KR830004354A - 알킬화 또는 알킬화 전-세라믹(pre-ceramic)중합체에서의 고수율의 실리콘 카바이드 제조방법 - Google Patents
알킬화 또는 알킬화 전-세라믹(pre-ceramic)중합체에서의 고수율의 실리콘 카바이드 제조방법Info
- Publication number
- KR830004354A KR830004354A KR1019800004208A KR800004208A KR830004354A KR 830004354 A KR830004354 A KR 830004354A KR 1019800004208 A KR1019800004208 A KR 1019800004208A KR 800004208 A KR800004208 A KR 800004208A KR 830004354 A KR830004354 A KR 830004354A
- Authority
- KR
- South Korea
- Prior art keywords
- polysilane
- atoms
- alkylated
- mol
- alkyl
- Prior art date
Links
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 title claims 2
- 229910010271 silicon carbide Inorganic materials 0.000 title claims 2
- 239000000919 ceramic Substances 0.000 title 1
- 229920000642 polymer Polymers 0.000 title 1
- 229920000548 poly(silane) polymer Polymers 0.000 claims 12
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 8
- 125000000217 alkyl group Chemical group 0.000 claims 5
- 125000004432 carbon atom Chemical group C* 0.000 claims 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 4
- 238000004519 manufacturing process Methods 0.000 claims 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 1
- 239000007818 Grignard reagent Substances 0.000 claims 1
- -1 aryl Grignard reagent Chemical class 0.000 claims 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 1
- 229910052794 bromium Inorganic materials 0.000 claims 1
- 125000001246 bromo group Chemical group Br* 0.000 claims 1
- 229910010293 ceramic material Inorganic materials 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 229910052736 halogen Inorganic materials 0.000 claims 1
- 150000002367 halogens Chemical group 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/60—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which all the silicon atoms are connected by linkages other than oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/90—Carbides
- C01B32/914—Carbides of single elements
- C01B32/956—Silicon carbide
- C01B32/963—Preparation from compounds containing silicon
- C01B32/977—Preparation from organic compounds containing silicon
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
- C04B35/571—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide obtained from Si-containing polymer precursors or organosilicon monomers
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/6303—Inorganic additives
- C04B35/6316—Binders based on silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5053—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials non-oxide ceramics
- C04B41/5057—Carbides
- C04B41/5059—Silicon carbide
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31551—Of polyamidoester [polyurethane, polyisocyanate, polycarbamate, etc.]
- Y10T428/31609—Particulate metal or metal compound-containing
- Y10T428/31612—As silicone, silane or siloxane
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31678—Of metal
- Y10T428/31714—Next to natural gum, natural oil, rosin, lac or wax
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (3)
- 다음 일반식(Ⅱ)의 폴리실란을 일반식 RngX(여기에서 R은 탄소수 1 내지 4의 알킬 또는 페닐이고 X는 할로겐임)인 알킬 또는 아릴 그리나드 시약과 무수조건하에 0 내지 120℃에서 1 내지 48시간 동안 적합한 용매중에서 반응시킨 후 다음 일반식(I)의 폴리실란을 회수함을 특징으로 하는 다음 일반식(I)의 폴리실란을 제조하는 방법.{(CH3)2Si} {CH3Si} (I)여기에서 폴리실란은 25℃에서 고화되고 0 내지 60몰%의 (CH3)2Si=단위 및 40내지 100몰%의 CH3Si단위를 함유하며 실리콘 원자는 다른 실리콘 원자 및 탄소수 1 내지 4의 알킬 또는 페닐에 결합되어 있다.{(CH3)2Si} {CH3Si} (Ⅱ)여기에서 폴리실란은 25℃에서 고화되고 0 내지 60몰%의 (CH3)2Si=단위 및 400 내지 100몰%의 CH3Si단위를 함유하며 실리콘 원자상의 나머지 결합은 다른 실리콘 원자, 염소원자 또는 브롬원자에 부착되고 있으며 폴리실란 중량 기준으로 10 내지 38%의 가수분해성 염소 또는 폴라실란 중량 기준으로 21내지 58중량%의 가수분해성 브롬이 폴리실란에 함유되어 있다.
- 다음 일반식을 가지며 실온에서 고화되며 폴리실란으로 이루어진 물질의 조성물{(CH3)2Si} {CH3Si}여기에서 폴리실란은 0 내지 60몰%의(CH3)2Si=단위 및 40 내지 100몰%의 CH3Si=단위를 함유하며 실리콘 원자는 다른 실리콘 원자 및 탄소수 1 내지 4의 알킬 또는 페닐에 결합되어 있다.
- 다음 일반식을 가진 폴리실란을 1200℃ 이상으로 가열함을 특징으로 하는 실리콘 카바이드 세라믹물질을 제조하는 방법.{(CH3)2Si} {CH3Si}여기에서 폴리실란은 0 내지 60몰%의 (CH3)2Si단위 및 40 내지 100몰%의 CH3Si단위를 함유하며 실리콘 원자는 다른 실리콘 원자 및 탄소수 1 내지 4의 알킬 또는 페닐에 결합되어 있다.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US06/171,557 US4298559A (en) | 1980-07-23 | 1980-07-23 | High yield silicon carbide from alkylated or arylated pre-ceramic polymers |
US171,557 | 1980-07-23 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR830004354A true KR830004354A (ko) | 1983-07-09 |
KR840001536B1 KR840001536B1 (ko) | 1984-10-04 |
Family
ID=22624196
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019800004208A KR840001536B1 (ko) | 1980-07-23 | 1980-11-03 | 폴리실란의 제조방법 |
Country Status (13)
Country | Link |
---|---|
US (1) | US4298559A (ko) |
JP (1) | JPS5734132A (ko) |
KR (1) | KR840001536B1 (ko) |
AU (1) | AU537992B2 (ko) |
BE (1) | BE886611A (ko) |
CA (1) | CA1151197A (ko) |
CH (1) | CH648322A5 (ko) |
DE (1) | DE3041758C2 (ko) |
FR (1) | FR2487367A1 (ko) |
GB (1) | GB2081290B (ko) |
IT (1) | IT1168078B (ko) |
NL (1) | NL8005963A (ko) |
SE (1) | SE446871B (ko) |
Families Citing this family (44)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4534948A (en) * | 1980-03-31 | 1985-08-13 | Dow Corning Corporation | Method for preparing silicon carbide |
JPS5939708A (ja) * | 1982-08-25 | 1984-03-05 | Shin Etsu Chem Co Ltd | 炭化けい素微粉末の製造方法 |
US4446169A (en) * | 1982-09-16 | 1984-05-01 | Westinghouse Electric Corp. | Method for making silicon carbide coatings |
US4783516A (en) * | 1983-03-31 | 1988-11-08 | Union Carbide Corporation | Polysilane precursors containing olefinic groups for silicon carbide |
JPS60179356A (ja) * | 1984-02-28 | 1985-09-13 | Yazaki Corp | 自動車のワイヤリングシステム |
US4546163A (en) * | 1984-09-04 | 1985-10-08 | Dow Corning Corporation | Silicon carbide preceramic vinyl-containing polymers |
US4595472A (en) * | 1984-09-04 | 1986-06-17 | Dow Corning Corporation | Silicon carbide preceramic vinyl-containing polymers |
US4681860A (en) * | 1984-12-04 | 1987-07-21 | Dow Corning Corporation | Ceramic materials from polycarbosilanes |
DE3503763A1 (de) * | 1985-02-05 | 1986-08-07 | Fritz Studer Ag, Thun | Verfahren zum herstellen von gegenstaenden, insbesondere von maschinenteilen aus polymerbeton sowie maschinenteile aus polymerbeton |
US4687657A (en) * | 1986-06-09 | 1987-08-18 | Celanese Corporation | Fabrication of SiC - AlN alloys |
JPH064699B2 (ja) * | 1986-07-04 | 1994-01-19 | 有機合成薬品工業株式会社 | 1,2,2−トリメチル−1−フエニルポリジシランおよびその製造方法 |
US4767728A (en) * | 1986-07-30 | 1988-08-30 | The United States Of America As Represented By The United States National Aeronautics And Space Administration | Boron-containing organosilane polymers and ceramic materials thereof |
GB8629593D0 (en) * | 1986-12-11 | 1987-01-21 | Dow Corning Ltd | Polysilanes |
US4962175A (en) * | 1986-12-22 | 1990-10-09 | Dow Corning Corporation | Alkylpoly (polysilyl) azane preceramic polymers |
US4962176A (en) * | 1986-12-22 | 1990-10-09 | Dow Corning Corporation | Polysilane preceramic polymers |
AU618233B2 (en) * | 1986-12-24 | 1991-12-19 | Dow Corning Corporation | Derivatized alkylpolysilane preceramic polymers |
US4818732A (en) * | 1987-03-19 | 1989-04-04 | The Standard Oil Company | High surface area ceramics prepared from organosilane gels |
US4810443A (en) * | 1987-07-02 | 1989-03-07 | Dow Corning Coporation | Method for forming filaments from a resin |
US4806612A (en) * | 1987-08-10 | 1989-02-21 | Dow Corning Corporation | Preceramic acetylenic polysilanes |
US4761458A (en) * | 1987-08-17 | 1988-08-02 | Dow Corning Corporation | Preceramic polycarbosilane derivatives |
US4824918A (en) * | 1987-09-04 | 1989-04-25 | Dow Corning Corporation | Method of producing silicon carbide preceramic vinyl-containing polymers |
US4889899A (en) * | 1987-09-08 | 1989-12-26 | Dow Corning Corporation | Method of producing silicon carbide preceramic vinyl-containing polymers |
US4921917A (en) * | 1987-10-01 | 1990-05-01 | Dow Corning Corporation | Pre-ceramic methylpolysilanes |
US4889904A (en) * | 1988-07-22 | 1989-12-26 | Dow Corning Corporation | Process for the preparation of methylpolysilanes having controlled carbon content |
US5023307A (en) * | 1988-07-22 | 1991-06-11 | Dow Corning Corporation | Methylpolysilanes having controllable rheology and method for their preparation |
US4906710A (en) * | 1988-10-31 | 1990-03-06 | Dow Corning Corporation | Preceramic metallopolysilanes |
US4945072A (en) * | 1988-10-31 | 1990-07-31 | Dow Corning Corporation | Preceramic metallopolysilanes |
US5545687A (en) * | 1990-02-21 | 1996-08-13 | Dow Corning Corporation | Preparation of high density boron carbide ceramics with preceramic polymer binders |
US5051215A (en) * | 1990-03-21 | 1991-09-24 | Dow Corning Corporation | Curing preceramic polymers by exposure to nitrogen dioxide |
US5268336A (en) * | 1990-06-18 | 1993-12-07 | Dow Corning Corporation | Preparation of substantially polycrystalline silicon carbide fibers from methylpolydisilylazanes |
US6146559A (en) | 1994-07-28 | 2000-11-14 | Dow Corning Corporation | Preparation of high density titanium diboride ceramics with preceramic polymer binders |
US5449646A (en) | 1994-07-29 | 1995-09-12 | Dow Corning Corporation | Preparation of high density zirconium diboride ceramics with preceramic polymer binders |
US5447893A (en) | 1994-08-01 | 1995-09-05 | Dow Corning Corporation | Preparation of high density titanium carbide ceramics with preceramic polymer binders |
BRPI0306736B8 (pt) * | 2002-01-21 | 2021-05-25 | Akzo Nobel Nv | processo para a preparação de 7alfa-metilesteróides, e, composto |
DE102008064372A1 (de) | 2008-12-22 | 2010-06-24 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Polysilan-Polycarbosilane mit reduziertem Chlorgehalt auf Basis von Methylchlorpolysilanen sowie daraus hergestellte Spinnmassen und keramische Formkörper |
US9045347B2 (en) * | 2010-02-26 | 2015-06-02 | General Electric Company | Stiochiometric silicon carbide fibers from thermo-chemically cured polysilazanes |
JP5571992B2 (ja) * | 2010-03-30 | 2014-08-13 | 大阪ガスケミカル株式会社 | ポリシランの製造方法 |
JP5595083B2 (ja) * | 2010-03-30 | 2014-09-24 | 大阪ガスケミカル株式会社 | 末端封鎖されたネットワーク状ポリシラン |
US8697901B2 (en) | 2011-12-30 | 2014-04-15 | Momentive Performance Materials Inc. | Synthesis of organohalosilane monomers via enhanced cleavage of direct process residue |
US8637695B2 (en) | 2011-12-30 | 2014-01-28 | Momentive Performance Materials Inc. | Synthesis of organohalosilane monomers from conventionally uncleavable Direct Process Residue |
WO2014014542A2 (en) | 2012-04-27 | 2014-01-23 | Burning Bush Group | High performance silicon based coating compositions |
US10138381B2 (en) | 2012-05-10 | 2018-11-27 | Burning Bush Group, Llc | High performance silicon based thermal coating compositions |
CN104812543B (zh) | 2012-07-03 | 2017-06-13 | 伯宁布什集团有限公司 | 硅基高性能涂料组合物 |
US9006355B1 (en) | 2013-10-04 | 2015-04-14 | Burning Bush Group, Llc | High performance silicon-based compositions |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2218960A1 (de) * | 1972-04-19 | 1973-11-08 | Bayer Ag | Formkoerper aus mogenen mischungen von siliciumcarbid und siliciumnitrid und verfahren zu ihrer erstellung |
JPS51126300A (en) * | 1975-04-26 | 1976-11-04 | Res Inst Iron Steel Tohoku Univ | Method for manufacturing an organoo silicon polymer having silicon and carbon atoms as main skeleton component |
GB1590011A (en) * | 1976-08-17 | 1981-05-28 | Kyoto Ceramic | Method of producing dense sintered silicon carbide body from polycarbosilane |
CA1121971A (en) * | 1978-05-30 | 1982-04-20 | Dow Corning Corporation | Method for preparing silicon carbide |
-
1980
- 1980-07-23 US US06/171,557 patent/US4298559A/en not_active Expired - Lifetime
- 1980-10-17 CA CA000362697A patent/CA1151197A/en not_active Expired
- 1980-10-27 AU AU63733/80A patent/AU537992B2/en not_active Ceased
- 1980-10-29 GB GB8034800A patent/GB2081290B/en not_active Expired
- 1980-10-30 NL NL8005963A patent/NL8005963A/nl not_active Application Discontinuation
- 1980-11-03 KR KR1019800004208A patent/KR840001536B1/ko active
- 1980-11-05 DE DE3041758A patent/DE3041758C2/de not_active Expired
- 1980-11-27 JP JP16733480A patent/JPS5734132A/ja active Granted
- 1980-12-08 FR FR8026009A patent/FR2487367A1/fr active Granted
- 1980-12-11 BE BE0/203134A patent/BE886611A/fr not_active IP Right Cessation
-
1981
- 1981-02-26 IT IT20021/81A patent/IT1168078B/it active
- 1981-07-22 SE SE8104494A patent/SE446871B/sv not_active IP Right Cessation
- 1981-07-22 CH CH4789/81A patent/CH648322A5/de not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE3041758A1 (de) | 1982-02-11 |
AU537992B2 (en) | 1984-07-26 |
SE8104494L (sv) | 1982-01-24 |
NL8005963A (nl) | 1982-02-16 |
SE446871B (sv) | 1986-10-13 |
JPS623112B2 (ko) | 1987-01-23 |
GB2081290B (en) | 1984-12-12 |
FR2487367A1 (fr) | 1982-01-29 |
CH648322A5 (de) | 1985-03-15 |
IT8120021A0 (it) | 1981-02-26 |
BE886611A (fr) | 1981-06-11 |
JPS5734132A (en) | 1982-02-24 |
IT1168078B (it) | 1987-05-20 |
GB2081290A (en) | 1982-02-17 |
CA1151197A (en) | 1983-08-02 |
AU6373380A (en) | 1982-01-28 |
KR840001536B1 (ko) | 1984-10-04 |
FR2487367B1 (ko) | 1983-12-30 |
US4298559A (en) | 1981-11-03 |
DE3041758C2 (de) | 1985-07-11 |
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