KR830006369A - 알콕시실란의 제조 방법 - Google Patents
알콕시실란의 제조 방법 Download PDFInfo
- Publication number
- KR830006369A KR830006369A KR1019810001908A KR810001908A KR830006369A KR 830006369 A KR830006369 A KR 830006369A KR 1019810001908 A KR1019810001908 A KR 1019810001908A KR 810001908 A KR810001908 A KR 810001908A KR 830006369 A KR830006369 A KR 830006369A
- Authority
- KR
- South Korea
- Prior art keywords
- formula
- carbon atoms
- aryl
- integer
- hydrogen
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 9
- 125000003118 aryl group Chemical group 0.000 claims 6
- 229910052739 hydrogen Inorganic materials 0.000 claims 6
- 239000001257 hydrogen Substances 0.000 claims 6
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 6
- 229920001651 Cyanoacrylate Polymers 0.000 claims 3
- 125000000217 alkyl group Chemical group 0.000 claims 3
- MWCLLHOVUTZFKS-UHFFFAOYSA-N Methyl cyanoacrylate Chemical compound COC(=O)C(=C)C#N MWCLLHOVUTZFKS-UHFFFAOYSA-N 0.000 claims 2
- -1 acrylate halide Chemical class 0.000 claims 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims 2
- 150000004820 halides Chemical class 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims 2
- IJVRPNIWWODHHA-UHFFFAOYSA-N 2-cyanoprop-2-enoic acid Chemical compound OC(=O)C(=C)C#N IJVRPNIWWODHHA-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 229910052697 platinum Inorganic materials 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Catalysts (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (3)
- (1) 다음 구조식(Ⅱ)의 시아노아크릴레이트를 염기 존재하에서 가수분해하고(2) 생성된 시아노아클릴산을 상응하는 산할라이드로 전화시키고(3) 생성된 아클릴산 할라이드와 다음 구조식(Ⅲ)의 아미노알킬알콕시실란을 반응시켜 다음 구조식(I)의 알콕시실란을 제조하는 방법.상기 구조식에서R는 탄소수 1 내지 8의 알킬이고R1은 R, 탄소수 6 내지 13의 아릴 또는 이들의 할로겐화유도체이며,R2는 수소 또는 R기이며,R3는 탄소수 6 내지 13의 아릴이고,R4는 수소, R 또는 R3이며,Y는 구조식의 그룹이며 Q는 -O- 또는a는 1 내지 3의 정수이며,b는 0 내지 2의 정수이고,a+b는 1 내지 3이다.
- (1) 다음 구조식(Ⅳ)의 시아노아크릴레이트와 구조식(Ⅴ)의 알릴알콜을 염기존재하에 반응시키고(2) 상기 (1)항의 생성 내전물을 유효량의 백금촉매 존재하에 구조식(Ⅵ)의 알콕시실란과 반응시켜 구조식(I)의 알콕실란을 제조하는 방법.상기 구조식에서R는 탄소수 1 내지 8의 알킬이고R1은 R, 탄소수 6 내지 13의 아릴 또는 이들의 할로겐화유도체이며,R2는 수소 또는 R기이며,R3는 탄소수 6 내지 13의 아릴이고,R4는 수소, R 또는 R3이며,Y는 구조식의 그룹이며a는 1 내지 3의 정수이며,b는 0 내지 2의 정수이고,a+b는 1 내지 3이다.
- 다음 구조식(Ⅶ)의 알콕시아미노실란을 하이드록시피리덴 존재하에 구조식(Ⅷ)의 시아노아클릴레이트 에스테르와 반응시켜 구조식(I)의 알콕시실란을 제조하는 방법.상기 구조식에서R는 탄소수 1 내지 8의 알킬이고R1은 R, 탄소수 6 내지 13의 아릴 또는 이들의 할로겐화유도체이며,R2는 수소 또는 R기이며,R3는 탄소수 6 내지 13의 아릴이고,R4는 수소, R 또는 R3이며,Y는 구조식의 그룹이며a는 1 내지 3의 정수이며,b는 0 내지 2의 정수이고,a+b는 1 내지 3이다.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019840003403A KR840001686B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
KR1019840003402A KR840001685B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US154,626 | 1980-05-30 | ||
US06/154,626 US4307240A (en) | 1980-05-30 | 1980-05-30 | Alkoxysilanes and method for making |
US154626 | 1980-05-30 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019840003402A Division KR840001685B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
KR1019840003403A Division KR840001686B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR830006369A true KR830006369A (ko) | 1983-09-24 |
KR840001684B1 KR840001684B1 (ko) | 1984-10-15 |
Family
ID=22552093
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019810001908A KR840001684B1 (ko) | 1980-05-30 | 1981-05-29 | 알콕시실란의 제조 방법 |
KR1019840003402A KR840001685B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
KR1019840003403A KR840001686B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
Family Applications After (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019840003402A KR840001685B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
KR1019840003403A KR840001686B1 (ko) | 1980-05-30 | 1984-06-16 | 알콕시실란의 제조방법 |
Country Status (8)
Country | Link |
---|---|
US (1) | US4307240A (ko) |
JP (2) | JPS5721392A (ko) |
KR (3) | KR840001684B1 (ko) |
AU (1) | AU7118881A (ko) |
CA (1) | CA1173454A (ko) |
DE (1) | DE3120847A1 (ko) |
FR (1) | FR2483401A1 (ko) |
GB (1) | GB2077748B (ko) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3312611A1 (de) * | 1983-04-08 | 1984-10-11 | Röhm GmbH, 6100 Darmstadt | Verfahren zur herstellung uv-geschuetzter mehrschichtiger kunststoff-formkoerper |
AT393464B (de) * | 1983-05-25 | 1991-10-25 | Johannes Zimmer | Vorrichtung zum auftragen von aufgeschaeumten oder hochviskosen medien |
JPH067944B2 (ja) * | 1985-10-18 | 1994-02-02 | 富士写真フイルム株式会社 | 塗布方法 |
JPH0655796B2 (ja) * | 1986-06-19 | 1994-07-27 | 日本ペイント株式会社 | ケイ素含有ビニル系重合体 |
JPH0765150B2 (ja) * | 1987-04-30 | 1995-07-12 | 新日本製鐵株式会社 | 溶融金属被覆装置用ノズル |
DE3721593A1 (de) * | 1987-06-30 | 1989-01-26 | Henning J Claassen | Vorrichtung zum auftragen von fluessigen klebstoffen auf ein substrat |
FR2727113B1 (fr) * | 1994-11-17 | 1996-12-27 | Oreal | Nouveaux filtres solaires, compositions cosmetiques photoprotectrices les contenant et utilisations |
CN100368133C (zh) * | 2005-12-19 | 2008-02-13 | 西北工业大学 | 导电杆钎焊方法 |
US8431112B2 (en) | 2007-08-09 | 2013-04-30 | Hallstar Innocations Corp. | Photostabilization of cholecalciferol with alkoxycrylene compounds |
US8070989B2 (en) | 2007-08-09 | 2011-12-06 | Hallstar Innovations Corp. | Photostabilization of retinoids with alkoxycrylene compounds |
US7776614B2 (en) * | 2007-08-09 | 2010-08-17 | Hallstar Innovations Corp. | Test method for determining compounds capable of quenching electronic singlet state excitation of photoactive compounds |
US7588702B2 (en) * | 2007-08-09 | 2009-09-15 | Hallstar Innovations Corp. | Method of quenching electronic excitation of chromophore-containing organic molecules in photoactive compositions |
US8133477B2 (en) * | 2007-08-09 | 2012-03-13 | Hallstar Innovations Corp. | Dispersions of inorganic particulates containing alkoxycrylene |
US8329148B1 (en) | 2007-08-09 | 2012-12-11 | Hallstar Innovations Corp. | Photostabilization of coenzyme Q compounds with alkoxycrylene compounds |
US7754191B2 (en) * | 2007-08-09 | 2010-07-13 | Hallstar Innovations Corp. | Method of quenching electronic excitation of chromophore-containing organic molecules photoactive compositions |
US7597825B2 (en) * | 2007-08-09 | 2009-10-06 | Hallstar Innovations Corp. | Method of quenching electronic excitation of chromophore-containing organic molecules in photoactive compositions |
US8263051B2 (en) | 2007-08-09 | 2012-09-11 | Hallstar Innovations Corp. | Photostabilization of resveratrol with alkoxycrylene compounds |
US20090039322A1 (en) * | 2007-08-09 | 2009-02-12 | Hallstar Innovations Corp. | Alkoxy polyester compounds, compositions and methods of use thereof |
US8257687B2 (en) | 2007-08-09 | 2012-09-04 | Hallstar Innovations Corp. | Photostabilization of coenzyme Q compounds with alkoxycrylene compounds |
WO2009033019A2 (en) * | 2007-09-06 | 2009-03-12 | Hallstar Innovations Corp. | Photostabilizing silicone fluids |
US7964245B2 (en) * | 2008-06-27 | 2011-06-21 | Hallstar Innovations Corp. | UV-absorbing and photostabilizing polymers |
JP5955583B2 (ja) * | 2012-02-24 | 2016-07-20 | 株式会社Adeka | 新規化合物、染料及び着色感光性組成物 |
CN113423671A (zh) | 2019-03-22 | 2021-09-21 | 日本电气硝子株式会社 | Li2O-Al2O3-SiO2系结晶化玻璃 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2775605A (en) * | 1955-06-01 | 1956-12-25 | Rohm & Haas | Organo-silicon compounds and methods for making them |
US2872435A (en) * | 1956-08-15 | 1959-02-03 | Dow Corning | (cyanoalkoxy) alkyl substituted organosilicon compounds |
US4097511A (en) * | 1967-12-20 | 1978-06-27 | General Electric Company | Organofunctional-silicon materials |
US3584026A (en) * | 1968-07-17 | 1971-06-08 | Gen Electric | Cyanoalkoxyalkenyl and aminoalkoxyalkenylsilanes |
US3646091A (en) * | 1969-07-18 | 1972-02-29 | Gen Electric | Cyanoalkyl (organofunctional) silicon compounds |
US3878263A (en) * | 1972-07-10 | 1975-04-15 | Stauffer Chemical Co | Acrylate-functional polysiloxane polymers |
US4051161A (en) * | 1972-09-15 | 1977-09-27 | E. I. Du Pont De Nemours And Company | Ultraviolet screening agents and coating materials containing organosilane ester groups |
US4012402A (en) * | 1974-10-04 | 1977-03-15 | Johnson & Johnson | Modified cyanoacrylate monomers and methods for preparation |
US4122233A (en) * | 1975-05-08 | 1978-10-24 | E. I. Du Pont De Nemours And Company | Ultraviolet screening agents and coating materials containing organosilane ester groups |
US4188451A (en) * | 1978-04-12 | 1980-02-12 | General Electric Company | Polycarbonate article coated with an adherent, durable, silica filled organopolysiloxane coating and process for producing same |
-
1980
- 1980-05-30 US US06/154,626 patent/US4307240A/en not_active Expired - Lifetime
-
1981
- 1981-04-16 CA CA000375664A patent/CA1173454A/en not_active Expired
- 1981-05-20 GB GB8115485A patent/GB2077748B/en not_active Expired
- 1981-05-26 DE DE19813120847 patent/DE3120847A1/de not_active Withdrawn
- 1981-05-27 FR FR8110608A patent/FR2483401A1/fr active Pending
- 1981-05-29 AU AU71188/81A patent/AU7118881A/en not_active Abandoned
- 1981-05-29 KR KR1019810001908A patent/KR840001684B1/ko active IP Right Grant
- 1981-05-29 JP JP8124881A patent/JPS5721392A/ja active Granted
-
1984
- 1984-06-16 KR KR1019840003402A patent/KR840001685B1/ko active IP Right Grant
- 1984-06-16 KR KR1019840003403A patent/KR840001686B1/ko active IP Right Grant
-
1989
- 1989-01-11 JP JP1002954A patent/JPH02182A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
DE3120847A1 (de) | 1982-02-25 |
KR840001685B1 (ko) | 1984-10-15 |
US4307240A (en) | 1981-12-22 |
CA1173454A (en) | 1984-08-28 |
JPS5721392A (en) | 1982-02-04 |
FR2483401A1 (fr) | 1981-12-04 |
KR840001684B1 (ko) | 1984-10-15 |
KR840001686B1 (ko) | 1984-10-15 |
GB2077748A (en) | 1981-12-23 |
JPH0143759B2 (ko) | 1989-09-22 |
AU7118881A (en) | 1981-12-03 |
JPH02182A (ja) | 1990-01-05 |
JPH0314837B2 (ko) | 1991-02-27 |
GB2077748B (en) | 1985-06-26 |
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