KR20220123598A - An ecofriendly Anti-biotic deodorizaton composition manufactured by distillation of natural materials - Google Patents

Abstract

An antibacterial disinfectant and deodorant composition of the present invention is manufactured by a distillation method of cinnamon, ginkgo leaves, Lonicera japonica, Glycyrrhiza uralensis Fischer, pine needles, and oak leaves such that distillate is a clear volatile liquid and provides excellent deodorizing ability without leaving a precipitate, and also provides antibacterial activity of inhibiting growth of microorganisms or killing the microorganisms. Accordingly, the antibacterial disinfectant and deodorant composition uses a distillate obtained by using only eco-friendly natural materials, thereby being not harmful to the human body even when used in a table, sink, or refrigerator at home, being used as a hand sanitizer for offices or bathrooms, providing excellent harmless deodorizing effect for pets, and being eco-friendly to be used in various fields related to people's lives such as deodorization, food, water treatment, living, hygiene, etc. The antibacterial disinfectant and deodorant composition is manufactured by a step of preparing an herbal medicine mixture; a primary extraction step; a step of obtaining a distillate; and a step of obtaining an eco-friendly disinfectant and deodorant composition.

Description

An ecofriendly Anti-biotic deodorizaton composition manufactured by distillation of natural materials

The present invention relates to an eco-friendly sterilizing and deodorizing composition prepared by a distillation method of natural materials, and more specifically, an antibacterial action and deodorizing effect obtained by extracting a pure natural material consisting of cinnamon, licorice, phosphorus, ginkgo leaves, pine needles, and oak leaves by distillation. It relates to an environmentally friendly sterilizing and deodorizing composition prepared by a distillation method of natural materials that are excellent and harmless to the human body.

In general, deodorants are used in various ways at home or office space in a sprayable form. Since they are used in places close to animals or people, they should not be harmful to people or animals when they come into contact with eyes or skin.

Therefore, as a raw material with excellent deodorization performance and sterilization effect, the deodorization performance is maintained for a long time in native plants, and the development of a nature-friendly material that has a strong sterilization effect and does not harm the human body or animals is being promoted.

For example, in Korean Patent No. 10-0780087, it is possible to increase the efficiency of deodorization by an eco-friendly deodorant using wood vinegar and natural plant materials, and to prevent the destruction of the natural environment when liquid deodorant is sprayed. A deodorizing material is known.

However, when these deodorants are manufactured with natural product extracts, there is a problem that continuous use is difficult because stains or deposits may occur when sprayed on office space or personal clothes.

On the other hand, odor components include hydrogen sulfide, methyl mercaptan, and the like. Since these components are generated during microbial decomposition of organic matter, it is preferable to include a component having a bactericidal effect on these microorganisms. In addition, the distillation method is required to have a characteristic that does not leave a precipitate as a volatile, clear liquid.

Accordingly, the present inventors have been continuously researching to develop an eco-friendly deodorant that can efficiently remove odors because it has the ability to sterilize microorganisms while solving the above problems while having a fast decomposition ability and decomposition rate for odors and pollutants. The distillate of cinnamon, ginkgo leaves, ginseng, licorice, pine needles, and oak leaves obtained by the medium and distillation method is a non-volatile, clear liquid that has antibacterial activity that inhibits or sterilizes the growth of microorganisms, and has excellent deodorizing ability against bad odors. The present invention was completed by finding that it has

Therefore, the technical problem to be solved in the present invention is to provide a sterilizing and deodorizing composition excellent in antibacterial and deodorizing effects using natural materials.

In order to solve the above technical problem, the present invention provides an antibacterial disinfectant and deodorant composition obtained by distilling cinnamon, ginkgo leaves, honeysuckle, licorice, pine needles, and oak leaves.

(S1) With respect to 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of phosphorus, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, 600 to 650 parts by weight of oak leaves to prepare a herbal mixture manufacturing;

(S2) immersing the herbal medicine mixture obtained in step (S1) in water to perform primary extraction at 40 to 60° C. for 1 to 2 hours;

(S3) obtaining a distillate by condensing the steam produced by secondary extraction of the herbal medicine extract first extracted in step (S2) at 130 to 150° C. for 5 to 10 hours; and

(S4) aging the distillate obtained in step (S3) at room temperature for 1 to 2 days to obtain an antibacterial disinfectant and deodorant composition.

In addition, the present invention provides an environmentally friendly antibacterial disinfectant and deodorant obtained by the above manufacturing method.

As described above, the antibacterial disinfectant and deodorant composition of the present invention is a distillation method of cinnamon, ginkgo leaves, ginseng, licorice, pine needles, and oak leaves. It has the effect of inhibiting the proliferation of or having antibacterial activity to sterilize.

Therefore, the deodorant composition of the present invention is not harmful to the human body even when used in home tables, sinks, and refrigerators, can be used as a hand sanitizer for offices or toilets, and has excellent deodorizing effects for pets and is harmless, environmentally friendly deodorizing, It can be used in various fields related to people's lives, such as food, water treatment, daily life, and hygiene.

1 is a process diagram for manufacturing the antibacterial disinfectant and deodorant of the present invention.
2 is an example of a distillation cooling device for manufacturing the antibacterial disinfectant and deodorant of the present invention.
Figure 3 is a cotton cloth for immersing in water to wrap the mixed herbal medicine for manufacturing the antibacterial disinfectant and deodorant of the present invention.

Hereinafter, examples and the like will be described in detail to help the understanding of the present invention. However, the embodiments according to the present invention may be modified in various other forms, and the scope of the present invention should not be construed as being limited to the following examples. The embodiments of the present invention are provided to more completely explain the present invention to those of ordinary skill in the art.

In the present invention, as a method for producing an antibacterial disinfectant and deodorant composition obtained by distilling cinnamon, licorice, phosphorus, ginkgo leaves, pine needles, and oak leaves (S1) based on 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of phosphorus copper parts, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, and 600 to 650 parts by weight of oak leaves to prepare a herbal medicine mixture; (S2) immersing the herbal medicine mixture obtained in step (S1) in water to perform primary extraction at 40 to 60° C. for 1 to 2 hours; (S3) the herbal medicine extract first extracted in step (S2) Condensing the vapor produced by secondary extraction at 130 to 150° C. for 5 to 10 hours with a distillation condenser to obtain a distillate; and (S4) aging the distillate obtained in step (S3) at room temperature for 1 to 2 days to obtain an antibacterial disinfectant and deodorant composition.

The materials used in the present invention use herbal medicine materials and natural materials such as ginkgo leaves, pine needles, and oak leaves that can be easily obtained from the mountains of Korea. do. The extract of the herbal medicine extracted first in (S2) is extracted with hot water at a high temperature of 130 to 150 ℃, and the high temperature steam is sent to the distillation cooler to improve the extraction of the active ingredient, and the active ingredient is sent together with the high temperature steam to increase the content of the active ingredient raised to obtain a distillate.

Cinnamon, the active ingredient of the deodorant composition of the present invention, is a medicinal material made from the bark of Saengdal tree (Cinnamomum japonicum SIEB.), an evergreen tree belonging to the camphoraceae. It activates the function, stops quadriplegia and pain, and is widely applied to neuralgia and joint diseases that cause cold and sore back or knees. Recently, it has been attracting attention due to its excellent effect of inhibiting skin fungus.

Licorice of the present invention has an effect on detoxification, hepatitis, urticaria, dermatitis, eczema, etc.

Indong, the active ingredient of the deodorant composition of the present invention, is a semi-evergreen broad-leaved vine that grows wild in mountains and fields across the country. It has antipyretic, detoxifying, antibacterial, antiviral and antifungal, anti-inflammatory, astringent, and diuretic effects, promoting phagocytic action of white blood cells, relieving small intestine spasms, and inhibiting the growth of Bacillus subtilis and Staphylococcus aureus.

Ginkgo leaf, an active ingredient of the deodorant composition of the present invention, is a deciduous tree native to the Korean Peninsula and Manchuria, and taxonomically, flavonoid glycosides and terpene compound, Ginkgo Ride, contained in the extract of Ginkgo biloba, coniferous ginkgo, and ginkgo leaf are peripheral nerves. It has been found to have an effect on the expansion and activation of neurotransmitters, and is known to have excellent antibacterial and anti-inflammatory properties.

The active ingredient of the deodorant composition of the present invention, pine leaves, refers to the leaves of pine, a coniferous tree that grows in the mountains of Korea, and contains a phytoncide component. .

Oak, which is the active ingredient of the deodorant composition of the present invention, does not refer to any one species, but to several species belonging to the genus Oak family Oak. It is known to exhibit a strong antibacterial effect against microorganisms involved in deterioration.

The manufacturing step of the deodorant composition of the present invention is as shown in FIG. 1 (S1) is based on 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of phosphorus, 100 to 150 parts by weight of ginkgo leaves, 200 parts by weight of pine needles. to 300 parts by weight, and 600 to 650 parts by weight of oak.

Step (S2) in the manufacturing method of the deodorant composition of the present invention is the first step for 1 to 2 hours at 40 to 60 ℃ by wrapping the mixed herbal medicine and material in a cotton cloth (see FIG. 3) and immersing it in water, that is, distilled or bottled water. In the extraction step, water penetrates the material sufficiently to help leaching the active substance. At this time, the primary extraction may be performed in a triple pot as shown in the lower part of FIG. 2 .

In the manufacturing method of the present invention, step (S3) is a step to obtain a clear distillate by condensing the vapor produced by secondary extraction of the first extracted extract at 130 to 150° C. for 5 to 10 hours in a distillation cooler. The extraction rate of the active ingredient is increased, and the active ingredient along with the volatile ingredient is transferred to the distillation chiller equipped with a water-cooled chiller installed at the top together with high-temperature steam, leaving the polymer residue material. It is preferable that this high-temperature heating is a triple pot with a paraffin layer inserted therein. At this time, the reason for heating in the triple pot with the paraffin layer inserted is that it prevents the pot from overheating to 150℃ or more, and the oriental medicines that have sunk to the bottom stick to it and prevent the occurrence of odor. The distillation cooler used at this time is as shown in FIG.

In the manufacturing method of the deodorant composition of the present invention, step (S4) is a step of aging the distillate obtained above at room temperature for 1 to 2 days, so that the overall components become homogeneous and stabilize at room temperature.

The sterilization and deodorant composition of the present invention may include an additional component capable of increasing the sterilization and deodorization effect, and the type thereof is not particularly limited. For example, by adding water to the sterilization and deodorant composition of the present invention, the concentration can be adjusted and used, and the sterilization effect can be enhanced by using 1 to 5 parts by weight of hypochlorous acid water added by mixing.

The deodorant composition of the present invention may be prepared in the form of a spray or lotion, and there is no particular limitation on the form of the formulation.

In addition, the present invention provides a method for purifying indoor or outdoor air using the eco-friendly deodorant composition.

<Example 1>

Based on 100 parts by weight of cinnamon as the selected material, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of phosphorus, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, 600 to 650 parts by weight of oak leaves were mixed.

The herbal medicines formulated as described above were wrapped in cotton cloth and immersed in 100 liters of water, and the first extraction was performed at a temperature of 50° C. for 2 hours. Then, a water-cooled cooler is mounted on the upper part, and the extract is put in a triple pot with a paraffin layer inserted in the middle, and the extract is secondarily extracted at a temperature of 140 ° C. for 8 hours. The heated steam is condensed in a cooler to obtain 50 kg of a clear distillate The distillate was aged at room temperature for 1 to 2 days.

<Test Example 1>

After putting 20ml of the sterilization and deodorizing agent prepared in Example into a 5L size reactor and sealing it, the initial concentration of the test gas was injected at 50 μmol/mol, and the concentration of the test gas was adjusted at 0, 30, 60, 90, and 120 minutes. measured and the resulting value is called the sample concentration.

At this time, the test gas was tested with ammonia, trimethylamine, hydrogen sulfide and methyl mercaptan.

At this time, the concentration of the test gas was measured by a gas detection tube (formerly KS I 2218:2009), and the temperature during the test was (23.5±5.0)°C, and the humidity was maintained at (50±10)%R.H.

In addition, the concentration was measured without adding a sterilizing and deodorizing agent under the same conditions, and this is called the blank concentration.

The deodorization rate of the test gas for each time period was calculated by Equation 1 below.

[Equation 1]

Deodorization rate (%) of test gas = [{(blank concentration)-(sample concentration)/(blank concentration)}]×100

Test Items unit Test result Blank density
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(ammonia) 0 minutes % 50 50 0.0 30 minutes % 49 One 98.0 60 minutes % 49 One 98.0 90 minutes % 49 One 98.0 120 minutes % 49 <0.2 99.6

Test Items unit Test result Blank density
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(trimethylamine) 0 minutes % 50 50 0.0 30 minutes % 49 2 95.9 60 minutes % 49 2 95.9 90 minutes % 49 One 98.0 120 minutes % 49 One 98.0

Test Items unit Test result Blank density
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(hydrogen sulfide) 0 minutes % 50 50 0.0 30 minutes % 49 <0.1 99.8 60 minutes % 49 <0.1 99.8 90 minutes % 49 <0.1 99.8 120 minutes % 49 <0.1 99.8

Test Items unit Test result Blank density
(μmol/mol) sample concentration
(μmol/mol) Deodorization rate (%) test gas
(methyl mercaptan) 0 minutes % 50 50 0.0 30 minutes % 49 <0.1 99.8 60 minutes % 49 <0.1 99.8 90 minutes % 49 <0.1 99.8 120 minutes % 49 <0.1 99.8

<Test Example 2> The antifungal activity of the antibacterial disinfectant and deodorant prepared in Examples at each concentration, 1000 μg/ml, 800 μg/ml, 500 μg/ml, 300 μg/ml, 100 μg/ml, 50 μg/ After the treatment by spraying at a concentration of ㎖, the actual antifungal power was compared with that of the untreated group from 1 to 10 days, and the following results were obtained.

Antifungal effect of this extract when treated directly on fungal culture samples Date/Concentration gray mold fungus note 1000 800 500 300 100 50 1 day ○ ○ ○ - - - Confirmation of sterilization power 2 days ○ ○ ○ ○ ○ - 5 days ○ ○ ○ ○ ○ - 7 days ○ ○ ○ ○ ○ ○ ○ 10 days ○ ○ ○ ○ ○ ○ ○

Therefore, the antibacterial disinfectant and deodorant of the present invention can confirm high sterilization power, so the deodorant of the present invention is environmentally friendly, has a sterilization function and can be suitable for manufacturing a deodorant with a deodorizing function maximized. Having been described in detail, it will be apparent to those skilled in the art that these specific descriptions are only preferred embodiments, and the scope of the present invention is not limited thereby. Accordingly, the substantial scope of the present invention will be defined by the appended claims and their equivalents.

Claims (1)

An eco-friendly sterilization and deodorant composition prepared by a natural material distillation method comprising the following steps:
(S1) With respect to 100 parts by weight of cinnamon, 30 to 50 parts by weight of licorice, 50 to 100 parts by weight of phosphorus, 100 to 150 parts by weight of ginkgo leaves, 200 to 300 parts by weight of pine needles, 600 to 650 parts by weight of oak leaves in a cotton cloth, manufacturing;
(S2) immersing the herbal medicine mixture contained in the cotton cloth obtained in step (S1) in water to perform primary extraction at 40 to 60° C. for 1 to 2 hours;
(S3) Secondary extraction of the herbal extract extracted in step (S2) at 130 to 150° C. for 5 to 10 hours in a triple pot with a paraffin layer inserted in the middle, and sending the resulting vapor to a cooler to condense it and distillate obtaining a; and
(S4) aging the distillate obtained in step (S3) at room temperature for 1 to 2 days to obtain an eco-friendly sterilization and deodorant composition.

Images