KR102635645B1 - A hair care composition comprising the natural plant mixture - Google Patents

Abstract

The hair care composition containing a mixture of horsetail, sorghum, nettle, pumpkin seed, tomato, sorghum, linseed, centella asiatica and rosemary as active ingredients according to the present invention has hair loss prevention and hair growth effects, as well as a hair moisturizing effect and an anti-static effect on the hair. , has a hair splitting prevention effect and has a strong antibacterial effect against dandruff bacteria. Therefore, the hair care composition containing the natural plant mixture according to the present invention can simultaneously improve both the scalp and hair, and can be used in functional hair care products such as hair conditioner, hair tonic, hair cream, hair lotion, and hair face. , hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol spray, aerosol mousse, aerosol spray, perm, bleach, dye, ampoule, shampoo or rinse, etc. can be used

Description

A hair care composition comprising the natural plant mixture as an active ingredient {A hair care composition comprising the natural plant mixture}

The present invention relates to a hair care composition containing a mixture of natural plants as an active ingredient, and more specifically, to a hair care composition containing a mixture of horsetail, horsetail, nettle, pumpkin seed, tomato, sorghum, linseed, centella asiatica, and rosemary as active ingredients. The active ingredient is a natural plant extract or fermented product mixture that has a hair growth effect as well as an itching and hair loss prevention effect by suppressing excessive production of sebum and has a strong antibacterial effect against dandruff bacteria, an anti-static effect on the hair, an anti-splitting effect on the hair, and a hair growth effect. Containing hair conditioner, hair tonic, hair cream, hair lotion, hair face, hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol spray, aerosol. It relates to hair care compositions such as mousses, aerosol sprays, perms, bleaches, dyes, ampoules, shampoos or rinses.

There are about 80,000 to 90,000 hairs on the human scalp. It is normal for the average person to lose up to 50 to 70 hairs every day, but if about 100 or more hairs fall out excessively without any particular reason after washing your hair or going to bed, you may have alopecia. can be suspected. The exact cause of this hair loss has not yet been determined, but in general, it is genetic factors, hormonal imbalance, excessive stress, seborrheic dermatitis, poor blood circulation in the scalp (scalp muscle tension), eating habits, nutritional and iron deficiency, and hair pulling. (Traction alopecia), atopic constitution, hair pollution (frequent perm, dyeing, use of hair dryer, etc.), air pollution, infection and inflammatory diseases, chemical factors (alcohol, drugs, smoking), childbirth, menopausal disorders, etc. It is known.

In the human body, hair grows from hair follicles in the skin, and the hair follicles from which hair grows are complex organs composed of the inner root epithelial sheath, outer root epithelial sheath, hair stem, and hair matrix, and have cycles such as growth phase, catagen phase, and resting phase throughout life. It has the characteristic of being continuously repeated. In particular, among the cells that form hair follicles, dermal papilla cells play an important role in hair growth, and during the growth period of hair follicles, proliferation of hair follicle constituent cells, including keratinocytes of the stroma surrounding the dermal papilla, occurs. In the catagen phase, hair follicle growth stops and apoptosis, condensation of the dermal papilla, and reorganization of the extracellular matrix occur. In the telogen phase, which is the stage in which the hair follicle prepares to enter the growth phase again, only the permanent parts, including the ridges, remain. This remains.

Hair is damaged by various external factors such as shampooing, drying, styling, and the surrounding environment, and also remains dry, rough, and dull due to excessive friction on the scalp or removal of natural moisturizing ingredients when washing with shampoo. I do it.

Hair is composed of cuticle, cortex, and medula. Among them, the cortex accounts for more than 80% and has a great influence on the characteristics of hair. The fur cortex is divided into a crystalline region and an amorphous region. It is a fibrous layer composed of fibrous keratin proteins, and its physicochemical properties are determined by the way the keratin molecules are combined and the amount or amount of sulfur (S) it contains.

At this time, hard keratin, which is a fibrous tissue, forms a crystalline region, and between the fibrous tissues is an amorphous region where interstitial substances are located. This liver material layer is largely composed of soft proteins (soft keratin) and lipids, such as cholesterol and its derivatives, fatty alcohols, fatty acids, and ceramides, as well as small amounts of phospholipids, Includes polysaccharide, etc. It is known that this part is largely lost in damaged hair. This is because the amorphous region made of intercellular material is more vulnerable to various stimuli and is easily lost compared to the tightly bonded fibrous region.

Therefore, it is important to fundamentally protect or restore these amorphous regions in hair conditioning such as hair softness, flexibility, shine, anti-static, and ease of combing.

Since hair is a part of one's appearance and plays an important role in improving one's public image, the importance of research on hair growth, hair loss, and hair loss prevention has recently been increasing. In particular, as lifestyle patterns become westernized, quality of life improves, and stress increases, concerns such as hair loss and scalp disease are becoming more of a concern for everyone. The causes are simple genetic factors and acquired factors, and the causes are simple. Importance and interest are gradually growing. Since hair loss can cause psychological withdrawal, which can lead to interpersonal avoidance and loss of confidence, it can have a significant impact on maintaining an individual's prosperous life, and the hair loss industry market is continuously growing rapidly.

Hair loss refers to an abnormal increase in the number of hairs falling out during the growth cycle of hair follicles, as the ratio of hair growing in hair follicles in the catagen or telogen phase increases compared to hair growing in hair follicles in the growth phase. It is generally known to be caused by an unbalanced diet, excessive drinking and smoking, drug use, lack of sleep, excessive stress, childbirth, menopausal disorders, frequent perms and dyeing, and hormonal imbalance. Hair growing on a person's head maintains a certain density as the process of birth, growth, and loss is repeated, but when hair loss progresses due to the various causes above, the hair on the crown or forehead first becomes thinner and begins to lose strength, causing hair loss. The number increases.

In other words, hair is rooted in the scalp and receives nutrients from the blood, but over a long period of time, when the capillaries shrink and the scalp becomes thin and hair cannot grow normally, the hair in that area gradually becomes thinner and the lifespan of the hair in that specific area decreases. Hair becomes shorter and its lifespan is shortened, and not only does it fall out easily, but hair cannot grow again from the pores where the hair has fallen out, ultimately leading to symptoms of thin hair.

Recently, as the tendency to focus on appearance has become more prominent, interest in hair loss is also increasing. The causes of this hair loss have been discussed as poor blood circulation, excessive male hormone action, excessive sebum secretion, decreased scalp function due to peroxides and bacteria, genetic factors, aging, stress, etc., but there is still no clear explanation for hair loss. The cause is unknown. In general, the most typical form of hair loss is male-pattern alopecia, which is caused by excessive action of male hormones. It occurs dependent on androgens, male hormones. Representative androgens include testosterone and dihydrotestosterone, and hair loss patients are more likely to have DHT. It is known. Testosterone is converted to DHT by 5-reductase, and this conversion occurs by Type 2 5-alpha-reductase among the two types of 5-alpha-reductase, Type 1 and Type 2. It has been reported that converted DHT causes gradual shrinkage of dermal papillae and hair follicles.

Representative hair loss treatments currently approved by the U.S. Food and Drug Administration (FDA) include minoxidil for application and Propecia for oral use, which are synthetic drugs, and several side effects are continuously reported. Propecia is effective by inhibiting the process of converting male hormone (testosterone) to dihydrotestosterone (DHT), the causative agent of hair loss, but concerns have been raised that it may reduce men's libido, and minoxidil was developed as a treatment for high blood pressure, but causes hair follicle activation. It was developed as a hair growth agent as it was reported to promote hair growth, but side effects such as various skin diseases have been reported.

Natural substances useful for hair growth that have been studied so far include soybean (Glycine linne, isoflavone), ginger (Zingiber officinale, 6-gingerol), red pepper (Capsicum annuum), aloe (Aloe arborescens), licorice (Glycyrrhiza glabra), and tea tree (Camellia sinensis). ), Ginkgo biloba, avocado (Persea americana), and Polygonum multiflorum have been reported.

Additionally, studies based on natural extracts have also been conducted. For example, extracts of Cheongung (Patent No. 2010-0119761), Sanghwang Mushroom (Patent No. 2012-0038426), Honeysuckle (Patent No. 2012-0038426), Chemomile, etc. (Patent No. 2012-0015874, Patent No. 2010) -0091571), Hasuo (Patent No. 2013-0021464, Patent No. 2011-0097386), Calamus (Patent No. 2012-0115980), Pomegranate (Patent No. 2012-7012465), Ginkgo Leaf Extract (Patent No. 2006-7008793) There are results such as: However, when these hair growth agents or hair growth agents are used in actual clinical practice, the effect on the scalp is not that excellent, and hair growth agents made of natural substances that are more effective and have fewer side effects than Minoxidil or Propecia, which are reluctant to be used due to concerns about side effects, are used. Exploratory research is actively underway.

However, despite efforts to utilize such natural products, the commercialization of hair growth promoters or hair loss inhibitors is still minimal due to their lower activity compared to pharmaceuticals.

Accordingly, while continuing research to develop a hair care composition that can solve the above-mentioned problems and improve hair and fur, the present inventors used a mixture of horsetail, horsetail, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica, and rosemary. The present invention was completed by discovering that hair products containing active ingredients have anti-hair loss and hair growth effects while also having a moisturizing effect on hair, an anti-static effect on hair, an effect on preventing hair splitting, and a strong antibacterial effect against dandruff bacteria. .

The technical problem to be solved by the present invention is to provide a hair care composition that has hair loss prevention and hair growth effects, as well as a hair moisturizing effect, an anti-static effect on the hair, an anti-splitting effect on the hair, and a strong antibacterial effect against dandruff bacteria.

In order to solve the above-described technical problem, the present invention provides a hair care composition comprising a mixture of horsetail, horsetail, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica, and rosemary as active ingredients.

Preferably, the mixture contains 90 to 110 parts by weight of horsetail, 40 to 60 parts by weight of nettle, 140 to 160 parts by weight of pumpkin seeds, 140 to 160 parts by weight of tomatoes, 40 to 60 parts by weight of sorghum, and 140 to 140 parts by weight of flax seeds. It is characterized by a mixture of 160 parts by weight, 90 to 110 parts by weight of Centella asiatica, and 140 to 160 parts by weight of rosemary.

Preferably, the horsetail, horsetail, nettle, pumpkin seed, tomato, sorghum, linseed, centella asiatica, and rosemary are each extract or fermented product.

Preferably, the complex extract or complex fermentation product is characterized in that it is included in an amount of 0.5 to 10% by weight based on the total weight of the hair care composition.

Preferably, the extract is characterized in that it is obtained by freeze-drying and pulverizing a natural plant, performing hot water extraction for 50 to 70 minutes using purified water at 90 to 110° C., followed by filtration and concentration under reduced pressure.

Preferably, the fermented product is characterized in that it is manufactured by freeze-drying and pulverizing a natural plant, extracting it with hot water for 50 to 70 minutes using purified water at 90 to 110°C, and then fermenting 100 parts by weight of the hot water extract using fermentation bacteria. .

Preferably, the hair care composition is a hair conditioner, hair tonic, hair cream, hair lotion, hair face, hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol. It is characterized by being a spray, aerosol mousse, aerosol spray, perm, bleach, dye, ampoule, shampoo or rinse.

As such, the hair care composition containing the natural plant mixture according to the present invention has hair loss prevention and hair growth effects, as well as a hair moisturizing effect, an anti-static effect on the hair, an anti-splitting effect on the hair, and a strong antibacterial effect against dandruff bacteria. Therefore, the hair care composition containing the natural plant mixture according to the present invention can simultaneously improve both the scalp and hair, and can be used in functional hair care products such as hair conditioner, hair tonic, hair cream, hair lotion, and hair face. , hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol spray, aerosol mousse, aerosol spray, perm, bleach, dye, ampoule, shampoo or rinse, etc. can be used

Hereinafter, the present invention will be described in more detail.

The present invention provides a hair care composition comprising a mixture of horsetail, sorghum, nettle, pumpkin seed, tomato, sorghum, linseed, centella asiatica, and rosemary as active ingredients.

The hair care composition containing the natural plant mixture according to the present invention has hair loss prevention and hair growth effects, as well as a hair moisturizing effect, an anti-static effect on the hair, an anti-splitting effect on the hair, and a strong antibacterial effect against dandruff bacteria.

According to one embodiment of the present invention, the natural plant mixture may be a natural plant extract or a mixture of natural plant fermentation products.

According to one embodiment of the present invention, the natural plant mixture contains 90 to 110 parts by weight of horsetail, 40 to 60 parts by weight of nettle, 140 to 160 parts by weight of pumpkin seeds, 140 to 160 parts by weight of tomatoes, and sorghum. It is characterized by a mixture of 40 to 60 parts by weight, 140 to 160 parts by weight of flaxseed, 90 to 110 parts by weight of Centella asiatica, and 140 to 160 parts by weight of rosemary.

The horsetail (Equisetum arvense) is a type of perennial fern belonging to the Horsetail family and is a perennial herbaceous plant that grows in mountains and fields across the country. In oriental medicine, siliceous substances are accumulated in the reproductive stems, so the ones that are dug up in the fall and dried in the shade are called munhyeong (門荊). They are known to have pharmacological effects such as diuresis, colic treatment, flushing, and lowering blood pressure, and have been used as oriental medicine since ancient times. The main components of horsetail are known to include silicic acid, galuteolin, luteolin, isoquercitrin, aconitic acid, and articulatidin, and trace amounts of fatty acids, In addition to fat and amino acids, it contains more minerals and silicic acid (5 to 8% of dry weight) than other plants. Research on horsetail has so far reported blood sugar control effects, antibacterial activity, skin aging prevention by inhibiting elastase activity, and heavy metal removal effects. In addition, it has been revealed that it also has the effect of controlling blood sugar levels in diabetic patients.

Polygonum multiflorum thunberg is a perennial vine belonging to the knotweed family. Its leaves are heart-shaped and its roots grow into the ground, often forming round tubers. In general, when we say red ash, we mean red ash, and white cypress is often confused with cypress, but it is Cynanchumm wilfordii Hemsley, the tuberous root of the silver squirrel of the Pakchummidae family, and is completely different from cynanchumm. Sewage is widely used as an herbal medicine material mainly in China and Japan, and has the characteristic of being toxic and requiring legal regulation for its use.

The nettle (Urtica thunbergiana) is a herbaceous plant of the nettle family and has stinging hairs. The hairs on the inside of the leaves contain antibacterial and antioxidant substances. Additionally, the leaf stem is known to contain magnesium, vitamin C, vitamin B, vitamin K, potassium, silica, zinc, iron, omega-3, lignan, selenium, and vitamin E.

The pumpkin seeds are a food containing arginine and are known to have effects such as acting as a vasodilator to promote blood circulation, improve kidney function, and suppress edema.

The above tomatoes grow well at relatively high temperatures and like strong sunlight. In general, they are divided into finite-growth tomatoes and indefinite-growth tomatoes. Finite-growth tomatoes are mainly used for processing, and the tomatoes that are mainly grown and consumed in Korea are indefinite-growth tomatoes. Ingredients contained in tomatoes include citric acid, malic acid, succinic acid, amino acids, rutin, protein carbohydrates, calcium, iron, phosphorus, vitamins A, B1, B2, C, and dietary fiber. In the case of vitamin C, one tomato contains about half of the recommended daily intake.

The sorghum (Sorghum bicolor L. Moench, sorghum) is an annual herb of the monocotyledonous plant family Rice family and is mainly consumed as food. It is native to tropical Africa and is most widely cultivated in dry areas. Depending on the use, grain sorghum, sweet sorghum, and broom-corn are cultivated in Asia, Africa, and Central America. It is a food resource that is being cultivated. Sorghum is produced globally at 57,772 thousand tons, ranking 5th among grains after rice, barley, wheat, and corn, and contains a large amount of active ingredients such as dietary fiber and phenolic compounds. Phenolic compounds are composed of condensed tannin, flavonoid, and phenolic acid, and most of them are known as flavonoids. These phytochemicals are known to exhibit various health functional activities beneficial to the human body, and polyphenol extracts from sorghum have been reported to have strong anti-mutagenic properties.

The flaxseed is a seed of flax, an annual plant of the flax family, and is rich in omega-3 fatty acids, which can prevent various cardiovascular diseases and heart diseases. It also has an anti-inflammatory effect and helps prevent dermatitis. In addition, flax seeds contain a large amount of lignan, which has anti-cancer effects. This is a type of phytoestrogen that acts similar to female hormones in the body and helps alleviate menopausal increased production. It is also rich in dietary fiber, which is good for constipation and dieting. It contains a large amount of unsaturated fatty acids.

Centella asiatica is a perennial plant that commonly grows in the mountains and fields of the southern islands of the Korean Peninsula. The main stem extends to the side, and there are two degenerated scale-shaped leaves near the node where the root comes from. The leaves grow densely at the nodes, are kidney-shaped, 2 to 5 cm in diameter, have a glossy surface, have dull sawtooth edges, and the length of the petiole is 4 to 20 cm. The flowers are red-purple, grow in umbels of 3 to 4 at each leaf axil, and are shaped like a head. The style is two-pronged, and the fruit is an oblong shape. In India, after seeing a wounded tiger rolling around in a place where there were a lot of centella asiatica to heal, it was called tiger plant and has been used as medicine for a long time. Madecassic acid, a component found in the leaves and stems of Centella asiatica, has been found to have the power to relieve inflammation and heal wounds such as tumors and ulcers, and is now used as a raw material for ointments, toothpaste, and cosmetics.

The rosemary (Rosmarinus officinalis) is an evergreen tree native to the Mediterranean belonging to the Labiatae family, and is one of the traditional European spices mainly cultivated in southern Europe. It contains 1,8-cineole, It contains essential oils containing camphor as its main ingredient and active ingredients such as rosmarinic acid, so it is widely used in the fields of medicine and cosmetics for anti-inflammatory, diuretic, anti-aging, and whitening purposes.

The term "extract" in the present invention refers to a preparation obtained by squeezing raw materials into an appropriate leachate and evaporating and concentrating the leachate. It is not limited thereto, but includes the extract, dilution or concentrate of the extract, and extract obtained through extraction treatment. It may be a dried product obtained by drying, a crude product thereof, or a purified product.

The extraction can be performed using general extraction, separation and purification methods known in the art. The extraction method may include boiling water extraction, hot water extraction, cold needle extraction, reflux cooling extraction, or ultrasonic extraction, but is not limited thereto.

The term "extract" in the present invention refers to a preparation obtained by squeezing a herbal medicine into an appropriate leachate and evaporating and concentrating the leachate. It is not limited thereto, but includes, but is not limited to, the extract obtained through extraction processing, the diluted or concentrated liquid of the extract, and the extract. It may be a dried product obtained by drying, a crude product thereof, or a purified product.

The extract liquid used in the present invention can be extracted using a conventional extraction solvent known in the art, and the extracted liquid can be used in liquid form or after being concentrated and/or dried. At this time, the extraction solvent is, for example, (a) water, (b) anhydrous or hydrous lower alcohol having 1-4 carbon atoms (methanol, ethanol, propanol, butanol, etc.), (c) a mixture of the lower alcohol and water. It can be obtained by using (d) acetone, (e) ethyl acetate, (f) chloroform, or (g) 1,3-butylene glycol as an extraction solvent. Preferably, extraction is performed using methanol, ethanol or butane. The degree of extraction and loss of the active ingredients of the extract may vary depending on the extraction solvent, so select and use an appropriate extraction solvent. The extraction method is not particularly limited and includes, for example, hot water extraction, cold needle extraction, reflux cooling extraction, solvent extraction, steam distillation, ultrasonic extraction, elution, compression, etc.

In addition, the extract can be obtained through a conventional purification process in addition to extraction using the extraction solvent. For example, separation using an ultrafiltration membrane with a certain molecular weight cut-off value, separation using various chromatographs (designed for separation according to size, charge, hydrophobicity, or affinity), etc., were obtained through various additional purification methods. It can also be obtained through fractionation.

According to an embodiment of the present invention, about 1 to 10 times the weight of the natural plant sample, preferably about 2 to 5 times the weight of water, methanol, ethanol, propanol, and isopropanol. , butanol, etc., with an alcohol having 1 to 5 carbon atoms or a mixed solvent of water and alcohol, and extraction methods such as stirring extraction, hot water extraction, cold extraction, reflux cooling extraction, or ultrasonic extraction for about 10 to 20 hours. A natural plant extract can be obtained by performing hot water extraction, preferably at 50 to 100°C, and then filtering, concentrating under reduced pressure, or drying the obtained extract.

Specifically, the natural plant extract can be obtained by freeze-drying and pulverizing the natural plant, performing hot water extraction for 50 to 70 minutes using purified water at 90 to 110°C, followed by reduced pressure filtration and concentration.

In the present invention, the “fermented product” is characterized in that it is manufactured by freeze-drying and pulverizing natural plants, extracting them hot water for 50 to 70 minutes using purified water at 90 to 110°C, and then fermenting 100 parts by weight of the hot water extract using fermentation bacteria. do.

The fermenting bacteria include lactic acid bacteria such as Lactobacillus plantarum and Pediococcus acidilactici ; Bacillus bacteria such as Bacillus subtilis and Bacillus licheniformis ; and one or more strains selected from yeast such as Saccharomyces cerevisiae and Saccharomyces boulardii .

Fermentation bacteria used in the present invention include lactic acid bacteria, Bacillus bacteria, and yeast bacteria such as Lactobacillus plantarum and Pediococcus acidilactici ; Bacillus bacteria such as Bacillus subtilis and Bacillus licheniformis ; and yeast bacteria such as Saccharomyces cerevisiae and Saccharomyces boulardii . It is preferable to use a mixed strain in which one strain each from lactic acid bacteria, Bacillus bacteria, and yeast bacteria is selected and mixed. In particular, in the present invention, it is preferable to use a mixed strain of Lactobacillus plantarum, Bacillus subtilis , and Saccharomyces cerevisiae .

Lactic acid bacteria, such as Lactobacillus , suppress harmful microorganisms by lowering the intestinal pH by producing acid, and produce substances such as vitamins and various amino acids. They dominate the intestinal flora and have the effect of suppressing the growth of other bacteria, and yeast, such as Saccharomyces , have the effect of suppressing the growth of other bacteria. It produces nutrient-decomposing enzymes and has the effect of suppressing the generation of ammonia or improving the palatability of livestock feed due to alcohol, glutamic acid, etc. (Helle et al., 1993).

In the present invention, Saccharomyces cerevisiae is a representative yeast fungus belonging to Ascomycetes, is non-pathogenic, and produces alcohol and carbon dioxide by fermenting polysaccharides or monosaccharides even in stressful environments such as salt, ions, and heat. It has been used for food fermentation for a long time.

According to one specific embodiment of the present invention, a total of three strains were selected as the strain combination: one type of lactic acid bacteria ( Lactobacillus plantarum ), one type of Bacillus subtilis , and one type of yeast ( Saccharomyces cerevisiae ).

According to one embodiment of the present invention, the lactic acid bacteria, Bacillus bacteria, and yeast bacteria are preferably mixed at a weight ratio of 2:2:1.

In a preferred embodiment of the present invention, the natural plant fermentation product can be prepared by inoculating a natural plant mixture with lactic acid bacteria in an amount of 2 to 7% by weight based on the weight of the extract and culturing for 10 to 20 hours.

According to one embodiment of the present invention, the natural plant mixture is characterized in that it is included in an amount of 0.5 to 10% by weight based on the total weight of the hair care composition. At this time, if the natural plant mixture is contained in an amount of less than 0.5% by weight, it is difficult to obtain the effect of restoring the scalp and damaged hair, and if the natural plant mixture is contained in an amount exceeding 10.0% by weight, nutrients are excessive in the scalp. Rather, there is a risk of scalp waste and dead skin cells forming.

According to a preferred feature of the present invention, the hair care raw material is one of a hair shampoo raw material, a hair conditioner raw material, and a hair essence raw material.

According to a more preferred feature of the present invention, the hair care raw materials include 15 parts by weight of Ammonium Laureth Sulfate, 8 parts by weight of Sodium Lauroamphoacetate, and Potassium Cocoyl Glycinate. glycinate) 5.5 parts by weight, Sodium Cocoyl Amino Acids (5.5 parts by weight), Cocamide Methyl MEA (2.5 parts by weight), Hydroxypropyltrimonium Hydrolyzed Wheat Protein) 2.5 parts by weight, Zinc Gluconate 2 parts by weight, Senna Seed Polysaccharide (Cassia Angustifolia Seed Polysaccharide) 2 parts by weight, PEG-40 Hydrogenated Caster Oil (PEG-40 Hydrogenated Caster Oil) 2.5 Parts by weight, 2 parts by weight of Polyquaternium-10, 1.5 parts by weight of vegetable Coceth-7, 1 part by weight of Sodium Chloride (NaCl), 1.5 parts by weight of Oleanolic Acid Parts by weight, 2 parts by weight Linoleamidopropyl PG-dimonium chloride phosphate, 2 parts by weight Biotinoyl Tripeptide-1, 1.5 parts by weight Biotin, 1.5 parts by weight of Citric acid, 1.5 parts by weight of Nicotinic Acid Amide, 1.5 parts by weight of Dexpanthenol, 2 parts by weight of Allantoin, and 1.5 parts by weight of Cetearyryl Alcohol. It is a hypoallergenic hair shampoo raw material containing booze.

According to a more preferred feature of the present invention, the hair care raw material includes 9 parts by weight of Ammonium Laureth Sulfate, 5 parts by weight of Potassium cocoyl glycinate, and Sodium Cocoyl Apple Amino Acid ( Sodium Cocoyl Amino Acids 6 parts by weight, Stearamidopropyl Dimethylamine 9 parts by weight, Polysorbate 20 3 parts by weight, Argania Spinosa Kernel Oil 3 parts by weight, Hydrolyzed Keratin 3 parts by weight, Cyclopentasiloxane 4 parts by weight, Propylene Glycol 2 parts by weight, Ceteardimonium Chloride 3 parts by weight, dimethicone (Dimethicone) 5 parts by weight, Glutamic Acid 5 parts by weight, Sodium Chloride 1 part by weight, Oleanolic Acid 1.5 parts by weight, Linoleamidopropyl sebum-dimonium chloride phosphate (Linoleamidopropyl PG-dimonium chloride phosphate) 2 parts by weight, Glycosyl Trehalos 2 parts by weight, Biotin 0.5 parts by weight, Citric Acid 1 part by weight, D-Limonene ) 0.5 parts by weight, Tocopheryl Acetate 0.5 parts by weight, Dexpanthenol 0.5 parts by weight, Allantoin 2 parts by weight, Behenyl Alcohol 2 parts by weight, and Cetearyl Alcohol It is a hypoallergenic hair conditioner raw material containing 1.5 parts by weight of Alcohol).

According to a more preferred feature of the present invention, the hair care raw materials include 5 parts by weight of Ethanol, 2.5 parts by weight of Ethoxydiglycol, 2.5 parts by weight of Butylene Glycol, and propylene glycol. 2.5 parts by weight of Propylene Glycol, 4 parts by weight of PEG-40 Hydrogenated Caster Oil, 5 parts by weight of Argania Spinosa Kernel Oil, Tocopheryl Acetate ) 5 parts by weight, Caffeine 3 parts by weight, Salicylic Acid 3 parts by weight, Glycosyl Trehalos 3 parts by weight, Glutamic Acid 5 parts by weight, Sodium Chloride , NaCl) 0.5 parts by weight, Ammonium Chloride 0.5 parts by weight, L-Limonene 1 part by weight, Zinc Gluconate 4 parts by weight, Dimethicone 5 parts by weight, Biotin (Biotin) 2 parts by weight, Citric Acid 1 part by weight, Dexpanthenol 2 parts by weight, Allantoin 2 parts by weight, Mannitol 3 parts by weight, Dicaprylyl Carbonate ) It is a hair essence raw material containing 3 parts by weight of Senna Seed Polysaccharide (Cassia Angustifolia Seed Polysaccharide) and 4.5 parts by weight of Nicotinic Acid Amide.

Here, hair care raw materials can be formed of hair shampoo raw materials that make up hair shampoo that provides a cleaning function, hair conditioner raw materials that provide a conditioning function, and hair essence raw materials that protect and restore damaged hair or scalp.

If the hair care raw material is a hair shampoo raw material, it may be composed of a composition that constitutes a general hair shampoo, but to minimize irritation to the scalp and hair, ammonium laureth sulfate (Ammonium laureth sulfate), a hypoallergenic cleansing ingredient extracted from coconut, etc. 15 parts by weight of Laureth Sulfate, 8 parts by weight of Sodium Lauroamphoacetate, a foam-forming cleaning ingredient derived from coconut acid (cocos nucifera acid), and potassium cocoil, a vegetable natural surfactant extracted from coconut fruits. 5.5 parts by weight of glycinate (Potassium cocoyl glycinate), 5 parts by weight of Sodium Cocoyl Amino Acids, a vegetable cleaning ingredient extracted from apples, and an ethanolamide mixture of coconut acid that acts as a thickener or foam accelerator. 2.5 parts by weight of Cocamide Methyl MEA, Hydroxypropyltrimonium Hydrolyzed Wheat Protein, a hydrolyzed wheat protein that is used as a conditioning agent for hair and skin through film formation and prevents static electricity. Protein) 2.5 parts by weight, Zinc Gluconate, a zinc complex skin conditioning agent derived from natural sugar, 2 parts by weight, Cassia Angustifolia Seed Polysaccharide, a skin emollient and antioxidant derived from senna seeds, 2 parts by weight Parts by weight, 2.5 parts by weight of PEG-40 Hydrogenated Caster Oil, an emulsifying aid mixed with PEG and castor oil, Polyquaternium-, which prevents static electricity through film formation 2 parts by weight of Polyquaternium-10, 1.5 parts by weight of Coceth-7, a vegetable surfactant, 1 part by weight of Sodium Chloride (NaCl), and Oleanolic Acid, which acts as a skin conditioner. ) 1.5 parts by weight, Linoleamidopropyl PG-dimonium chloride phosphate, used as an emulsifier and antistatic agent, 2 parts by weight, biotinoyl tripeptide-1 (a peptide that produces 3 molecules of amino acid) 2 parts by weight of Biotinoyl Tripeptide-1), 1.5 parts by weight of Biotin, a type of water-soluble vitamin, 1.5 parts by weight of Citric acid, a pH adjuster extracted from citrus, a complex of water-soluble vitamins and vitamin B that protects the blood 1.5 parts by weight of Nicotinic Acid Amide, which promotes circulation, 1.5 parts by weight of Dexpanthenol, a precursor of vitamin B that treats inflammation and regenerates the skin, 2 parts by weight of Allantoin, a vegetable soothing ingredient, and coconut. It is preferable that it is a hypoallergenic hair shampoo raw material containing 1.5 parts by weight of Ceteayryl Alcohol, an emulsifier extracted from natural substances such as fat components.

In addition, when the hair care raw material is a hair conditioner raw material, it may be composed of a composition that constitutes a general hair conditioner, but to minimize irritation to the scalp and hair, ammonium laureth sulfate (ammonium laureth sulfate), a hypoallergenic cleansing ingredient extracted from coconut, etc. 9 parts by weight of Ammonium Laureth Sulfate, 5 parts by weight of potassium cocoyl glycinate, a foam-forming cleaning ingredient derived from coconut acid (cocos nucifera acid), and sodium coco, a vegetable cleaning ingredient extracted from apples. 6 parts by weight of Sodium Cocoyl Amino Acids, 9 parts by weight of Stearamidopropyl Dimethylamine, which is a fatty mineral salt that acts as a hair conditioning agent, antistatic agent and hypoallergenic surfactant, emulsifier and dissolving agent. 3 parts by weight of Polysorbate 20, which acts as an adjuvant, and 3 parts by weight of Argania Spinosa Kernel Oil, a moisturizing agent extracted from the fruit of the argan tree and rich in omega-6 and tocopherol, which protects against static electricity by forming a film. 3 parts by weight of Hydrolyzed Keratin, which prevents and acts as a conditioning agent for hair and hair, 4 parts by weight of Cyclopentasiloxane, which acts as a hair conditioning agent and skin softener, and an aliphatic alcohol that acts as a moisturizer and skin conditioning. 2 parts by weight of Propylene Glycol, which acts as an antistatic agent, 3 parts by weight of Ceteardimonium Chloride, which acts as an antistatic agent and hair conditioning agent, and dimethicone (which acts as a skin emollient, moisturizer and skin conditioning agent). Dimethicone 5 parts by weight, Glutamic Acid, an amino acid extracted from wheat starch that is effective in moisturizing the skin, 1 part by weight Sodium Chloride, Oleanolic Acid (which acts as a skin conditioner) 1.5 parts by weight of Oleanolic Acid, 2 parts by weight of Linoleamidopropyl PG-dimonium chloride phosphate, which acts as an emulsifier and antistatic agent, and Glycosyl Trehalos, a moisturizing ingredient extracted from corn. ) 2 parts by weight, 0.5 parts by weight of Biotin, a type of water-soluble vitamin, 1 part by weight of Citric Acid, a pH adjuster extracted from citrus, 0.5 parts by weight of D-Limonene, an orange oil extract ingredient. Parts by weight, vegetable antioxidant, 0.5 parts by weight of Tocopheryl Acetate, which acts as a skin conditioning agent, 0.5 parts by weight of Dexpanthenol, a precursor of vitamin B that treats inflammation and regenerates the skin, and allantoin, a vegetable soothing ingredient. (Allantoin) 2 parts by weight, a hypoallergenic product containing 2 parts by weight of Behenyl Alcohol, a hypoallergenic thickener, and 1.5 parts by weight of Cetearyl Alcohol, an emulsifier extracted from natural substances such as coconut fat. It is preferable that it is a hair conditioner raw material.

If the hair care raw material is a hair essence raw material, it may be composed of a composition that constitutes a general hair conditioner, but to minimize irritation to the scalp and hair, 5 parts by weight of ethanol, which acts as a solvent, a humectant, a fragrance, 2.5 parts by weight of Ethoxydiglycol, which acts as a solvent, 2.5 parts by weight of Butylene Glycol, which acts as a fragrance, skin conditioning agent, solvent, and humectant, and an aliphatic alcohol that acts as a preservative, skin moisturizer, and skin conditioning. 2.5 parts by weight of Propylene Glycol, which acts as a viscosity reducer, and PEG-40 Hydrogenated Caster Oil, an emulsifying aid mixed with PEG and castor oil. 4 parts by weight, Argania Spinosa Kernel Oil, a moisturizer extracted from the fruit of the argan tree and rich in omega-6 and tocopherol, 5 parts by weight, Tocopheryl Acetate, which acts as a vegetable antioxidant and skin conditioning agent. Parts by weight, 3 parts by weight caffeine, which is a plant-based active ingredient that improves blood circulation and acts as a skin conditioning agent, 3 parts by weight salicylic acid, which acts as an exfoliant and hair and skin conditioning agent, and 3 parts by weight, a moisturizing ingredient extracted from corn. 3 parts by weight of Glycosyl Trehalos, 5 parts by weight of Glutamic Acid, an amino acid extracted from wheat starch that is effective in moisturizing the skin, 0.5 parts by weight of Sodium Chloride (NaCl), pH 0.5 parts by weight of Ammonium Chloride, an alkaline salt used for conditioning, 1 part by weight of L-Liminene, an essential oil extracted from peppermint oil, and zinc gluconate, a zinc complex skin conditioning agent derived from natural sugar. (Zinc Gluconate) 4 parts by weight, Dimethicone, which acts as a skin softener, moisturizer and skin conditioning agent, 5 parts by weight, Biotin, a type of water-soluble vitamin, 2 parts by weight, Citric Acid, a pH adjuster extracted from citrus (Citric Acid) 1 part by weight, Dexpanthenol, a precursor of vitamin B that treats inflammation and regenerates the skin, 2 parts by weight, Allantoin, a vegetable soothing ingredient, 2 parts by weight, mannitol, a plant extract with antioxidant properties (Mannitol) 3 parts by weight, Dicaprylyl Carbonate (Docaprylyl Carbonate) 3 parts by weight, Senna Seed Polysaccharide (Cassia Angustifolia Seed Polysaccharide), a skin emollient and antioxidant derived from senna seeds, 3 parts by weight, and water-soluble vitamins and vitamin B. It is preferable that the hair essence raw material contains 4.5 parts by weight of Nicotinic Acid Amide, which promotes blood circulation as a complex of.

According to one embodiment of the present invention, the hair care composition containing the hair has a moisturizing effect, an anti-static effect on the hair, an anti-splitting effect on the hair, a softening effect, a strong antibacterial effect against dandruff bacteria, and an effect on excessive production of sebum. We provide hair care products that have anti-itching, anti-dandruff and hair loss prevention effects.

The hair care products include hair conditioner, hair tonic, hair cream, hair lotion, hair face, hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol spray, and aerosol. It can be mousse, aerosol spray, perm, bleach, hair dye, ampoule, shampoo or rinse.

According to one embodiment of the present invention, the hair care composition may further include 2 to 8 parts by weight of natural fragrance extract.

The natural fragrance extracts include aloe vera leaf extract, lavender leaf extract, lavender flower extract, calendula flower extract, guava leaf extract, green tea leaf extract, honeysuckle flower extract, jojoba extract, rosemary leaf extract, Lilium Madonna flower extract, and mistletoe leaf. Composed of extract, evening primrose seed extract, safflower extract, lotus extract, citron peel extract, prickly pear flower extract, olive leaf extract, eucaritus extract, chamomile extract, jojoba seed oil, tangerine peel oil, lime oil, rose oil and olive oil. This is done by selecting one or more of the groups.

As such, the hair care composition containing the natural plant mixture according to the present invention has hair loss prevention and hair growth effects, as well as a hair moisturizing effect, an anti-static effect on the hair, an anti-splitting effect on the hair, and a strong antibacterial effect against dandruff bacteria. Therefore, the hair care composition containing the natural plant mixture according to the present invention can simultaneously improve both the scalp and hair, and can be used in functional hair care products such as hair conditioner, hair tonic, hair cream, hair lotion, and hair face. , hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol spray, aerosol mousse, aerosol spray, perm, bleach, dye, ampoule, shampoo or rinse, etc. can be used

Hereinafter, to aid understanding of the present invention, it will be described in detail through examples. However, the embodiments according to the present invention may be modified into various other forms, and the scope of the present invention should not be construed as being limited to the following embodiments. Embodiments of the present invention are provided to more completely explain the present invention to those skilled in the art.

<Preparation Example 1> Preparation of natural plant extract

1 kg of each natural material was placed in purified water and subjected to hot water extraction at 100°C for 1 hour to obtain extracts of horsetail, sorghum, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica, and rosemary. Each of the above extracts was filtered under reduced pressure with Advantec No. 2 (110 mm) filter paper to remove insoluble substances, and then concentrated under reduced pressure at 40°C using a concentrator equipped with a cooling condenser. In order to completely remove the solvent from the extract concentrated under reduced pressure, 0.5 liters of purified water was added to suspend it, and then extracts of horsetail, sorghum, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica, and rosemary were obtained using a freeze dryer.

<Preparation Example 2> Production of natural plant fermentation product

Lactobacillus plantarum ( L.plantarum ) was added to 100 parts by weight of each horsetail, sorghum, nettle, pumpkin seed, tomato, sorghum, linseed, centella asiatica and rosemary extract obtained in Preparation Example 1, at an amount of 1 to 1 to 100 grams of the aged liquid. It was inoculated at an amount of 5 million CFU and fermented at a temperature of 35 to 40°C for 1 to 3 days to prepare fermented products of horsetail, sorghum, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica, and rosemary.

Subsequently, the prepared coffee waste fermentation was sterilized by heating at a temperature of 90° C. for 15 minutes.

<Example 1> Preparation of hair shampoo containing natural plant extracts

A hair shampoo was prepared containing mixed natural plant extracts including 20 mg of horsetail extract, 20 mg of hawthorn extract, 10 mg of nettle extract, 30 mg of pumpkin seed extract, 30 mg of tomato extract, 10 mg of sorghum extract, 30 mg of flax seed extract, 20 mg of centella asiatica extract, and 30 mg of rosemary extract. .

<Example 2> Preparation of hair shampoo containing fermented natural plants

A natural plant blend containing 20mg horsetail fermentation, 20mg horsetail fermentation, 10mg nettle fermentation, 30mg pumpkin seed fermentation, 30mg tomato fermentation, 10mg sorghum fermentation, 30mg flax seed fermentation, 20mg centella asiatica fermentation, and 30mg rosemary fermentation. A hair shampoo containing the ferment was prepared.

<Comparative Example 1>

A commercially available anti-hair loss hair shampoo was used.

<Comparative Example 2>

A commercially available general hair shampoo was used.

<Test Example 1> Evaluation of hair improvement and hair loss prevention effects

For the sensory evaluation, a total of 60 people (15 from each age group from 20s to 50s) were divided into 4 groups, and once every evening, the hair shampoo containing the natural plant mixture of Examples 1 and 2 and Comparative Examples 1 and 2 were used in the usual manner. Washed using shampoo 2. After 3 months, the hair moisturizing effect, hair anti-static effect, hair split prevention effect, hair loss prevention effect, and refreshing feeling after shampooing were tested. For each evaluation item, the highest excellent condition was evaluated as 10 points, the average condition as 5 points, and the poor condition as 0 points.

hair moisturizing anti static Prevent cracking Prevent hair loss refreshing feeling Example 1 10 10 10 10 10 Example 2 10 10 10 10 10 Comparative Example 1 3 3 3 5 6 Comparative Example 2 One One One One 3

As shown in Table 1, the hair shampoo containing the natural plant mixture of the present invention has a moisturizing effect on the hair, an anti-static effect on the hair, an anti-splitting effect on the hair, compared to the shampoos of Comparative Examples 1 and 2 that do not contain a natural plant mixture. It was confirmed that the hair loss prevention effect and the refreshing feeling after shampooing were evaluated very well.

<Test Example 2> Evaluation of hair growth effect, hair nutrition effect, anti-dandruff effect, and itching removal effect

The hair shampoo containing the natural plant mixture prepared in the present invention was tested for hair growth effect, hair nutrition effect, anti-dandruff effect, and itching removal effect by the following method.

60 people with dandruff and itchy scalp were divided into 6 groups and washed once every evening in the usual manner using the hair shampoo containing the natural plant mixture of Examples 1 and 2 and the shampoo of Comparative Examples 1 and 2. . Dandruff and scalp itchiness were evaluated after 3 months, and the results are shown in Table 2 below.

In the above evaluation, in the case of hair growth, if there are hair growth symptoms on the entire head and an increase in the number of hairs, it is 'very good'; if there are hair growth symptoms on a part of the head and there is an increase in the number of hairs in a part of the head, 'good', hair growth If there were no symptoms, it was rated as 'no change'; in the case of hair nutrition, if the hair was almost completely damaged and smooth and abundant overall, it was rated as 'very good'; if the hair damage was limited to a few areas and the hair was smooth, it was rated as 'good'. ', if there was no improvement in hair condition before use, it was rated as 'no change'; in case of scalp condition, if it had the effect of reducing dandruff on the entire head, it was 'very good'; if it had the effect of reducing dandruff in a part of the head, it was rated as 'good'. If there was no reduction effect, it was rated as 'no change'; if sebum disappeared from the entire scalp, there was no itching, and the scalp was clean, it was rated as 'very good'; if sebum or itching was partially improved and the cleanliness improved, it was rated as 'good'. , If there was no change in the condition of the scalp before use, it was rated as ‘no change’.

hair growth effect hair nutrition Anti-dandruff anti-itch Example 1 Very good 8 9 9 10 good 2 One One 0 No change 0 0 0 0 Example 2 Very good 9 9 9 10 good 2 One One 0 No change 0 0 0 0 Comparative Example 1 Very good 0 0 0 0 good 3 2 2 One No change 7 8 8 9 Comparative Example 2 Very good 0 0 0 0 good 0 4 3 2 No change 10 6 7 8

As can be seen in Table 2 above, when the hair shampoo containing the natural plant mixture prepared in the present invention was continuously used, not only did all users have anti-dandruff and anti-itching effects, but it also had the effect of thickening fine hair or fine hair. . In addition, there was a good change in the hair nutritional status in most cases, and for those who had dandruff and itching, dandruff and itching were completely resolved, and it was confirmed that the scalp condition was mostly improved.

<Test Example 3> Hair growth promotion efficacy analysis

The hair growth effect through cell proliferation was confirmed in the hair shampoo containing the natural plant mixture of Examples 1 and 2 and the shampoo of Comparative Examples 1 and 2.

Human hair follicle dermal papilla cells (hair papilla cells, DP cells) were purchased from Cell Bio, and low glucose DMEM medium supplemented with 10% FBS (fetal bovine serum) and 1% penicillin was used as a culture medium at 37°C in a CO ₂ incubator. It was cultured in .

The DP cell suspension was added to a 96-well plate at an appropriate concentration, and then stabilized in an incubator for 24 hours. Then, the hair shampoo containing the natural plant mixture of Examples 1 and 2 and the shampoo of Comparative Examples 1 and 2 were added at a concentration of 2 μg/ml each. They were treated with sheep and cultured for 48 hours. After 48 hours, the media was removed and washed with PBS. Dispense 100 ㎕ of the MTT solution dissolved in PBS at a concentration of 1 mg/㎖ and incubate in an incubator at 37°C for 4 hours. Then, remove the supernatant and add 200 ㎕ DMSO to completely dissolve formazan using an ELISA plate reader. The OD value was measured at 540 nm.

The statistical significance of the test scores was expressed as mean ± standard deviation, and the difference between each group was analyzed using the SPSS 25 (SPSS Inc. USA) program, and significance was analyzed by performing post-hoc tests using ANOVA and Duncan tests. If P<0.05 or less, it was recognized as significant. Each experiment was performed at least three times and statistically processed, and the proliferation rate (%) of dermal papilla cells is shown in Table 3 below.

Dermal papilla cell proliferation rate (%) DMSO 100.00±0.00 minoxidil 105.14±0.22 Example 1 107.13±0.01 Example 2 108.11±0.22 Comparative Example 1 101.11±0.22 Comparative Example 2 100.01±0.28

As shown in Table 3, compared to the control group which was 100.00±0.00%, the minoxidil (MNXD) group as a positive control group increased to 105.14±0.22%, and while Comparative Examples 1 and 2 showed a slight effect, the practice of the present invention In Examples 1 and 2, it can be seen that the dermal papilla cell proliferation rate was significantly increased to 107.13 ± 0.01 and 108.11 ± 0.22.

<Test Example 4> Analysis of hair growth promotion effect

Criteria for test subject selection: Men and women diagnosed with androgenetic alopecia aged 18 to 54 years, according to the Basic and Specific (BASP) classification, the basic type is M2 or higher, C2 or higher, or U1 or higher, and the specific type is V1 or higher or F1 or higher. The subjects were male and female androgenic alopecia patients, male patients diagnosed with grade 3 or higher according to the Orwood-Hamilton classification, or female patients diagnosed with grade 3 or higher according to the Ludwig classification.

Equipment used: (1) Folliscope ^ⓡ (a computer equipped with a high-resolution color video imaging device (video microscopic camera) and separate folliscope software Phototrichogram) can be used to analyze the main characteristics of hair, such as density, thickness, and growth speed. system equipment), (2) digital camera Canon EOD 750D) (used when taking clinical pictures and attached to a fixed holder to enable taking pictures of the subject's crown and hairline at the same angle and position).

Test procedure: 2 weeks before the start of the test, test subjects were judged, consented wash out products were issued, dot tattoos were performed on the test area, phototricograms were performed focusing on the dot tattoos, and photographs were taken. At the 10th and 20th weeks of testing, 20 weeks worth of test samples were issued after visual evaluation, stability evaluation, and questionnaire evaluation through folliscope operation and photography.

Table 4 below shows the average number of hairs after 10 and 20 weeks of testing.

0 parking Week 10 Week 20 Example 1 78.62±11.91 87.35±12.68 98.38±10.24 Example 2 78.61±10.36 87.23±11.23 99.12±11.63 Comparative Example 1 78.43±10.02 82.21±02.31 83.21±08.15 Comparative Example 2 78.25±10.27 80.25±11.35 80.73±12.41

As shown in Table 4, for the shampoo containing natural plant extract of Example 1, the ratio was 78.62 at week 0, 87.35 at week 10, and 98.38 at week 20, and for the shampoo containing fermented natural plant material of Example 2, the ratio was 78.61 at week 0, 10. The number of hairs increased at a statistically significant level (p<005), such as 87.23 at week 1 and 99.12 at week 20. On the other hand, in the case of Comparative Examples 1 and 2, statistically significant differences (p<005) could not be confirmed at weeks 0, 10, and 20.

<Test Example 5> Formulation stability test

A formulation stability test was performed on the hair shampoo containing the natural plant mixture of Examples 1 and 2.

The observation period was the same for one week, and stability was observed at various temperatures, and the results are shown in Table 5 below.

temperature 0℃ 40℃ -10℃ Example 1 Good Good Good Example 2 Good Good Good

As shown in Table 5, it was confirmed that the hair shampoo containing the natural plant mixture of Examples 1 and 2 had good stability at various temperatures.

<Test Example 6> Human safety confirmation experiment

In order to confirm whether the hair care composition of the present invention is safe for human skin, a skin safety verification experiment was performed. For this purpose, a skin cumulative irritation test was conducted. A formulation was prepared using squalene as a base and adding 1% of each hair shampoo containing the natural plant mixture of Examples 1 and 2, and using this formulation, applied to the upper forearm area of 20 healthy adults every other day for a total of 9 times for 24 hours. A patch was applied to determine whether the hair care composition of the present invention irritated the skin. The patch method used a Finn chamber (Epitest Ltd, Finland). After dropping 15 ㎕ of each skin external preparation into the chamber, a patch was applied. The degree of reaction that appeared on the skin each time was scored using Equation 2 below, and the results are shown in Table 6 below.

In reactivity, ± is given a score of 1 point, + is 2 points, and ++ is given a score of 4 points, and when the average reactivity is less than 3, the composition is judged to be safe.

test substance Number of subjects who responded average
Responsiveness 1 week 2 weeks 3 weeks Primary Secondary 3rd 4th 5th 6th 7th 8th 9th ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ ±＋ ＋＋ control group
(squalene) One - - 0 - - - - - - - - - - - - - - - - - - - - - - - 0.09 [Test group 1] 0 - - 0 - - - - - - - - - - - - - - - - - - - - - - - 0.00

In Table 6 above, the number of people in test group 1 corresponding to ±, +, and ++ was 0, 0, and 1, respectively, and the average reactivity was 0.00 and 0.00, respectively. Therefore, since the average reactivity was less than 3, the hair care composition according to the present invention was determined to be safe for human skin without showing a clear cumulative irritation pattern.

Below are examples of formulations for the composition of the present invention.

<Formulation Example 1> Hair shampoo production

A hair shampoo containing a hair care composition having the composition shown in Table 7 below was prepared.

Ingredient name content(%) Purified water 45.75 Polyquaternium-10 0.20 carbomer 0.15 Disodium Cocoamphodiacetate 2.00 Sodium Laureth Sulfate 10.00 Lauryl Hydroxylsteine 2.00 cetyl alcohol 0.50 Disodium EDTA 0.05 Trihydroxystearin 0.05 Polyquaternium-7 0.30 Cocamide Methyl MEA 2.50 Phenoxyethanol 0.50 caprylyl glycol 0.10 Spices 0.70 Hair care composition of Example 1 35.20

<Formulation example 2> Hair treatment manufacturing

A hair treatment containing a hair care composition having the composition shown in Table 8 below was prepared.

Ingredient name content(%) Purified water 39.40 Trehalose 1.00 Hydroxyethylcellulose 0.30 glycerin 3.00 Cetrimonium chloride 0.20 behentrimonium chloride 2.40 isopropyl alcohol 0.60 propylene glycol 1.10 steartrimonium chloride 1.50 cetyl alcohol 5.00 Behenyl alcohol 1.00 Butylene Glycol Dicaprylate/Dicaprate 6.00 dimethicone 2.00 Hair care composition of Example 1 35.50 Spices 0.50 Propanediol 0.40 caprylyl glycol 0.08 Ethylhexylglycerin 0.02

As the specific parts of the present invention have been described in detail above, it is clear to those skilled in the art that these specific techniques are merely preferred embodiments and do not limit the scope of the present invention. Accordingly, the substantial scope of the present invention will be defined by the appended claims and their equivalents.

Claims (7)

Contains a mixture of horsetail, horsetail, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica and rosemary as active ingredients,
The mixture contains 90 to 110 parts by weight of horsetail, 40 to 60 parts by weight of nettle, 140 to 160 parts by weight of pumpkin seeds, 140 to 160 parts by weight of tomatoes, 40 to 60 parts by weight of sorghum, and 140 to 160 parts by weight of flax seeds. , 90 to 110 parts by weight of centella asiatica and 140 to 160 parts by weight of rosemary are mixed,
The horsetail, horsetail, nettle, pumpkin seed, tomato, sorghum, flax seed, centella asiatica, and rosemary are each extract or fermented product,
The mixture is included in an amount of 0.5 to 10% by weight based on the total weight of the hair care composition,
The extract is obtained by freeze-drying and pulverizing natural plants, performing hot water extraction for 50 to 70 minutes using purified water at 90 to 110°C, followed by filtration and concentration under reduced pressure,
The fermented product is a hair care composition prepared by freeze-drying and pulverizing a natural plant, hot-water extracting it for 50-70 minutes using purified water at 90-110°C, and then fermenting 100 parts by weight of the hot-water extract using fermentation bacteria. .
According to paragraph 1,
A hair care composition characterized in that the fermentation bacteria use a mixed strain obtained by selecting one strain from each of lactic acid bacteria, Bacillus bacteria, and yeast bacteria and mixing them at a weight ratio of 2:2:1.
delete delete delete delete According to claim 1 or 2,
The hair care composition includes hair conditioner, hair tonic, hair cream, hair lotion, hair face, hair gel, hair pack, hair massage, hair liquid, hair spray, hair mousse, treatment, non-aerosol mousse, non-aerosol spray, aerosol. A hair care composition characterized as a mousse, aerosol spray, perm, bleach, dye, ampoule, shampoo or rinse.