KR20240087737A - 플루오렌온의 제조 방법 - Google Patents

플루오렌온의 제조 방법 Download PDF

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Publication number
KR20240087737A
KR20240087737A KR1020247009828A KR20247009828A KR20240087737A KR 20240087737 A KR20240087737 A KR 20240087737A KR 1020247009828 A KR1020247009828 A KR 1020247009828A KR 20247009828 A KR20247009828 A KR 20247009828A KR 20240087737 A KR20240087737 A KR 20240087737A
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KR
South Korea
Prior art keywords
fluorenone
mass
phosphoric acid
distillation
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
KR1020247009828A
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English (en)
Korean (ko)
Inventor
히로키 스미
유키 와타나베
히데아키 후지타
고 나카무라
다쓰유키 구마노
Original Assignee
미쯔비시 가스 케미칼 컴파니, 인코포레이티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 미쯔비시 가스 케미칼 컴파니, 인코포레이티드 filed Critical 미쯔비시 가스 케미칼 컴파니, 인코포레이티드
Publication of KR20240087737A publication Critical patent/KR20240087737A/ko
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/36—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in compounds containing six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06—Halogens; Compounds thereof
    • B01J27/128—Halogens; Compounds thereof with iron group metals or platinum group metals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/783—Separation; Purification; Stabilisation; Use of additives by gas-liquid treatment, e.g. by gas-liquid absorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/85—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/657—Unsaturated compounds containing a keto groups being part of a ring containing six-membered aromatic rings
    • C07C49/665—Unsaturated compounds containing a keto groups being part of a ring containing six-membered aromatic rings a keto group being part of a condensed ring system
    • C07C49/675—Unsaturated compounds containing a keto groups being part of a ring containing six-membered aromatic rings a keto group being part of a condensed ring system having three rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B61/00—Other general methods
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
    • C07C2603/06—Ortho- or ortho- and peri-condensed systems containing three rings containing at least one ring with less than six ring members
    • C07C2603/10—Ortho- or ortho- and peri-condensed systems containing three rings containing at least one ring with less than six ring members containing five-membered rings
    • C07C2603/12—Ortho- or ortho- and peri-condensed systems containing three rings containing at least one ring with less than six ring members containing five-membered rings only one five-membered ring
    • C07C2603/18—Fluorenes; Hydrogenated fluorenes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
KR1020247009828A 2021-10-01 2022-09-29 플루오렌온의 제조 방법 Pending KR20240087737A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JPJP-P-2021-162749 2021-10-01
JP2021162749 2021-10-01
PCT/JP2022/036595 WO2023054644A1 (ja) 2021-10-01 2022-09-29 フルオレノンの製造方法

Publications (1)

Publication Number Publication Date
KR20240087737A true KR20240087737A (ko) 2024-06-19

Family

ID=85782932

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020247009828A Pending KR20240087737A (ko) 2021-10-01 2022-09-29 플루오렌온의 제조 방법

Country Status (6)

Country Link
US (1) US20250129005A1 (https=)
EP (1) EP4410769A4 (https=)
JP (1) JPWO2023054644A1 (https=)
KR (1) KR20240087737A (https=)
CN (1) CN118043300A (https=)
WO (1) WO2023054644A1 (https=)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3038940A (en) 1958-04-25 1962-06-12 Standard Oil Co Process for preparation of aromatic ketones
US3875237A (en) 1974-03-21 1975-04-01 Gen Electric Preparation of fluorenone
JP2004115390A (ja) 2002-09-24 2004-04-15 Osaka Gas Co Ltd 高純度フルオレノン及びその製造方法
JP2007182399A (ja) 2006-01-06 2007-07-19 Air Water Inc フルオレノン類の製造方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1095348A (fr) * 1954-11-26 1955-06-01 Inst Francais Du Petrole Procédé de fabrication de cétones bicycliques
GB1275771A (en) * 1968-07-15 1972-05-24 Ashland Oil Inc Liquid phase oxidation of condensed ring aromatic hydrocarbons
US4297514A (en) * 1978-12-26 1981-10-27 The Dow Chemical Company Method of oxidizing compounds having activated methylene radicals
DE3207572A1 (de) * 1981-04-22 1982-11-11 Rütgerswerke AG, 6000 Frankfurt Verfahren zur oxidation von reaktiven aromaten
US5545760A (en) * 1995-02-07 1996-08-13 The Dow Chemical Company Process for making fluorenones
CA2253746A1 (en) * 1996-05-24 1997-12-04 The Dow Chemical Company Process for making fluorenones
JP4039730B2 (ja) * 1998-02-18 2008-01-30 ダイセル化学工業株式会社 酸化触媒系及びそれを用いた酸化方法
JP2001288122A (ja) * 2000-04-04 2001-10-16 Daicel Chem Ind Ltd 反応生成物と触媒との分離方法
JP4095281B2 (ja) * 2001-11-19 2008-06-04 ダイセル化学工業株式会社 有機化合物製造用触媒、及びこの触媒を用いた有機化合物の製造法
CN106977378A (zh) * 2017-04-12 2017-07-25 大连理工大学 一种芴催化氧化制备9‑芴酮的方法
US12545633B2 (en) * 2020-10-23 2026-02-10 Mitsubishi Gas Chemical Company, Inc. Method for producing fluorenone

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3038940A (en) 1958-04-25 1962-06-12 Standard Oil Co Process for preparation of aromatic ketones
US3875237A (en) 1974-03-21 1975-04-01 Gen Electric Preparation of fluorenone
JP2004115390A (ja) 2002-09-24 2004-04-15 Osaka Gas Co Ltd 高純度フルオレノン及びその製造方法
JP2007182399A (ja) 2006-01-06 2007-07-19 Air Water Inc フルオレノン類の製造方法

Also Published As

Publication number Publication date
US20250129005A1 (en) 2025-04-24
TW202323233A (zh) 2023-06-16
CN118043300A (zh) 2024-05-14
EP4410769A1 (en) 2024-08-07
WO2023054644A1 (ja) 2023-04-06
JPWO2023054644A1 (https=) 2023-04-06
EP4410769A4 (en) 2025-06-04

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