KR102375530B1 - 소량의 바나듐이 도핑된 반절연 탄화규소 단결정, 기판, 제조 방법 - Google Patents
소량의 바나듐이 도핑된 반절연 탄화규소 단결정, 기판, 제조 방법 Download PDFInfo
- Publication number
- KR102375530B1 KR102375530B1 KR1020197037935A KR20197037935A KR102375530B1 KR 102375530 B1 KR102375530 B1 KR 102375530B1 KR 1020197037935 A KR1020197037935 A KR 1020197037935A KR 20197037935 A KR20197037935 A KR 20197037935A KR 102375530 B1 KR102375530 B1 KR 102375530B1
- Authority
- KR
- South Korea
- Prior art keywords
- silicon carbide
- single crystal
- carbide single
- energy level
- concentration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/36—Carbides
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/02—Epitaxial-layer growth
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B33/00—After-treatment of single crystals or homogeneous polycrystalline material with defined structure
- C30B33/02—Heat treatment
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B35/00—Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
- C30B35/002—Crucibles or containers
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B35/00—Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
- C30B35/007—Apparatus for preparing, pre-treating the source material to be used for crystal growth
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02365—Forming inorganic semiconducting materials on a substrate
- H01L21/02518—Deposited layers
- H01L21/02521—Materials
- H01L21/02524—Group 14 semiconducting materials
- H01L21/02529—Silicon carbide
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Inorganic Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Manufacturing & Machinery (AREA)
- Computer Hardware Design (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- General Physics & Mathematics (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Physical Vapour Deposition (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811204702.6 | 2018-10-16 | ||
| CN201811204690.7A CN109280965B (zh) | 2018-10-16 | 2018-10-16 | 一种掺杂少量钒的高质量半绝缘碳化硅单晶及衬底 |
| CN201811204702.6A CN109280966B (zh) | 2018-10-16 | 2018-10-16 | 掺杂少量钒的高质量半绝缘碳化硅单晶及衬底的制备方法 |
| CN201811204690.7 | 2018-10-16 | ||
| PCT/CN2018/123707 WO2020077846A1 (zh) | 2018-10-16 | 2018-12-26 | 掺杂少量钒的半绝缘碳化硅单晶、衬底、制备方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20200044728A KR20200044728A (ko) | 2020-04-29 |
| KR102375530B1 true KR102375530B1 (ko) | 2022-03-16 |
Family
ID=70283621
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020197037935A Active KR102375530B1 (ko) | 2018-10-16 | 2018-12-26 | 소량의 바나듐이 도핑된 반절연 탄화규소 단결정, 기판, 제조 방법 |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP3666936A4 (enExample) |
| JP (1) | JP7235318B2 (enExample) |
| KR (1) | KR102375530B1 (enExample) |
| TW (1) | TWI703242B (enExample) |
| WO (1) | WO2020077846A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113151895B (zh) * | 2020-06-09 | 2023-02-03 | 北京世纪金光半导体有限公司 | 大直径高纯半绝缘碳化硅生长工艺方法 |
| WO2023119755A1 (ja) * | 2021-12-20 | 2023-06-29 | 住友電気工業株式会社 | 炭化珪素基板、炭化珪素半導体装置の製造方法および炭化珪素基板の製造方法 |
| CN117585678B (zh) * | 2023-11-30 | 2024-08-27 | 宁波合盛新材料有限公司 | 一种用于pvt炉合成碳化硅粉新热场的吸氮处理方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004533720A (ja) * | 2001-05-11 | 2004-11-04 | クリー インコーポレイテッド | 高い降伏電圧を有する半導体デバイスのための高抵抗率炭化珪素基板 |
| JP2008505833A (ja) * | 2004-07-07 | 2008-02-28 | トゥー‐シックス・インコーポレイテッド | 低ドーピング半絶縁性SiC結晶と方法 |
| JP2008053667A (ja) * | 2006-07-28 | 2008-03-06 | Central Res Inst Of Electric Power Ind | SiC結晶の質を向上させる方法およびSiC半導体素子 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61219787A (ja) * | 1985-03-26 | 1986-09-30 | Kyocera Corp | 高純度半導体単結晶製造用ルツボ |
| US6218680B1 (en) * | 1999-05-18 | 2001-04-17 | Cree, Inc. | Semi-insulating silicon carbide without vanadium domination |
| SE520968C2 (sv) | 2001-10-29 | 2003-09-16 | Okmetic Oyj | Högresistiv monokristallin kiselkarbid och metod för dess framställning |
| US7601441B2 (en) | 2002-06-24 | 2009-10-13 | Cree, Inc. | One hundred millimeter high purity semi-insulating single crystal silicon carbide wafer |
| JP5068423B2 (ja) * | 2004-10-13 | 2012-11-07 | 新日本製鐵株式会社 | 炭化珪素単結晶インゴット、炭化珪素単結晶ウェハ及びその製造方法 |
| CN102560672A (zh) * | 2010-12-31 | 2012-07-11 | 中国科学院物理研究所 | 半绝缘碳化硅单晶材料 |
| CN102560671B (zh) * | 2010-12-31 | 2015-05-27 | 中国科学院物理研究所 | 半绝缘碳化硅单晶 |
| JP2013173655A (ja) | 2012-02-27 | 2013-09-05 | Nagoya Institute Of Technology | 半導体結晶材料およびこれを用いた半導体素子 |
-
2018
- 2018-12-26 WO PCT/CN2018/123707 patent/WO2020077846A1/zh not_active Ceased
- 2018-12-26 KR KR1020197037935A patent/KR102375530B1/ko active Active
- 2018-12-26 EP EP18922091.6A patent/EP3666936A4/en active Pending
- 2018-12-26 JP JP2019571538A patent/JP7235318B2/ja active Active
-
2019
- 2019-10-14 TW TW108136953A patent/TWI703242B/zh active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004533720A (ja) * | 2001-05-11 | 2004-11-04 | クリー インコーポレイテッド | 高い降伏電圧を有する半導体デバイスのための高抵抗率炭化珪素基板 |
| JP2008505833A (ja) * | 2004-07-07 | 2008-02-28 | トゥー‐シックス・インコーポレイテッド | 低ドーピング半絶縁性SiC結晶と方法 |
| JP2008053667A (ja) * | 2006-07-28 | 2008-03-06 | Central Res Inst Of Electric Power Ind | SiC結晶の質を向上させる方法およびSiC半導体素子 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP7235318B2 (ja) | 2023-03-08 |
| EP3666936A4 (en) | 2020-10-28 |
| WO2020077846A1 (zh) | 2020-04-23 |
| EP3666936A1 (en) | 2020-06-17 |
| TWI703242B (zh) | 2020-09-01 |
| TW202026470A (zh) | 2020-07-16 |
| JP2021502944A (ja) | 2021-02-04 |
| KR20200044728A (ko) | 2020-04-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US9893152B2 (en) | Semi-insulating silicon carbide monocrystal and method of growing the same | |
| US11542631B2 (en) | Method for producing p-type 4H-SiC single crystal | |
| CN109280965B (zh) | 一种掺杂少量钒的高质量半绝缘碳化硅单晶及衬底 | |
| JP6760721B2 (ja) | バナジウムでドープしたSiC塊状単結晶の製造方法及びバナジウムでドープしたSiC基板 | |
| CN107385512B (zh) | 一种抑制碳化硅单晶中碳包裹体缺陷的生长方法 | |
| US20090053125A1 (en) | Stabilizing 4H Polytype During Sublimation Growth Of SiC Single Crystals | |
| CN109355705B (zh) | 一种制备高质量单晶碳化硅的装置及其应用 | |
| EP2940196B1 (en) | Method for producing n-type sic single crystal | |
| CN109280966B (zh) | 掺杂少量钒的高质量半绝缘碳化硅单晶及衬底的制备方法 | |
| KR102375530B1 (ko) | 소량의 바나듐이 도핑된 반절연 탄화규소 단결정, 기판, 제조 방법 | |
| CN106968018A (zh) | 一种锗氮共掺的碳化硅单晶材料的生长方法 | |
| TWI723578B (zh) | 高純度碳化矽單晶基材及其製備方法、應用 | |
| CN109338463B (zh) | 一种高纯碳化硅单晶衬底 | |
| WO2019095632A1 (zh) | 一种半绝缘碳化硅单晶的制备方法 | |
| CN114481307B (zh) | 一种SiC单晶衬底及其制备方法与应用 | |
| CN115142123B (zh) | 一种掺锗改善碳化硅单晶衬底面型参数的方法 | |
| CN114214723B (zh) | 一种准本征半绝缘碳化硅单晶的制备方法 | |
| KR20240080952A (ko) | 대구경 단결정 및 대구경 단결정 성장 방법 | |
| KR20250050993A (ko) | 대구경 탄화 규소 단결정 성장 방법, 성장 장치 및 이를 이용하여 성장된 탄화 규소 단결정 | |
| CN117737856A (zh) | 一种电性能优良的高纯半绝缘碳化硅衬底及其制备方法 | |
| CN119932723A (zh) | 一种氮化铝晶锭退火方法 | |
| CN121023645A (zh) | 一种高纯半绝缘碳化硅衬底的制备方法 | |
| CN116288672A (zh) | 一种碳化硅单晶的生长方法 | |
| KR20160089973A (ko) | 탄화규소 분말의 질소함유량을 감소시키는 방법, 이에 의해 제조된 탄화규소 단결정 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20191223 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PA0201 | Request for examination | ||
| AMND | Amendment | ||
| PG1501 | Laying open of application | ||
| A302 | Request for accelerated examination | ||
| AMND | Amendment | ||
| PA0302 | Request for accelerated examination |
Patent event date: 20210330 Patent event code: PA03022R01D Comment text: Request for Accelerated Examination |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 20210817 Patent event code: PE09021S01D |
|
| AMND | Amendment | ||
| E601 | Decision to refuse application | ||
| PE0601 | Decision on rejection of patent |
Patent event date: 20211220 Comment text: Decision to Refuse Application Patent event code: PE06012S01D Patent event date: 20210817 Comment text: Notification of reason for refusal Patent event code: PE06011S01I |
|
| AMND | Amendment | ||
| PX0901 | Re-examination |
Patent event code: PX09011S01I Patent event date: 20211220 Comment text: Decision to Refuse Application Patent event code: PX09012R01I Patent event date: 20211018 Comment text: Amendment to Specification, etc. Patent event code: PX09012R01I Patent event date: 20210330 Comment text: Amendment to Specification, etc. Patent event code: PX09012R01I Patent event date: 20200114 Comment text: Amendment to Specification, etc. |
|
| PX0701 | Decision of registration after re-examination |
Patent event date: 20220214 Comment text: Decision to Grant Registration Patent event code: PX07013S01D Patent event date: 20220113 Comment text: Amendment to Specification, etc. Patent event code: PX07012R01I Patent event date: 20211220 Comment text: Decision to Refuse Application Patent event code: PX07011S01I Patent event date: 20211018 Comment text: Amendment to Specification, etc. Patent event code: PX07012R01I Patent event date: 20210330 Comment text: Amendment to Specification, etc. Patent event code: PX07012R01I Patent event date: 20200114 Comment text: Amendment to Specification, etc. Patent event code: PX07012R01I |
|
| X701 | Decision to grant (after re-examination) | ||
| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 20220314 Patent event code: PR07011E01D |
|
| PR1002 | Payment of registration fee |
Payment date: 20220314 End annual number: 3 Start annual number: 1 |
|
| PG1601 | Publication of registration | ||
| PR1001 | Payment of annual fee |
Payment date: 20250304 Start annual number: 4 End annual number: 4 |