KR102446032B1 - 헬륨 가스의 정제 방법 및 정제 시스템 - Google Patents
헬륨 가스의 정제 방법 및 정제 시스템 Download PDFInfo
- Publication number
- KR102446032B1 KR102446032B1 KR1020160028236A KR20160028236A KR102446032B1 KR 102446032 B1 KR102446032 B1 KR 102446032B1 KR 1020160028236 A KR1020160028236 A KR 1020160028236A KR 20160028236 A KR20160028236 A KR 20160028236A KR 102446032 B1 KR102446032 B1 KR 102446032B1
- Authority
- KR
- South Korea
- Prior art keywords
- gas
- helium
- adsorption
- adsorption tower
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000007789 gas Substances 0.000 title claims abstract description 789
- 238000000034 method Methods 0.000 title claims abstract description 366
- 239000001307 helium Substances 0.000 title claims abstract description 341
- 229910052734 helium Inorganic materials 0.000 title claims abstract description 341
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 title claims abstract description 341
- 238000000746 purification Methods 0.000 title claims description 59
- 238000001179 sorption measurement Methods 0.000 claims abstract description 600
- 230000008569 process Effects 0.000 claims abstract description 330
- 238000003795 desorption Methods 0.000 claims abstract description 136
- 239000002994 raw material Substances 0.000 claims abstract description 100
- 239000012535 impurity Substances 0.000 claims abstract description 46
- 239000003463 adsorbent Substances 0.000 claims abstract description 37
- 238000004891 communication Methods 0.000 claims description 61
- 238000004140 cleaning Methods 0.000 claims description 50
- 238000005406 washing Methods 0.000 claims description 41
- 238000004064 recycling Methods 0.000 claims description 37
- 238000007599 discharging Methods 0.000 claims description 25
- 230000006837 decompression Effects 0.000 claims description 23
- 230000001105 regulatory effect Effects 0.000 claims description 11
- 230000007423 decrease Effects 0.000 claims description 7
- 230000001276 controlling effect Effects 0.000 claims description 3
- 230000003247 decreasing effect Effects 0.000 claims description 3
- 150000002371 helium Chemical class 0.000 claims 1
- 238000011084 recovery Methods 0.000 abstract description 51
- 230000009467 reduction Effects 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- 230000006872 improvement Effects 0.000 description 10
- 238000007670 refining Methods 0.000 description 10
- 238000010586 diagram Methods 0.000 description 8
- 238000011946 reduction process Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 239000013307 optical fiber Substances 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 230000002195 synergetic effect Effects 0.000 description 4
- 230000002463 transducing effect Effects 0.000 description 4
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 229910021536 Zeolite Inorganic materials 0.000 description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000010457 zeolite Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- -1 and for example Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000000112 cooling gas Substances 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B23/00—Noble gases; Compounds thereof
- C01B23/001—Purification or separation processes of noble gases
- C01B23/0036—Physical processing only
- C01B23/0052—Physical processing only by adsorption in solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
- B01D53/047—Pressure swing adsorption
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/04—Purification or separation of nitrogen
- C01B21/0405—Purification or separation processes
- C01B21/0433—Physical processing only
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40007—Controlling pressure or temperature swing adsorption
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0001—Separation or purification processing
- C01B2210/0009—Physical processing
- C01B2210/0014—Physical processing by adsorption in solids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0029—Obtaining noble gases
- C01B2210/0031—Helium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0042—Making ultrapure specific gas
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Separation Of Gases By Adsorption (AREA)
- Separation By Low-Temperature Treatments (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JPJP-P-2015-059204 | 2015-03-23 | ||
| JP2015059204A JP6384960B2 (ja) | 2015-03-23 | 2015-03-23 | ヘリウムガスの精製方法および精製システム |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20160113969A KR20160113969A (ko) | 2016-10-04 |
| KR102446032B1 true KR102446032B1 (ko) | 2022-09-21 |
Family
ID=57043939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020160028236A Active KR102446032B1 (ko) | 2015-03-23 | 2016-03-09 | 헬륨 가스의 정제 방법 및 정제 시스템 |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JP6384960B2 (enExample) |
| KR (1) | KR102446032B1 (enExample) |
| CN (1) | CN105983296A (enExample) |
| TW (1) | TWI680791B (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108217616A (zh) * | 2018-01-16 | 2018-06-29 | 中科睿凌江苏低温设备有限公司 | 一种用于低温超导磁体氦气液化的杂质气体分离筒 |
| CN108355416A (zh) * | 2018-04-19 | 2018-08-03 | 合肥硕朗自动化科技有限公司 | 一种用于真空箱检漏系统的氦气回收净化装置 |
| CN109883623B (zh) * | 2019-03-04 | 2021-06-22 | 浙江工业职业技术学院 | 一种基于真空箱检漏用的氦气回收净化装置 |
| CN110748788A (zh) * | 2019-10-18 | 2020-02-04 | Tcl空调器(中山)有限公司 | 气体回收系统及气体回收方法 |
| KR102667907B1 (ko) * | 2023-11-29 | 2024-05-22 | 주식회사 케이와이테크 | 고순도 가스 정제 시스템, 이를 위한 제어 장치 및 제어 방법 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2010275150A (ja) | 2009-05-29 | 2010-12-09 | Sumitomo Seika Chem Co Ltd | ヘリウム精製方法およびヘリウム精製装置 |
| JP2014009139A (ja) | 2012-07-02 | 2014-01-20 | Sumitomo Seika Chem Co Ltd | ヘリウムガスの精製方法および精製装置 |
| WO2014104196A1 (ja) | 2012-12-28 | 2014-07-03 | 大阪瓦斯株式会社 | ガス精製装置 |
| WO2014156467A1 (ja) | 2013-03-28 | 2014-10-02 | 住友精化株式会社 | 水素ガスの精製方法及び精製装置 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3564816A (en) | 1968-12-30 | 1971-02-23 | Union Carbide Corp | Selective adsorption process |
| US3986849A (en) | 1975-11-07 | 1976-10-19 | Union Carbide Corporation | Selective adsorption process |
| DE3716898A1 (de) * | 1987-05-20 | 1988-12-15 | Bergwerksverband Gmbh | Verfahren und vorrichtung zur heliumanreicherung |
| US5542966A (en) * | 1994-10-21 | 1996-08-06 | Nitrotec Corporation | Helium recovery |
| US5707425A (en) * | 1994-10-21 | 1998-01-13 | Nitrotec Corporation | Helium recovery from higher helium content streams |
| US6699307B1 (en) * | 2002-10-11 | 2004-03-02 | H2Gen Innovations, Inc. | High recovery PSA cycles and apparatus with reduced complexity |
-
2015
- 2015-03-23 JP JP2015059204A patent/JP6384960B2/ja active Active
-
2016
- 2016-03-03 TW TW105106553A patent/TWI680791B/zh not_active IP Right Cessation
- 2016-03-09 KR KR1020160028236A patent/KR102446032B1/ko active Active
- 2016-03-16 CN CN201610150583.5A patent/CN105983296A/zh active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2010275150A (ja) | 2009-05-29 | 2010-12-09 | Sumitomo Seika Chem Co Ltd | ヘリウム精製方法およびヘリウム精製装置 |
| JP2014009139A (ja) | 2012-07-02 | 2014-01-20 | Sumitomo Seika Chem Co Ltd | ヘリウムガスの精製方法および精製装置 |
| WO2014104196A1 (ja) | 2012-12-28 | 2014-07-03 | 大阪瓦斯株式会社 | ガス精製装置 |
| WO2014156467A1 (ja) | 2013-03-28 | 2014-10-02 | 住友精化株式会社 | 水素ガスの精製方法及び精製装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2016175815A (ja) | 2016-10-06 |
| TWI680791B (zh) | 2020-01-01 |
| TW201637706A (zh) | 2016-11-01 |
| CN105983296A (zh) | 2016-10-05 |
| JP6384960B2 (ja) | 2018-09-05 |
| KR20160113969A (ko) | 2016-10-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 20160309 |
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| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 20201204 Comment text: Request for Examination of Application Patent event code: PA02011R01I Patent event date: 20160309 Comment text: Patent Application |
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| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 20220826 |
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| PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 20220919 Patent event code: PR07011E01D |
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| PR1002 | Payment of registration fee |
Payment date: 20220919 End annual number: 3 Start annual number: 1 |
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| PG1601 | Publication of registration |