KR20120089718A - 수크로오스-6-에스테르의 제조를 위한 저온 단일 용매 공정 - Google Patents

수크로오스-6-에스테르의 제조를 위한 저온 단일 용매 공정 Download PDF

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Publication number
KR20120089718A
KR20120089718A KR1020127012141A KR20127012141A KR20120089718A KR 20120089718 A KR20120089718 A KR 20120089718A KR 1020127012141 A KR1020127012141 A KR 1020127012141A KR 20127012141 A KR20127012141 A KR 20127012141A KR 20120089718 A KR20120089718 A KR 20120089718A
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South Korea
Prior art keywords
sucrose
reaction mixture
ester
organotin
temperature
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Ceased
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KR1020127012141A
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English (en)
Korean (ko)
Inventor
에드워드 미신스키
데이비드 콜맨
제임스 에드윈 윌리
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테이트 앤드 라일 테크놀러지 리미티드
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Publication of KR20120089718A publication Critical patent/KR20120089718A/ko
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/22—Tin compounds
    • C07F7/2224—Compounds having one or more tin-oxygen linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C07H13/06—Fatty acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020127012141A 2009-10-12 2010-10-12 수크로오스-6-에스테르의 제조를 위한 저온 단일 용매 공정 Ceased KR20120089718A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US25068109P 2009-10-12 2009-10-12
US61/250,681 2009-10-12
PCT/GB2010/001904 WO2011045566A1 (en) 2009-10-12 2010-10-12 Low temperature, single solvent process for the production of sucrose-6-ester

Publications (1)

Publication Number Publication Date
KR20120089718A true KR20120089718A (ko) 2012-08-13

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KR1020127012141A Ceased KR20120089718A (ko) 2009-10-12 2010-10-12 수크로오스-6-에스테르의 제조를 위한 저온 단일 용매 공정

Country Status (8)

Country Link
US (1) US8921540B2 (enExample)
EP (1) EP2488541A1 (enExample)
JP (1) JP5726195B2 (enExample)
KR (1) KR20120089718A (enExample)
CN (1) CN102639550B (enExample)
GB (1) GB2474311B (enExample)
IE (1) IE86139B1 (enExample)
WO (1) WO2011045566A1 (enExample)

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US10047038B2 (en) 2013-11-27 2018-08-14 Tate & Lyle Technology Limited Waste treatment process
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2544217B (en) 2014-08-08 2020-03-25 Tate & Lyle Tech Ltd Chlorination of sucrose-6-esters
CN104774226A (zh) * 2015-04-08 2015-07-15 常州市牛塘化工厂有限公司 一种蔗糖-6-乙酯的制备方法
CN105254684B (zh) * 2015-11-03 2019-01-01 浙江新和成股份有限公司 一种蔗糖-6-乙酸酯的制备方法
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF
CN106349300B (zh) * 2016-08-30 2019-02-26 安徽金禾实业股份有限公司 三氯蔗糖酯化单溶剂反应方法
CN108558962B (zh) 2018-05-22 2020-06-30 山东新和成精化科技有限公司 一种用于合成蔗糖-6-酯的方法
CN109438533A (zh) * 2018-12-10 2019-03-08 安徽金禾实业股份有限公司 一种三氯蔗糖生产中高温连续酰化的方法
CN109575069A (zh) * 2018-12-10 2019-04-05 安徽金禾实业股份有限公司 一种三氯蔗糖生产中催化剂的回收方法
CN112973166B (zh) * 2019-12-17 2024-04-30 无锡弘鼎华化工设备有限公司 一种三氯蔗糖中和液溶剂的回收装置及方法
CN111574572A (zh) * 2020-05-22 2020-08-25 安徽金禾实业股份有限公司 一种三氯蔗糖生产中有机锡催化剂连续性制备补充的方法
WO2022051988A1 (zh) 2020-09-10 2022-03-17 安徽金禾实业股份有限公司 一种蔗糖-6-酯的制备方法
CN112808048B (zh) * 2021-01-04 2022-05-31 安徽金禾实业股份有限公司 蔗糖-6-酯的制造设备及制造方法
US12434171B2 (en) * 2021-02-19 2025-10-07 Anhui Jinhe Industrial Co., Ltd. Production apparatus and production method of sucrose-6-ester
EP4163001B1 (en) * 2021-02-19 2024-12-11 Anhui Jinhe Industrial Co., Ltd. Production apparatus and production method for sucrose-6-ester
CN112933634B (zh) * 2021-03-04 2022-04-08 安徽金禾实业股份有限公司 一种环列式的蔗糖-6-酯连续生产设备及生产工艺流程
CN112973164B (zh) * 2021-03-04 2022-09-02 安徽金禾实业股份有限公司 一种高效率的蔗糖6酯连续生产设备及方法
WO2024082175A1 (zh) 2022-10-19 2024-04-25 安徽金禾实业股份有限公司 一种三氯蔗糖精品的制备方法
CN115894579A (zh) * 2022-11-17 2023-04-04 安徽金禾实业股份有限公司 一种三氯蔗糖生产中b糖的处理方法

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Publication number Publication date
GB2474311B (en) 2012-10-17
EP2488541A1 (en) 2012-08-22
GB0920385D0 (en) 2010-01-06
CN102639550A (zh) 2012-08-15
JP5726195B2 (ja) 2015-05-27
US8921540B2 (en) 2014-12-30
IE20100653A1 (en) 2011-05-11
GB2474311A (en) 2011-04-13
CN102639550B (zh) 2016-01-27
JP2013507349A (ja) 2013-03-04
WO2011045566A1 (en) 2011-04-21
US20110087018A1 (en) 2011-04-14
IE86139B1 (en) 2013-02-27

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