KR102590504B1 - An ecofriendly Anti-biotic deodorizaton composition manufactured by distillation of natural materials - Google Patents

Abstract

The antibacterial disinfectant and deodorant composition of the present invention is a distillation method of cinnamon, ginkgo leaves, honeysuckle, licorice, pine needles, and oak leaves. The distillate is a clear, fugitive liquid that not only leaves no sediment and has excellent deodorizing ability, but also inhibits the growth of microorganisms. It has an antibacterial effect that inhibits or sterilizes.
Therefore, the sterilizing and deodorizing composition of the present invention uses distillate obtained only from eco-friendly natural materials, so it is not harmful to the human body even when used on tables, sinks, and refrigerators at home, and can be used as a hand sanitizer for offices or bathrooms as well as for pets. It has an excellent deodorizing effect, is harmless, and is eco-friendly and can be used in various fields related to people's lives, such as deodorization, food, water treatment, living, and hygiene.

Description

An eco-friendly anti-biotic deodorizaton composition manufactured by distillation of natural materials}

The present invention relates to an eco-friendly sterilizing and deodorizing composition manufactured by a distillation method of natural materials. More specifically, the antibacterial and deodorizing effects of pure natural materials consisting of cinnamon, licorice, honeysuckle, ginkgo leaves, pine needles, and oak leaves extracted through a distillation method. It relates to an eco-friendly sterilizing and deodorizing composition manufactured by a distillation method from natural materials that are excellent and harmless to the human body.

In general, deodorants are used in a variety of ways at home or in office spaces in a sprayable form. Since they are used in places close to animals or people, they must not be harmful to people or animals when they come in contact with eyes or skin.

Therefore, as a raw material with excellent deodorizing performance and excellent sterilizing effect, the development of a nature-friendly material that has a strong sterilizing effect while maintaining long-term deodorizing performance in native plants and is harmless to humans or animals is being promoted.

For example, in Republic of Korea Patent No. 10-0780087, an eco-friendly deodorant using wood vinegar and natural plant materials increases deodorization efficiency and prevents destruction of the natural environment when spraying a liquid deodorant. A deodorizing agent that allows this is known.

However, if these deodorants are made from natural product extracts, they may stain or remain as sediment when sprayed on office spaces or personal clothes, making continuous use difficult.

Meanwhile, odor components include hydrogen sulfide, methyl mercaptan, etc., and since these components are generated during microbial decomposition of organic matter, it is desirable to include components that have a sterilizing effect on such microorganisms. In addition, the distillation method requires the distillate to be a fugitive, clear liquid that does not leave sediment.

Accordingly, the present inventors have continued to conduct research to solve the above-mentioned problems and develop an eco-friendly deodorant that can efficiently remove bad odors due to its fast decomposition ability and speed for odors and contaminants and the ability to sterilize microorganisms. The distillate of cinnamon, ginkgo leaves, honeysuckle, licorice, pine needles, and oak leaves obtained through heavy distillation is a clear liquid that not only has antibacterial activity to suppress or sterilize the growth of microorganisms, but also has excellent deodorizing ability against bad odors. The present invention was completed by discovering that it has.

Therefore, the technical problem to be solved by the present invention is to provide a sterilizing and deodorizing composition with excellent antibacterial disinfection and deodorizing effects using natural materials.

In order to solve the above technical problems, the present invention provides an antibacterial disinfectant and deodorant composition obtained by distilling cinnamon, ginkgo leaves, honeysuckle, licorice, pine needles, and oak leaves.

(S1) With respect to 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of honeysuckle, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, and 600 to 650 parts by weight of oak leaves are mixed to prepare a herbal medicine mixture. manufacturing step;

(S2) immersing the herbal medicine mixture obtained in step (S1) in water and performing primary extraction at 40 to 60° C. for 1 to 2 hours;

(S3) performing secondary extraction of the herbal medicine extract primarily extracted in step (S2) at 130 to 150° C. for 5 to 10 hours and condensing the resulting vapor with a cooler to obtain a distillate; and

(S4) Aging the distillate obtained in step (S3) at room temperature for 1 to 2 days to obtain an antibacterial disinfectant and deodorant composition.

In addition, the present invention provides an environmentally friendly antibacterial disinfectant and deodorant obtained by the above manufacturing method.

As such, the antibacterial disinfectant and deodorant composition of the present invention is a distillation method of cinnamon, ginkgo leaves, honeysuckle, licorice, pine needles, and oak leaves, and the distillate is a fugitive, clear liquid that not only leaves no sediment and has excellent deodorizing ability, but also protects against microorganisms. It has antibacterial activity that inhibits the growth of or sterilizes.

Therefore, the deodorant composition of the present invention is not harmful to the human body even when used on tables, sinks, and refrigerators at home, and can be used as a hand sanitizer for offices or bathrooms. It is also excellent and harmless for pets, and is environmentally friendly. It can be used in various fields related to people's lives, such as food, water treatment, living, and hygiene.

Figure 1 is a process diagram for manufacturing the antibacterial disinfectant and deodorant of the present invention.
Figure 2 is an example of a distillation cooling device for manufacturing the antibacterial disinfectant and deodorant of the present invention.
Figure 3 is a cotton cloth for wrapping mixed herbal medicine and immersing it in water to produce the antibacterial disinfectant and deodorant of the present invention.

Hereinafter, to aid understanding of the present invention, it will be described in detail through examples. However, the embodiments according to the present invention may be modified into various other forms, and the scope of the present invention should not be construed as being limited to the following embodiments. Embodiments of the present invention are provided to more completely explain the present invention to those skilled in the art.

In the present invention, there is a method for producing an antibacterial disinfectant and deodorant composition obtained by distilling cinnamon, licorice, honeysuckle, ginkgo leaves, pine needles, and oak leaves. (S1) For 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, and 50 to 100 parts by weight of honeysuckle. Preparing a herbal medicine mixture by mixing 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, and 600 to 650 parts by weight of oak leaves; (S2) immersing the herbal medicine mixture obtained in step (S1) in water and performing primary extraction at 40 to 60° C. for 1 to 2 hours; (S3) the herbal medicine extract primarily extracted in step (S2) Condensing the vapor generated by secondary extraction at 130 to 150°C for 5 to 10 hours with a distillation cooler to obtain a distillate; and (S4) the distillate obtained in step (S3) is aged at room temperature for 1 to 2 days to obtain an antibacterial disinfectant and deodorant composition.

The materials used in the present invention are herbal medicine and herbal medicine materials and natural materials that can be easily obtained in the mountains and fields of Korea, such as ginkgo leaves, pine needles, and oak leaves, and a method of obtaining a clear distillate by heating them in distilled water at high temperature and distilling them is used. do. The herbal medicine extract first extracted in (S2) is subjected to hot water extraction at a high temperature of 130 to 150°C, and the high-temperature steam is sent to a distillation cooler to improve extraction of the active ingredient, and the active ingredient is sent along with the high-temperature steam to increase the content of the active ingredient. Raise it to obtain distillate.

Cinnamon, the active ingredient of the deodorant composition of the present invention, is a medicinal material made from the bark of Cinnamomum japonicum SIEB., an evergreen tree belonging to the Lauraceae family. The taste of the medicine is spicy and sweet, and its medicinal properties are recessive, causing nasogastric problems. It activates function and stops paralysis and pain, and is widely applied to neuralgia and joint diseases that cause cold and sore back and knees. Recently, it has been attracting attention due to its excellent effect in suppressing skin fungi.

The licorice of the present invention is effective in detoxification, hepatitis, urticaria, dermatitis, eczema, etc., and harmonizes the toxicity of all drugs to enhance the efficacy of the drug.

Honeysuckle, the active ingredient in the deodorant composition of the present invention, is a semi-evergreen broad-leafed vine that grows wild in mountains and fields across the country, and its flowers change color from white to yellow, so it is also called ‘golden flower.’ Honeysuckle has antipyretic, detoxifying, antibacterial, antiviral, antifungal, anti-inflammatory, astringent, and diuretic effects, promotes the phagocytosis of white blood cells, relieves spasms in the small intestine, and inhibits the growth of Bacillus subtilis and Staphylococcus aureus.

Ginkgo biloba, the active ingredient of the deodorant composition of the present invention, is a deciduous tree native to the Korean Peninsula and Manchuria, and is taxonomically a germinal plant. Ginkgo biloba is a coniferous tree. In particular, ginkgolide, a flavonoid glycoside and terpene compound contained in the extract of ginkgo biloba, affects peripheral nerves. It has been found to expand and activate neurotransmitters, and is known to have excellent antibacterial and anti-inflammatory effects.

Pine needles, the active ingredient of the deodorant composition of the present invention, refer to the leaves of pine trees, a coniferous tree that grows in the mountains and fields of Korea, and contain phytoncide components, such as 'terpenes' and 'alkaloids', and are known to exhibit strong antibacterial activity. .

Quercus, which is the active ingredient of the deodorant composition of the present invention, does not refer to any one species, but is a name that refers to several tree species belonging to the Quercus family and Quercus genus. In particular, the leaves of Quercus and Quercus, which are abundant in the mountains and fields of Korea, are prone to rot and decay. It is known to have a strong antibacterial effect against microorganisms involved in deterioration.

As shown in Figure 1, the manufacturing step of the deodorant composition of the present invention (S1) is 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of honeysuckle, 100 to 150 parts by weight of ginkgo leaves, and 200 parts by weight of pine needles, based on 100 parts by weight of cinnamon. This is a step of mixing 300 to 300 parts by weight and 600 to 650 parts by weight of oak.

In the method for producing the deodorant composition of the present invention, step (S2) involves wrapping the mixed herbal medicine and material in a cotton cloth (see Figure 3) and immersing it in water, that is, distilled water or bottled water, at 40 to 60 ° C. for 1 to 2 hours. During the extraction step, water sufficiently penetrates the material and helps to leach out the active substances. At this time, the first extraction can be performed in a triple pot as shown at the bottom of Figure 2.

In the production method of the present invention, step (S3) is a step of obtaining a clear distillate by condensing the vapor generated by performing secondary extraction of the primarily extracted extract at 130 to 150° C. for 5 to 10 hours in a distillation cooler. The extraction rate of the active ingredient is increased, and the medicinal ingredient along with the dormant ingredient is transferred to a distillation cooler equipped with a water-cooled cooler installed at the top along with high-temperature steam, and the polymer residue remains. This high-temperature heating is preferably done in a triple pot with a paraffin layer inserted. At this time, the reason for heating in a triple pot with a paraffin layer is to prevent the pot from overheating above 150℃ and to prevent the herbal medicines that have settled at the bottom from sticking and causing off-flavors. The distillation cooler used at this time is as shown in Figure 2.

In the method for producing the deodorant composition of the present invention, step (S4) is a step of maturing the distillate obtained above at room temperature for 1 to 2 days, so that the overall components are homogeneous and stabilized at room temperature.

The sterilizing and deodorizing composition of the present invention may contain additional ingredients that can increase the sterilizing and deodorizing effect, and there is no particular limitation on the types thereof. For example, the concentration can be adjusted by adding water to the sterilizing and deodorizing composition of the present invention, and the sterilizing effect can be increased by mixing 1 to 5 parts by weight of hypochlorous acid water.

The deodorant composition of the present invention can be prepared in spray form or lotion form, and there is no particular limitation on the form of the formulation.

Additionally, the present invention provides a method for purifying indoor or outdoor air using the eco-friendly deodorant composition.

<Example 1>

As selected ingredients, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of honeysuckle, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, and 600 to 650 parts by weight of oak leaves were mixed with 100 parts by weight of cinnamon.

The herbal medicine mixed as above was wrapped in a cotton cloth and immersed in 100 liters of water for primary extraction at a temperature of 50°C for 2 hours. Next, the extract was placed in a triple pot equipped with a water-cooled cooler at the top and a paraffin layer inserted in the middle, and secondary extraction was performed at a temperature of 140°C for 8 hours, and the heated vapor was condensed in the cooler to obtain 50 kg of clear distillate. The obtained distillate was aged at room temperature for 1 to 2 days.

<Test Example 1>

After putting 20ml of the sterilizing deodorant prepared in the example into a 5L-sized reactor and sealing it, the initial concentration of the test gas was injected to 50μmol/mol, and the concentration of the test gas was adjusted at 0, 30 minutes, 60 minutes, 90 minutes, and 120 minutes. It was measured, and the resulting value is called the sample concentration.

At this time, the test gases were ammonia, trimethylamine, hydrogen sulfide, and methyl mercaptan.

At this time, the concentration of the test gas was measured by a gas detection tube (formerly KS I 2218:2009), and the temperature was maintained at (23.5±5.0)℃ and humidity at (50±10)%R.H. during the test.

In addition, the concentration was measured under the same conditions without adding a sterilizing or deodorizing agent, and this is called the blank concentration.

The deodorization rate of the test gas for each time period was calculated using Equation 1 below.

[Equation 1]

Deodorization rate of test gas (%)=[{(blank concentration)-(sample concentration)/(blank concentration)}]×100

Test Items unit Test result Blank concentration
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(ammonia) 0 minutes % 50 50 0.0 30 minutes % 49 One 98.0 60 minutes % 49 One 98.0 90 minutes % 49 One 98.0 120 minutes % 49 <0.2 99.6

Test Items unit Test result Blank concentration
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(trimethylamine) 0 minutes % 50 50 0.0 30 minutes % 49 2 95.9 60 minutes % 49 2 95.9 90 minutes % 49 One 98.0 120 minutes % 49 One 98.0

Test Items unit Test result Blank concentration
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(hydrogen sulfide) 0 minutes % 50 50 0.0 30 minutes % 49 <0.1 99.8 60 minutes % 49 <0.1 99.8 90 minutes % 49 <0.1 99.8 120 minutes % 49 <0.1 99.8

Test Items unit Test result Blank concentration
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(methyl mercaptan) 0 minutes % 50 50 0.0 30 minutes % 49 <0.1 99.8 60 minutes % 49 <0.1 99.8 90 minutes % 49 <0.1 99.8 120 minutes % 49 <0.1 99.8

<Test Example 2> The antifungal activity effect of the antibacterial disinfectant and deodorant prepared in Examples was measured at each concentration, 1000㎍/㎖, 800㎍/㎖, 500㎍/㎖, 300㎍/㎖, 100㎍/㎖, 50㎍/㎖. After treatment by spraying at a concentration of ㎖, the actual antifungal power was confirmed by comparing it with the untreated group from 1 to 10 days, and the following results were obtained.

Antifungal effect of this extract when treated directly on fungal culture samples Date/Concentration Gray mold fungus note 1000 800 500 300 100 50 1 day ○ ○ ○ - - - Confirmation of sterilizing power 2 days ○ ○ ○ ○ ○ - 5 days ○ ○ ○ ○ ○ - 7 days ○ ○ ○ ○ ○ ○ ○ 10 days ○ ○ ○ ○ ○ ○ ○

Therefore, the antibacterial disinfectant and deodorant of the present invention can be confirmed to have high sterilizing power, so the deodorant of the present invention can be suitable for manufacturing a deodorant that is environmentally friendly and has a sterilizing function while maximizing the deodorizing function. Above, the specific details of the present invention Having described the parts in detail, it will be clear to those skilled in the art that these specific techniques are merely preferred embodiments and do not limit the scope of the present invention thereby. Accordingly, the actual scope of the present invention will be defined by the appended claims and their equivalents.

Claims (1)

An eco-friendly sterilizing and deodorizing composition manufactured by a distillation method of natural materials comprising the following steps:
(S1) For 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of honeysuckle, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, and 600 to 650 parts by weight of oak are wrapped in cotton cloth to make a herbal medicine mixture. manufacturing step;
(S2) immersing the herbal medicine mixture contained in the cotton cloth obtained in step (S1) in water and performing primary extraction at 40 to 60° C. for 1 to 2 hours;
(S3) The herbal medicine extract primarily extracted in step (S2) is secondarily extracted at 130 to 150°C for 5 to 10 hours in a triple pot with a paraffin layer inserted in the middle, and the resulting vapor is sent to a cooler and condensed to produce a distillate. Obtaining a;
(S4) obtaining an environmentally friendly sterilizing and deodorizing composition by maturing the distillate obtained in step (S3) at room temperature for 1 to 2 days; and
(S5) adding 1 to 5 parts by weight of hypochlorous acid water to the composition obtained in step (S4) to increase the sterilizing effect and prepare a sterilizing deodorant that can be used in spray form;