KR20170103390A - Unpoisonous anticeptic composition comprising mineral ion activated water - Google Patents

Unpoisonous anticeptic composition comprising mineral ion activated water Download PDF

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KR20170103390A
KR20170103390A KR1020160026226A KR20160026226A KR20170103390A KR 20170103390 A KR20170103390 A KR 20170103390A KR 1020160026226 A KR1020160026226 A KR 1020160026226A KR 20160026226 A KR20160026226 A KR 20160026226A KR 20170103390 A KR20170103390 A KR 20170103390A
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water
mineral ion
hydrogen
mineral
toxic
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박혜정
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주식회사 블루텍
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06Aluminium; Calcium; Magnesium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]

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  • Agronomy & Crop Science (AREA)
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  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
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  • Inorganic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a non-toxic preservative composition which exhibits a preservative effect in cosmetics and sanitary goods by utilizing mineral ion water including mineral ion water having excellent sterilizing properties including metal ions and hydrogen-reduced water enriched with hydrogen, And 5 to 99% by volume of an ionic active water, wherein the mineral ion active water comprises mineral ion water including metal ions and exhibiting excellent sterilizing properties; And hydrogen-enriched hydrogen-containing water, wherein mineral ion water: hydrogen-reduced water is mixed in a volume ratio of 1: 0.5 to 1.5.

Description

[0001] The present invention relates to a non-toxic antiseptic composition comprising mineral ion activated water,

The present invention relates to a non-toxic antiseptic composition comprising mineral ion active water. More particularly, the present invention relates to a non-toxic antimicrobial composition comprising mineral ion active water and mineral water containing mineral ion water and hydrogen- The present invention relates to a non-toxic preservative composition exhibiting a preservative effect in articles and the like.

The biggest problem in the existing cosmetics business is the use of preservatives due to the use of natural ingredients, which may be a skin problem. The development of preservatives that do not cause skin troubles or the problem of cosmetic effects and skin troubles at the same time as a chemical synthetic ingredient that does not become a decay will be the core of cosmetic development.

Among the disinfection and sterilization methods currently used in everyday life, in addition to the physical methods using heat and radiation, chemical methods such as alcohols, phenols, halogen compounds, quaternary ammonium (quaternary ammonium salts, biguanide-based chemicals, and aldehydes. However, there is no satisfactory condition that the sterilizing effect is high, safe, low toxicity, excellent in stability and preservability, and low in cost. For example, the Bibguanide chemical name, Hibitane, is the best selling disinfectant sold, but it has no effect on spores. It has also been found that some bacteria have strong resistance, which is known to be the cause of infection in hospitals. Antibiotics are strongly resistant to chemically synthesized drugs that, for example, do not need to look at bacterial bodies, either by production of enzymes to eliminate rejection reactions or by production of alternative enzymes. This threatens humanity and is reappearing.

It has already been known that some metal ions exhibit a sterilizing action at a certain concentration or more and have been applied to mercury chemicals and the like. However, since mercury is heavy metal which is absolutely unnecessary for living organisms and is toxic, as described above, the development of various disinfecting drugs has made it impossible to use them as disinfectants, and thereafter, almost no disinfectant containing metal ions has been found. In recent years, however, metal elements have been recognized as essential materials of living organisms and have been developed as poison drugs and alchemy. In recent years, there has been no recognition as environmental pollutants, and one of the important factors that actively protect human health And supermarkets such as supermarkets in the US have tablets containing various kinds of minerals and metal elements together with foodstuffs.

Korean Unexamined Patent Publication No. 2000-0017001 discloses a sterilizing liquid containing at least one or more kinds of ferric ion, sorbic acid, benzoic acid and p-oxybenzoic acid ester, trivalent iron ion and L-ascorbic acid A sterilizing liquid containing at least one or more kinds of acid, sorbic acid, benzoic acid and p-oxybenzoic acid ester, and a sterilizing liquid containing trivalent iron, sorbic acid, benzoic acid and L-ascorbic acid, Discloses an invention relating to "iron ion-containing sterilizing liquid" for sterilizing pathogens in a short time.

On the other hand, there is an oxidation-reduction potential as an index for judging the redox potential of water. It is known that water (aqueous solution) in which the redox potential exhibits a negative value is referred to as reducing water and has a reducing property. Generally, the oxidation-reduction potential of tap water is from +500 to +750 mV, and from well water or commercially available mineral water is 0 to +500 mV. Reduced water having a negative oxidation-reduction potential has an effect of inhibiting oxidation of metals and corruption of foods. When ingested with drinking water, active oxygen in the body, which is a cause of aging and disease, is removed, and pollen allergy, Allergic diseases such as asthma, digestive system diseases such as gastrointestinal disorders, and health disorders such as hypertension. Here, most of the reduced water is generated by electrolysis. As a result, water having a high active hydrogen concentration on the cathode side is taken out as reduced water (see, for example, Japanese Patent Application Laid-Open No. 2002-254078), taking advantage of the property that hydrogen molecules gather on the cathode side by electrolysis of water. The reduced water obtained by the electrolytic method is called "electrolytic reduced water" or "alkaline reduced water" since the water on the cathode side is alkalized by distinguishing it from natural water having a reducing ability. On the other hand, there is known a method of removing dissolved oxygen in water by blowing activated hydrogen gas into water, instead of electrolyzing water (for example, Japanese Patent Application Laid-Open No. 8-276104). It is also known to increase the dissolved hydrogen concentration of water in the water tank by passing hydrogen gas through the water in the water tank (for example, Japanese Patent Laid-Open No. 2002-172317). However, as disclosed in Japanese Patent Application Laid-Open No. 2002-254078, the reduced water (electrolytic reduced water) obtained by electrolysis of water exhibits alkalinity, and as the minus value of the oxidation-reduction potential increases, the pH value showing alkalinity becomes higher. When it is appropriately suppressed to about 9 to 10, there is a problem that the redox potential becomes about 150 mV and the reducing property is lowered. On the other hand, as shown in Japanese Patent Application Laid-Open Nos. 8-276104 and 2002-172317, even if the hydrogen gas is blown into water, the redox potential becomes negative. However, Ring system), it is difficult to dissolve a large amount of hydrogen gas because the hydrogen gas does not dissolve only in the portion in contact with water. Moreover, it is difficult to recover the hydrogen gas that has reached the water surface without dissolving in water, Since most of the hydrogen gas is released into the atmosphere, a large amount of hydrogen gas is required in the dissolving treatment and the cost is also increased. In addition, the active hydrogen which is a source of reductivity is very unstable, and when it is left untreated, it is released into the atmosphere to change the redox potential of water in the positive direction, and the reductant is lost when reaching the hands of consumers there was.

Accordingly, there is still a demand and a demand for development of a non-toxic preservative composition that exhibits a harmless, non-toxic, highly sterilizing, preservative and odor-removing effect on the human body and can be used in cosmetics and sanitary articles.

In terms of marketing, Chinese and Southeast Asian countries, which are developing countries, are developing their economies and increasing their interest in hygiene, and the demand for Korean beauty and hygiene products is increasing due to the influence of Chinese tourists such as Yuccar and Korean Wave.

The present invention relates to a method for producing a cosmetic or sanitary product which uses a mineral ion active water containing metal ion harmless to the human body by electrolysis and containing hydrogen ionized water that enriched hydrogen mineral water and mineral ion water exhibiting excellent sterilizing properties, It is an object of the present invention to provide a non-toxic preservative composition.

The non-toxic preservative composition containing the mineral ion active water of the present invention comprises 5 to 99% by volume of mineral ion active water, wherein the mineral ion active water comprises mineral ion water including metal ions and exhibiting excellent sterilizing properties; And hydrogen-enriched hydrogen-containing water, wherein mineral ion water: hydrogen-reduced water is mixed in a volume ratio of 1: 0.5 to 1.5.

The mineral ionized water includes metal ions ionized by electrolysis of iron, copper, zinc, silver, aluminum, and two or more of them, and may have an oxidation-reduction potential (ORP) of -100 to -500 있다 .

The mineral ionized water may be one obtained by ionizing iron, copper, zinc, silver, aluminum and two or more of these alloys through electrolysis under a high voltage of 10,000 to 50,000V.

The hydrogen-reduced water may be one in which hydrogen gas is enriched in water by pressurizing hydrogen gas at a temperature within a range of 5 to 15 ° C at a pressure of 2 to 10 atm for 10 to 60 minutes.

The non-toxic preservative composition containing the mineral ion active water may further comprise a hardwood extract.

The above-mentioned Heliothis extract may be obtained by immersing the stem or root of the bracken tree so as to be immersed in a polar solvent, immersing in a temperature range of 10 to 40 ° C for 12 to 240 hours, and then removing the solid content by filtration.

The polar solvent may be selected from the group consisting of water, methanol, ethanol, hexane, methylene chloride, ethyl acetate, butanol, propylene glycol, butylene glycol, dipropylene glycol, glycerin and mixtures of two or more thereof, Water or ethanol.

According to the present invention, by utilizing mineral ion water containing mineral ions harmless to human body by electrolysis and having hydrogen ion-enriched mineral ion water which exhibits excellent sterilizing property, the cosmetic and sanitary products provide a preservative effect To provide a non-toxic antiseptic composition, and to provide cosmetic and sanitary products containing the same.

Figs. 1A and 1B are test results of an Escherichia coli sterilization effect test.
Figures 2a and 2b are test results of the antiseptic effect against P. aeruginosa.
FIGS. 3A and 3B are test results of sterilization effect of Salmonella.
4A and 4B are test results of sterilization effect of pneumococci.
5 is a test report on deodorizing effect on ammonia.
6 is a test report on deodorizing effect on hydrogen sulfide.
7 shows a deodorizing effect test report on methyl mercaptan.
Fig. 8 shows a deodorizing effect test report on trimethylamine.

Hereinafter, specific embodiments of the present invention will be described in detail with reference to the accompanying drawings.

The non-toxic preservative composition containing mineral ion active water according to the present invention comprises 5 to 99% by volume of mineral ion active water, wherein the mineral ion active water comprises mineral ion water including metal ions and exhibiting excellent sterilizing properties; And hydrogen-enriched hydrogen-containing water, wherein mineral ion water: hydrogen-reduced water is mixed in a volume ratio of 1: 0.5 to 1.5. That is, according to the present invention, at the time when it is necessary to develop a substance having an effect as a non-toxic preservative that can substitute for a chemical preservative which is a main cause of existing skin troubles, mineral ion active water has no toxicity, does not cause skin trouble, It acts as a preservative with its germicidal effect. It is a reductant against reactive oxygen species. It is characterized by its strong antioxidant action, which is suitable for use as a cosmetic raw material to prevent skin aging and protect skin.

Most of the oxygen that comes into our body is reduced to water through the energy metabolism of the cell, and some (2-3%) is caused by the partial change of the incompletely burned oxygen. Active oxygen in our body is produced every day, and active oxygen which is beneficial in our body protects body by killing bacteria, fungi and virus in body and contributes to synthesis of energy source and various hormones, but harmful active oxygen is normal It is known to attack cells to destroy or deform cells and cause problems such as inflammation, aging, DNA damage, protein denaturation, lipid peroxidation and blood fluidity deterioration. In particular, hydroxyl radicals, which are the most toxic among active oxygen species, are regarded as the most toxic active oxygen because they do not have enzymes that are eliminated in the human body. However, hydrogen selectively binds only with the most harmful hydroxyl radicals, A team of Professor Shigeo Ota of the Japan Medical University announced that a non-toxic preservative composition comprising mineral ion active water according to the present invention comprises a mineral ion active water and the mineral ion active water comprises mineral ion water and hydrogen reduced water And thus hydrogen in the hydrogen-reduced water is particularly effective for the removal of active oxygen species, particularly hydroxyl radicals.

The mineral ion active water newly developed by the present inventor was found to be highly effective in deodorizing as a result of a request to KTR (Korea Chemical Fusion Test Institute). In addition, It is anticipated that it will be possible to develop breakthrough functional products when it is used as a raw material for cosmetics.

When the mineral ion active water is contained in an amount of less than 5% by volume, the desired sterilization and deodorizing effect may be insufficient. On the contrary, when the amount is more than 99% by volume, it is difficult to formulate into cosmetics or the like Can be.

The mineral ionized water includes metal ions ionized by electrolysis of iron, copper, zinc, silver, aluminum, and two or more of them, and may have an oxidation-reduction potential (ORP) of -100 to -500 있다 . Such mineral ionic water may be used for the production of iron, copper, zinc, silver, aluminum and alloys of two or more thereof at a high voltage of 10,000 to 50,000 V, preferably 20,000 to 40,000 V, more preferably 25,000 to 35,000 V, Lt; RTI ID = 0.0 > electrolysis < / RTI > Specifically, for example, the above-mentioned mineral ion water may be sterilized using, for example, a sterilization water producing apparatus which is the same and / or similar to the apparatus for producing livestock sterilization water described in Korean Patent No. 1559360, which is patented and registered by the present applicant The electrode plate may be made of iron, copper, zinc, silver, aluminum, and alloys of two or more thereof, and may be manufactured by performing electrolysis by applying a high voltage of 10,000 to 50,000 V. When the voltage applied for electrolysis in the electrolysis is less than 10,000 V, there is a problem that the minerals content in the obtained mineral ion water, that is, the metal ion content is too small, On the other hand, if the voltage is higher than 50,000 V, it is difficult to control the voltage rise and the proper electrolysis in practice.

The hydrogen-reduced water may be one in which hydrogen gas is enriched in water by pressurizing hydrogen gas at a pressure of 2 to 10 atm for 10 to 60 minutes to purified water at a temperature within a range of 5 to 15 ° C, but the present invention is not limited thereto It should be understood that hydrogen enrichment can also be used for commercial applications.

The mixing ratio of the mineral ionized water and the hydrogenated water is preferably within a range of 0.5 to 1.5 based on the volume of the mineral ionized water. In the sterilization and deodorization of the mineral ion activated water obtained by combining the mineralized ionized water and the hydrogenated water within this range Synergy can be optimized.

The non-toxic preservative composition containing the mineral ion active water may further comprise a hardwood extract. The above-mentioned Heliothis extract may be obtained by immersing the stem or root of the bracken tree so as to be immersed in a polar solvent, immersing in a temperature range of 10 to 40 ° C for 12 to 240 hours, and then removing the solid content by filtration. The polar solvent for extraction may be selected from the group consisting of water, methanol, ethanol, hexane, methylene chloride, ethyl acetate, butanol, propylene glycol, butylene glycol, dipropylene glycol, glycerin, , It is preferable to use ethanol or water. The extraction condition is a moderate extraction condition, and a large amount of the extract can be efficiently obtained while containing a large amount of active active ingredient of spikelets. More specifically, in order to obtain the extracts of Pinus rigicum, 5-fold purified water was added to 1 kg of the intertwined herbaceous stem samples and allowed to stand at room temperature (about 25 캜) for 200 hours, followed by filtration to remove solid components, and then lyophilized using a rotary vacuum evaporator (4.23 g in terms of dry weight). When the extract is used as an extract of barley, the lyophilized product is dissolved by using 10 times of distilled water. It is to be understood that it is not intended to be limited thereto and that it is also possible to use an extract of Helicobacter pylori obtained in other solvents, other temperature conditions, and the like.

Abelophyllum (Scientific name: Abeliophyllum distichum ) is a shrub of aspens and shrubs, which are similar to the shape of a fruit and called as a spike tree. It is a Korean specialty plant that grows only in Korea. A study on the microbial tree has been carried out by Hirobumi et al., "Production of cornoside in Abelophyllum distichum cell suspension cultures" (Phytochemistry. Vol. 48, No. 2, pp. 273-277, &Quot; Four glycosides from the leaves of Abelophyllum distichum with inhibitory effects on angiotensin converting enzyme "(Phytother. Res., 17, 811 (Korean Patent No. 706,131) and "Anti-inflammatory Agent Containing Leaf Tree Extract" (Korea Patent No. 656,287 However, research on its components and physiological activity has not yet been carried out, and researches on cosmetic, skin and skin diseases have not yet been conducted.

The skin of a person changes with age, which is called aging of the skin. The causes of various skin aging may be ultraviolet rays, mental stress, skin diseases caused by germs, external stimuli, etc. However, the most important cause is active oxygen species, and reactive oxygen species are called skin cells and tissues Which promotes skin aging. Specifically, it is known that lipid, fat, protein, DNA, RNA, etc., which constitute the skin, are oxidized and destroyed, resulting in aging of skin cells and tissues. Based on the mineryl ion active water (i.e., a mixture of mineral ion water and hydrogen reduced water) according to the present invention having a strong antioxidant and a reducing ability in order to solve active oxygen species which is the main cause of skin damage and aging, It is possible to manufacture cosmetics raw materials that are competitive and effective globally by blending the extract of Spruce tree. Mineral ionic active water combined with mineral ionized water and hydrogenated water showed antioxidative effect to remove active oxygen species and showed strong sterilizing power and proved to be a bad odor removing effect. Anti-inflammatory, anti-inflammatory, anti-inflammatory, anti-inflammatory, anti-inflammatory, skin wrinkle-improving, whitening, moisturizing and anti-cancer effects. Especially, it is expected that it can be suitably commercialized especially for products applied to human body such as cosmetics.

The extract can be mixed with the non-toxic preservative composition containing the mineral ion active water according to the present invention at an arbitrary ratio. In particular, cosmetics containing the non-toxic preservative composition containing the mineral ion active water according to the present invention And may be mixed at an appropriate ratio depending on the application. Preferably, the mineral ion active water: extract of barley is mixed in a volume ratio of 100: 0.1 to 30.

The non-toxic preservative composition comprising the mineral ion active water according to the present invention may be prepared into various cosmetic formulations, which may or may not contain a vinegar extract.

The cosmetic formulation may be, for example, a mask pack or a vaginal detergent, but the invention is not intended to be limited thereto.

The mask pack is used for the purpose of moisturizing the skin, dissipating heat, and sedating the skin. However, since the cosmetic ingredient contained in the mask pack is vulnerable to corruption, the preservative ingredient must be used and the problem of skin trouble caused by the mask pack must be solved . If an economical and effective non-toxic preservative that does not cause skin troubles is developed, a mask pack intended for the treatment of skin diseases beyond the scope of cosmetics can be released. Accordingly, a non-toxic preservative composition containing mineral ion active water It is suitable for manufacturing. More specifically, the mask pack according to the present invention may be a product having enhanced adhesion and moisturizing property by blending with a conventional cosmetic raw material, ubiquinone, based on a mixture of mineral ion active water and an extract of Liliaceae. The mask pack may contain mineral ion activated water according to the present invention. For example, the mask pack may include a packaged nonwoven fabric and a composition for cosmetics impregnated in the packed nonwoven fabric. The packed nonwoven fabric may be formed, for example, in the form of a sheet without weaving cellulose, , And is a material suitable for the cosmetic composition to be delivered to the skin when a mask pack is applied to the skin by impregnating a cosmetic composition in a liquid state, a semi-solid state (gel state), and / And may be made of synthetic fibers such as cotton, viscose rayon, nylon and the like. Preferably, it may be formed to have various shapes and various incisions, have. The cosmetic composition may further comprise, in addition to the mineral ion active water according to the present invention, a gelled composition; Beauty agent; additive; And water; for example, the gelling composition may comprise carrageenan, glucomannan, and locust bean gum and calcium chloride, and the cosmetic agent may include one or more of a moisturizer, a nutrient, an emulsifier, and a conditioning agent And the additive may include one or more of preservatives, flavors, pigments, vitamins, thickeners, and stabilizers, all of which may be understood to be well known in the art of business. The herb extract may also contain extracts derived from natural products which can improve the feeling of use. Examples of herbal extracts include chamomile, calendula, cornflower, and the like. However, the present invention is not intended to be limited thereto, and it should be understood that the herb extract is representative of various herbs and herbal ingredients.

In particular, ubiquinone is a naturally occurring component commonly referred to as coenzyme Q10. Coenzyme Q10 means 2,3-dimethoxy-5-methyl-6-polyphenyl-1,4-benzoquinone in which the number of isoprene units in the side chain is 10 and is ubiquinone specific to human. This coenzyme Q10 is described as "ubidecarenone" in the Japanese Pharmacopoeia, "Coenzyme Q10" as a food additive, and "ubiquinone" as a cosmetic raw material. Ubiquinone is an essential coenzyme for energy production in mitochondria. In addition, ubiquinone is an important substance in vivo as an antioxidant, and since ubiquinone improves cell metabolism, its efficacy against heart disease, hypertension and rheumatic valve disease has been confirmed. It is also known that it has an effect of improving skin roughness as a cosmetic.

As the secretions are increased in the post-menstruation period of women, a vaginal detergent (such as zinobetadine) used as an inflammation and odor problem due to the infection of germs is problematic for sensitive skin due to the influence of hydrochloric acid component and alcohol component. It was found that the non-toxic preservative composition containing the mineral ion active water according to the present invention had excellent germicidal power, was completely non-toxic, was usable for drinking, and had no problem even when sprayed on the eyes , And it has an advantage that it is suitable as a vaginal detergent since it exhibits an epoch-making effect on the removal of odor. The vaginal detergent contains the mineral ion active water according to the present invention and can be prepared by adding a conventional cleaning composition. For example, dissolution aids, emulsifiers and pH adjusting agents may be added to the sterilized water, Derived extracts which can be improved. Examples of herbal extracts include chamomile, calendula, cornflower, and the like. However, the present invention is not intended to be limited thereto, and it should be understood that the herb extract is representative of various herbs and herbal ingredients.

In addition, it can be used in various other cosmetic formulations, and it is possible to completely replace the preservative ingredient of cosmetics to provide the best cosmetics without skin troubles. In addition to the effect of makeup, it can prevent acne, ringworm, athlete's foot, gonorrhea and atopic dermatitis And can be developed as an effective product for treatment. For example, it can be commercialized as an exfoliating massage cream that can be used for atopic dermatitis, a non-toxic deodorant that does not cause any trouble on the eyes, a moisturizer that removes dry blemishes, and a foot dry moisturizer to prevent and treat athlete's foot.

Hereinafter, preferred embodiments and comparative examples of the present invention will be described.

The following examples are intended to illustrate the invention and should not be construed as limiting the scope of the invention.

Example  One

An electrode plate was made of an alloy of silver (Ag): copper (Cu) = 50: 50 in weight ratio by using the same sterilization water producing apparatus as the apparatus for producing sterilization water for livestock described in Korean Patent No. 1559360, Mineral ionized water having a mineral ion concentration of about 10 ppm was obtained by applying a high voltage to purified water (TDS (Total Dissolved Solid) = 1 ppm or less), and performing electrolysis for 24 hours based on purified water 10t.

Further, hydrogen gas was pressurized to purified water at a temperature of 10 캜 at a pressure of 5 atm for 30 minutes to enrich hydrogen in water to obtain hydrogenated water.

The mineral ion water and hydrogen reduced water were mixed in a ratio of mineral ion water: hydrogen reduced water in a volume ratio of 1: 1 to obtain the mineral ion active water according to the present invention.

Experimental Example  One

The sterilization effect of the mineral ion active water obtained in Example 1 was compared with mineral ion water and hydrogen reduced water as a control, and the results thereof (sterilization rate,%) are shown in Table 1 below And conducted by a test institute). Figs. 1A and 1B show test results of sterilization effect of mineral ion activated water (Figs. 1A and 1B: test results of Escherichia coli sterilization effect test, Figs. 2A and 2B: test results of pseudomonas aeruginosa effect test, : Salmonella bactericidal effect test report, Fig. 4a and Fig. 4b: Test result of bactericidal effect of pneumococci).

division Example Control Mineral ion active water Mineral ion water Hydrogen reduced water Fungi Escherichia coli 99.999 85,000 50.247 P. aeruginosa 99,000 82.455 40.492 Pneumococcus 99.515 84.235 35.263 Salmonella 99.752 84.782 47.591

As shown in Table 1, it was confirmed that the mineral ion active water according to the present invention exhibits remarkably improved sterilization effect as compared with mineral ion water or hydrogen reduced water. In particular, regardless of the species, Respectively.

Experimental Example  2

The deodorizing effect of the mineral ion active water obtained in Example 1 was compared with mineral ion water and hydrogen reduced water as a control and the result (deodorization rate,%) is shown in the following Table 2 (KTR). ≪ / RTI > The results of the deodorizing effect test of the mineral ion activated water are shown in FIG. 5 to FIG. 8 (FIG. 5: Deodorizing effect test report on ammonia, FIG. 6: Deodorizing effect test report on hydrogen sulfide, Deodorizing effect test report on the product, Figure 8: Deodorizing effect test report on the trimethylamine).

division Example Control Mineral ion active water Mineral ion water Hydrogen reduced water Seed ammonia 99 75 45 Hydrogen sulfide 98 74 42 Methyl mercaptan 98 74 42 Trimethylamine 97 71 38

As shown in Table 2, it was confirmed that the mineral ion active water according to the present invention exhibits remarkably improved deodorizing effect as compared with mineral ion water or hydrogen reduced water. In particular, regardless of the kind of the seeds (odor type) It is possible to confirm that the deodorizing effect is uniformly high.

Example  2

In addition to the mineral ion active water according to the present invention obtained in Example 1, the herb extract was prepared in the same manner as in the preparation of the general mask pack except for the following ingredients: chamomile extract, sodium dry sulphate (conditioning agent), sodium hydrogencarbonate (detergent) A cosmetic composition was prepared by mixing cocamidopropyl betaine (a surfactant) and the like, and the mixture was impregnated with a pack nonwoven fabric to prepare a mask pack.

Experimental Example  3

Sensory tests were carried out on the mask pack obtained in Example 2 using adult women as a panel. The panel consisted of 30 subjects consisting of 20 to 5 people, 30 to 5 people, 40 to 10 people, 50 to 5 people, and 60 to 5 people. The subjects were divided into three categories: moisturizing effect, soothing effect, And the results were averaged. As a result, it showed excellent sensory test results with 9.1 points of moisturizing effect, 9.2 points of soothing effect, and 9.6 points of itching alleviation effect in evaluation after 2 hours of wear and detachment of 30 minutes. Thus, excellent mask pack which does not show irritation or toxicity on facial skin It was confirmed that the production was possible.

Example  3

In addition to the mineral ion active water according to the present invention obtained in Example 1, the herbal extracts were prepared in the same manner as in the preparation of general quality detergents except for chamomile extract, dried sodium sulfate (conditioning agent), sodium hydrogen carbonate (detergent), glycerin A surfactant), sodium sulfate, coco glucoside, glyceryl oleate, citric acid, limonene, benzyl alcohol, lactic acid, and the like were mixed to prepare a vaginal detergent.

Experimental Example  4

The vaginal cleanser obtained in Example 3 was subjected to a sensory test using adult women as a panel. The panel consisted of 40 subjects, 10 to 20, 10 to 30, 10 to 40, and 10 to 50. The subjects were divided into three groups: pain relief, deodorization, and itching relief. The scores were scored based on the score, and the results were averaged. As a result, it was confirmed that a superior quality detergent which does not exhibit irritation or toxicity can be manufactured by showing excellent sensory test results with pain relieving effect of 9.7, deodorizing effect of 9.5, and itching relieving effect of 9.6 in the evaluation after 3 days of use there was.

While the invention has been shown and described with reference to certain exemplary embodiments thereof, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention as defined by the appended claims.

(Without reference numerals)

Claims (5)

5 to 99% by volume of a mineral ion active water, wherein the mineral ion active water comprises mineral ion water including metal ions and exhibiting excellent sterilizing properties; And hydrogen-enriched hydrogen-containing water, wherein the mineral ion water: hydrogen-reduced water is mixed in a volume ratio of 1: 0.5 to 1.5. The method according to claim 1,
Wherein the mineral ionized water contains metal ions ionized by electrolysis at a high voltage of from 10,000 to 50,000 V, wherein the mineral ion water comprises iron, copper, zinc, silver, aluminum, and at least two of the alloys; and a redox potential of -100 to -500 ( ORP). ≪ RTI ID = 0.0 > 18. < / RTI >
The method according to claim 1,
Characterized in that the hydrogen-reduced water is hydrogenated at a temperature within a range of 5 to 15 占 폚 by pressurizing hydrogen gas at a pressure of 2 to 10 atm for 10 to 60 minutes to enrich hydrogen in the water. Composition.
The method according to claim 1,
Wherein the non-toxic antiseptic composition comprising the mineral ion active water further comprises a non-toxic extract.
5. The method of claim 4,
Wherein said stem extract is selected from the group consisting of water, methanol, ethanol, hexane, methylene chloride, ethyl acetate, butanol, propylene glycol, butylene glycol, dipropylene glycol, glycerin and mixtures of two or more thereof Wherein the water is immersed in a selected polar solvent, immersed in a temperature range of 10 to 40 占 폚 for 12 to 240 hours, and then filtered to remove solid content.
KR1020160026226A 2016-03-04 2016-03-04 Unpoisonous anticeptic composition comprising mineral ion activated water KR20170103390A (en)

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KR102261122B1 (en) * 2020-07-14 2021-06-07 농업회사법인 주식회사 오케이120 Composition for reduction of nicotine content in blood
KR20210076356A (en) * 2019-12-16 2021-06-24 주식회사 청명 농업회사법인 Peanut sprout cultivation method using abeliophyllum distichum extract

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210076356A (en) * 2019-12-16 2021-06-24 주식회사 청명 농업회사법인 Peanut sprout cultivation method using abeliophyllum distichum extract
KR102261122B1 (en) * 2020-07-14 2021-06-07 농업회사법인 주식회사 오케이120 Composition for reduction of nicotine content in blood
JP2022025032A (en) * 2020-07-14 2022-02-09 オーケー120 カンパニー リミテッド Composition for reducing blood nicotine concentration, and method for producing the same

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