GB2474311B - Low temperature, single solvent process for the production of sucrose-6-ester - Google Patents

Low temperature, single solvent process for the production of sucrose-6-ester

Info

Publication number
GB2474311B
GB2474311B GB0920385.2A GB0920385A GB2474311B GB 2474311 B GB2474311 B GB 2474311B GB 0920385 A GB0920385 A GB 0920385A GB 2474311 B GB2474311 B GB 2474311B
Authority
GB
United Kingdom
Prior art keywords
sucrose
ester
production
low temperature
single solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
GB0920385.2A
Other languages
English (en)
Other versions
GB0920385D0 (en
GB2474311A (en
Inventor
Edward Micinski
David Coleman
James Edwin Wiley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tate and Lyle Technology Ltd
Original Assignee
Tate and Lyle Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate and Lyle Technology Ltd filed Critical Tate and Lyle Technology Ltd
Publication of GB0920385D0 publication Critical patent/GB0920385D0/en
Publication of GB2474311A publication Critical patent/GB2474311A/en
Application granted granted Critical
Publication of GB2474311B publication Critical patent/GB2474311B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/22—Tin compounds
    • C07F7/2224—Compounds having one or more tin-oxygen linkages
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C07H13/06—Fatty acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
GB0920385.2A 2009-10-12 2009-11-20 Low temperature, single solvent process for the production of sucrose-6-ester Active GB2474311B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US25068109P 2009-10-12 2009-10-12

Publications (3)

Publication Number Publication Date
GB0920385D0 GB0920385D0 (en) 2010-01-06
GB2474311A GB2474311A (en) 2011-04-13
GB2474311B true GB2474311B (en) 2012-10-17

Family

ID=41565635

Family Applications (1)

Application Number Title Priority Date Filing Date
GB0920385.2A Active GB2474311B (en) 2009-10-12 2009-11-20 Low temperature, single solvent process for the production of sucrose-6-ester

Country Status (8)

Country Link
US (1) US8921540B2 (enExample)
EP (1) EP2488541A1 (enExample)
JP (1) JP5726195B2 (enExample)
KR (1) KR20120089718A (enExample)
CN (1) CN102639550B (enExample)
GB (1) GB2474311B (enExample)
IE (1) IE86139B1 (enExample)
WO (1) WO2011045566A1 (enExample)

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GB201110520D0 (en) * 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN104098617A (zh) * 2013-04-08 2014-10-15 南京工业大学 一种蔗糖-6-乙酸酯的制备方法
US10047038B2 (en) 2013-11-27 2018-08-14 Tate & Lyle Technology Limited Waste treatment process
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2544217B (en) 2014-08-08 2020-03-25 Tate & Lyle Tech Ltd Chlorination of sucrose-6-esters
CN104774226A (zh) * 2015-04-08 2015-07-15 常州市牛塘化工厂有限公司 一种蔗糖-6-乙酯的制备方法
CN105254684B (zh) * 2015-11-03 2019-01-01 浙江新和成股份有限公司 一种蔗糖-6-乙酸酯的制备方法
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF
CN106349300B (zh) * 2016-08-30 2019-02-26 安徽金禾实业股份有限公司 三氯蔗糖酯化单溶剂反应方法
CN108558962B (zh) 2018-05-22 2020-06-30 山东新和成精化科技有限公司 一种用于合成蔗糖-6-酯的方法
CN109438533A (zh) * 2018-12-10 2019-03-08 安徽金禾实业股份有限公司 一种三氯蔗糖生产中高温连续酰化的方法
CN109575069A (zh) * 2018-12-10 2019-04-05 安徽金禾实业股份有限公司 一种三氯蔗糖生产中催化剂的回收方法
CN112973166B (zh) * 2019-12-17 2024-04-30 无锡弘鼎华化工设备有限公司 一种三氯蔗糖中和液溶剂的回收装置及方法
CN111574572A (zh) * 2020-05-22 2020-08-25 安徽金禾实业股份有限公司 一种三氯蔗糖生产中有机锡催化剂连续性制备补充的方法
WO2022051988A1 (zh) 2020-09-10 2022-03-17 安徽金禾实业股份有限公司 一种蔗糖-6-酯的制备方法
CN112808048B (zh) * 2021-01-04 2022-05-31 安徽金禾实业股份有限公司 蔗糖-6-酯的制造设备及制造方法
US12434171B2 (en) * 2021-02-19 2025-10-07 Anhui Jinhe Industrial Co., Ltd. Production apparatus and production method of sucrose-6-ester
EP4163001B1 (en) * 2021-02-19 2024-12-11 Anhui Jinhe Industrial Co., Ltd. Production apparatus and production method for sucrose-6-ester
CN112933634B (zh) * 2021-03-04 2022-04-08 安徽金禾实业股份有限公司 一种环列式的蔗糖-6-酯连续生产设备及生产工艺流程
CN112973164B (zh) * 2021-03-04 2022-09-02 安徽金禾实业股份有限公司 一种高效率的蔗糖6酯连续生产设备及方法
WO2024082175A1 (zh) 2022-10-19 2024-04-25 安徽金禾实业股份有限公司 一种三氯蔗糖精品的制备方法
CN115894579A (zh) * 2022-11-17 2023-04-04 安徽金禾实业股份有限公司 一种三氯蔗糖生产中b糖的处理方法

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US5034551A (en) * 1990-04-23 1991-07-23 Noramco, Inc. Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
EP0475619A1 (en) * 1990-08-27 1992-03-18 McNEIL-PPC, INC. Catalyzed sucrose-6-ester process
WO2006120697A2 (en) * 2005-02-22 2006-11-16 Pharmed Medicare Private Limited Tin mediated regioselective synthesis of sucrose-6-esters
WO2009035503A1 (en) * 2007-09-13 2009-03-19 Polymed Therapeutics, Inc. Novel process for preparing sucrose-6-esters

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US4950746A (en) * 1988-07-18 1990-08-21 Noramco, Inc. Process for synthesizing sucrose derivatives by regioselective reaction
US5023329A (en) * 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
US5034551A (en) * 1990-04-23 1991-07-23 Noramco, Inc. Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
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WO2006120697A2 (en) * 2005-02-22 2006-11-16 Pharmed Medicare Private Limited Tin mediated regioselective synthesis of sucrose-6-esters
WO2009035503A1 (en) * 2007-09-13 2009-03-19 Polymed Therapeutics, Inc. Novel process for preparing sucrose-6-esters

Also Published As

Publication number Publication date
EP2488541A1 (en) 2012-08-22
GB0920385D0 (en) 2010-01-06
KR20120089718A (ko) 2012-08-13
CN102639550A (zh) 2012-08-15
JP5726195B2 (ja) 2015-05-27
US8921540B2 (en) 2014-12-30
IE20100653A1 (en) 2011-05-11
GB2474311A (en) 2011-04-13
CN102639550B (zh) 2016-01-27
JP2013507349A (ja) 2013-03-04
WO2011045566A1 (en) 2011-04-21
US20110087018A1 (en) 2011-04-14
IE86139B1 (en) 2013-02-27

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