KR101785739B1 - 1종 이상의 글리신-ｎ,ｎ-디아세트산 유도체를 포함하는 스프레이 분말의 제조 방법과 압축 응집체를 제조하기 위한 스프레이 분말의 용도 - Google Patents

1종 이상의 글리신-ｎ,ｎ-디아세트산 유도체를 포함하는 스프레이 분말의 제조 방법과 압축 응집체를 제조하기 위한 스프레이 분말의 용도 Download PDF

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Publication number
KR101785739B1
KR101785739B1 KR1020117029919A KR20117029919A KR101785739B1 KR 101785739 B1 KR101785739 B1 KR 101785739B1 KR 1020117029919 A KR1020117029919 A KR 1020117029919A KR 20117029919 A KR20117029919 A KR 20117029919A KR 101785739 B1 KR101785739 B1 KR 101785739B1
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South Korea
Prior art keywords
aqueous solution
glycine
diacetic acid
spray
spray powder
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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KR1020117029919A
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English (en)
Korean (ko)
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KR20120057581A (ko
Inventor
프랑크 메르체나
미카엘 쇤헤르
로버트 하인츠
토마스 하이덴펠더
Original Assignee
바스프 에스이
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Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20120057581A publication Critical patent/KR20120057581A/ko
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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0091—Dishwashing tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707—Polyethers, e.g. polyalkyleneoxides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Glanulating (AREA)
  • Medicinal Preparation (AREA)
KR1020117029919A 2009-05-20 2010-05-19 1종 이상의 글리신-ｎ,ｎ-디아세트산 유도체를 포함하는 스프레이 분말의 제조 방법과 압축 응집체를 제조하기 위한 스프레이 분말의 용도 Expired - Fee Related KR101785739B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP09160717.6 2009-05-20
EP09160717 2009-05-20
US25391109P 2009-10-22 2009-10-22
US61/253,911 2009-10-22
PCT/EP2010/056855 WO2010133617A1 (de) 2009-05-20 2010-05-19 Verfahren zur herstellung eines sprühpulvers enthaltend ein oder mehrere glycin-n,n-diessigsäure-derivate und verwendung des sprühpulvers zur herstellung von pressagglomeraten

Publications (2)

Publication Number Publication Date
KR20120057581A KR20120057581A (ko) 2012-06-05
KR101785739B1 true KR101785739B1 (ko) 2017-10-16

Family

ID=43125758

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020117029919A Expired - Fee Related KR101785739B1 (ko) 2009-05-20 2010-05-19 1종 이상의 글리신-ｎ,ｎ-디아세트산 유도체를 포함하는 스프레이 분말의 제조 방법과 압축 응집체를 제조하기 위한 스프레이 분말의 용도

Country Status (14)

Country Link
US (1) US8748366B2 (enExample)
EP (1) EP2432582B1 (enExample)
JP (1) JP5771191B2 (enExample)
KR (1) KR101785739B1 (enExample)
CN (1) CN102458635A (enExample)
AU (1) AU2010251173A1 (enExample)
BR (1) BRPI1012868A2 (enExample)
CA (1) CA2762506A1 (enExample)
MX (1) MX2011012364A (enExample)
MY (1) MY153903A (enExample)
RU (1) RU2533974C2 (enExample)
SG (1) SG178076A1 (enExample)
WO (1) WO2010133617A1 (enExample)
ZA (1) ZA201109262B (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011045266A1 (de) 2009-10-12 2011-04-21 Basf Se Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze
US8785685B2 (en) 2011-04-12 2014-07-22 Basf Se Process for preparing aminopolycarboxylates proceeding from amino acids
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
PL2584028T3 (pl) 2011-10-19 2017-10-31 Procter & Gamble Cząstka
RU2742268C2 (ru) * 2016-06-20 2021-02-04 Басф Се Порошки и гранулы и способ получения таких порошков и гранул
CN110799489A (zh) * 2017-06-28 2020-02-14 巴斯夫欧洲公司 制备络合剂的方法
US10836709B2 (en) 2017-07-07 2020-11-17 Nouryon Chemicals International B.V. Process to prepare a solid composition of an amino acid diacetic acid
EP4349949A1 (en) * 2022-10-05 2024-04-10 Basf Se Process for making a solid alkali metal salt of an aminocarboxylate complexing agent

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3066611A (en) * 1959-07-10 1962-12-04 Schwartmann Karl Membrane pump
AT339246B (de) * 1974-08-14 1977-10-10 Henkel & Cie Gmbh Als bestandteil von pulverformigen wasch- und bleichmitteln geeignetes bleichhilfsmittel
US5108646A (en) * 1990-10-26 1992-04-28 The Procter & Gamble Company Process for agglomerating aluminosilicate or layered silicate detergent builders
US5518180A (en) * 1992-06-12 1996-05-21 Niro Holding A/S Rotary atomizer and a method of operating it
DE4319935A1 (de) 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
DE19518986A1 (de) * 1995-05-29 1996-12-05 Basf Ag Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium
US5998356A (en) * 1995-09-18 1999-12-07 The Procter & Gamble Company Process for making granular detergents
DE19543162A1 (de) 1995-11-18 1997-05-22 Basf Ag Feste Textilwaschmittel-Formulierung aus anorganischen Buildern, Glycin-N,N-diessigsäure-Derivaten als organische Cobuilder sowie anionischen und nichtionischen Tensiden
JP3810854B2 (ja) * 1996-01-22 2006-08-16 花王株式会社 高密度粉末洗剤組成物
JP3810847B2 (ja) * 1996-01-22 2006-08-16 花王株式会社 高密度粉末洗剤組成物
DE19649681A1 (de) 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
JPH10204494A (ja) * 1997-01-27 1998-08-04 Kao Corp 粉末状酵素製剤及びそれを用いた造粒物
JPH1135986A (ja) * 1997-05-19 1999-02-09 Kao Corp 漂白剤含有洗剤組成物
JP4033955B2 (ja) * 1997-05-19 2008-01-16 花王株式会社 漂白剤含有洗剤組成物
JPH1121585A (ja) * 1997-07-03 1999-01-26 Kao Corp 洗浄剤組成物
CN1214947A (zh) * 1998-10-13 1999-04-28 苏州工业园区永达化工有限公司 甘氨酸钠的高速离心喷雾干燥法
DE10123621B4 (de) * 2001-05-15 2006-12-07 Henkel Kgaa Verfahren zur Herstellung einer Wasserenthärtertablette
US7008915B2 (en) * 2001-08-07 2006-03-07 The Procter & Gamble Co. Liquid detergent compositions with low-density particles
WO2003037303A1 (en) * 2001-11-01 2003-05-08 Nektar Therapeutics Spray drying methods and compositions thereof
US20030203832A1 (en) * 2002-04-26 2003-10-30 The Procter & Gamble Company Low organic spray drying process and composition formed thereby
DE102004012915A1 (de) * 2004-03-17 2005-10-13 Clariant Gmbh Feste Zubereitungen enthaltend einen sensitiven Wirkstoff
US7442679B2 (en) * 2004-04-15 2008-10-28 Ecolab Inc. Binding agent for solidification matrix comprising MGDA
DE102004032320A1 (de) * 2004-07-02 2006-01-19 Basf Ag Mischpulver oder Mischgranulat auf Basis von MGDA
DE102005041347A1 (de) * 2005-08-31 2007-03-01 Basf Ag Reinigungsformulierungen für die maschinelle Geschirrreinigung enthaltend hydrophil modifizierte Polycarboxylate
JP5328781B2 (ja) 2007-07-03 2013-10-30 ビーエーエスエフ ソシエタス・ヨーロピア 本質的にα−アラニン−Ｎ，Ｎ−二酢酸及び／又はα−アラニン−Ｎ，Ｎ−二酢酸の１以上の誘導体を含有する、易流動性でかつ貯蔵安定性の固体の製造法
JP2007308715A (ja) * 2007-07-05 2007-11-29 Kao Corp 粉末状酵素及びそれを用いた造粒物
WO2009103822A1 (en) * 2008-04-01 2009-08-27 Unilever Nv Preparation of free flowing granules of methyglycine diacetic acid
EP2158922A1 (de) 2008-08-28 2010-03-03 Basf Se Verfahren zur Trocknung von als Solubilisatoren für in Wasser schwerlösliche Verbindungen geeigneten Copolymeren auf Basis von Polyethern
US20110257431A1 (en) 2010-03-18 2011-10-20 Basf Se Process for producing side product-free aminocarboxylates

Also Published As

Publication number Publication date
WO2010133617A1 (de) 2010-11-25
EP2432582B1 (de) 2014-05-07
RU2533974C2 (ru) 2014-11-27
BRPI1012868A2 (pt) 2018-02-20
JP2012527506A (ja) 2012-11-08
EP2432582A1 (de) 2012-03-28
MY153903A (en) 2015-04-15
AU2010251173A1 (en) 2012-01-19
US8748366B2 (en) 2014-06-10
ZA201109262B (en) 2013-02-27
SG178076A1 (en) 2012-03-29
KR20120057581A (ko) 2012-06-05
US20120071381A1 (en) 2012-03-22
JP5771191B2 (ja) 2015-08-26
MX2011012364A (es) 2012-01-27
CN102458635A (zh) 2012-05-16
CA2762506A1 (en) 2010-11-25

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