. | Detergent compositions containing mobile liquid active systems |
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DE19911570A1 (de) * | 1999-03-16 | 2000-09-28 | Henkel Kgaa | Aniontensid-Granulate |
EP2154235A1 (en) * | 2008-07-28 | 2010-02-17 | The Procter and Gamble Company | Process for preparing a detergent composition |
WO2014072840A1 (en) | 2012-11-12 | 2014-05-15 | Galaxy Surfactants Ltd. | Flowable, high active, aqueous fatty alkyl sulfates |
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JPS6399797A (ja) * | 1986-10-16 | 1988-05-02 | Toshiba Corp | 可変電圧可変周波数電源装置 |
US4759865A (en) * | 1986-11-06 | 1988-07-26 | Colgate-Palmolive Company | Pasty acid detergent composition |
JPH0816236B2 (ja) * | 1986-12-18 | 1996-02-21 | ライオン株式会社 | 高嵩密度洗剤組成物の製造方法 |
DE68924373T2 (de) * | 1988-06-29 | 1996-05-15 | Procter & Gamble | Verfahren zur Herstellung konzentrierter Granulatkörner von oberflächenaktiven Mitteln. |
US4925585A (en) * | 1988-06-29 | 1990-05-15 | The Procter & Gamble Company | Detergent granules from cold dough using fine dispersion granulation |
CA2017922C (en) * | 1989-06-09 | 1995-07-11 | Frank Joseph Mueller | Formation of discrete, high active detergent granules using a continuous neutralization system |
-
1989
- 1989-06-09 US US07/364,732 patent/US5045238A/en not_active Expired - Lifetime
-
1990
- 1990-05-30 CA CA002017913A patent/CA2017913C/en not_active Expired - Fee Related
- 1990-06-06 EP EP90306138A patent/EP0403148B1/en not_active Expired - Lifetime
- 1990-06-06 DE DE69028045T patent/DE69028045T2/de not_active Expired - Fee Related
- 1990-06-06 ES ES90306138T patent/ES2090101T3/es not_active Expired - Lifetime
- 1990-06-07 EG EG33990A patent/EG19508A/xx active
- 1990-06-07 TR TR90/0558A patent/TR24394A/xx unknown
- 1990-06-08 PE PE1990170619A patent/PE35590A1/es unknown
- 1990-06-08 MA MA22138A patent/MA21870A1/fr unknown
- 1990-06-08 FI FI902876A patent/FI902876A0/fi not_active Application Discontinuation
- 1990-06-08 BR BR909002722A patent/BR9002722A/pt not_active Application Discontinuation
- 1990-06-08 NZ NZ233998A patent/NZ233998A/xx unknown
- 1990-06-08 AU AU56967/90A patent/AU643441B2/en not_active Ceased
- 1990-06-08 PT PT94314A patent/PT94314A/pt not_active Application Discontinuation
- 1990-06-08 MX MX021072A patent/MX170960B/es unknown
- 1990-06-08 IE IE902076A patent/IE902076L/xx unknown
- 1990-06-09 KR KR1019900008446A patent/KR910001027A/ko not_active Application Discontinuation
- 1990-06-09 CN CN90104552A patent/CN1027453C/zh not_active Expired - Fee Related
- 1990-06-11 JP JP2152493A patent/JP2935729B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
IE902076L (en) | 1990-12-09 |
AU643441B2 (en) | 1993-11-18 |
CA2017913C (en) | 1995-07-11 |
ES2090101T3 (es) | 1996-10-16 |
DE69028045T2 (de) | 1997-03-06 |
PE35590A1 (es) | 1991-01-16 |
EG19508A (en) | 1995-06-29 |
AU5696790A (en) | 1990-12-13 |
US5045238A (en) | 1991-09-03 |
EP0403148B1 (en) | 1996-08-14 |
CA2017913A1 (en) | 1990-12-09 |
EP0403148A3 (en) | 1991-02-20 |
PT94314A (pt) | 1991-02-08 |
DE69028045D1 (de) | 1996-09-19 |
JP2935729B2 (ja) | 1999-08-16 |
NZ233998A (en) | 1993-10-26 |
MX170960B (es) | 1993-09-22 |
EP0403148A2 (en) | 1990-12-19 |
CN1048406A (zh) | 1991-01-09 |
BR9002722A (pt) | 1991-08-20 |
MA21870A1 (fr) | 1990-12-31 |
JPH0388900A (ja) | 1991-04-15 |
FI902876A0 (fi) | 1990-06-08 |
CN1027453C (zh) | 1995-01-18 |
TR24394A (tr) | 1991-09-01 |
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