KR101511701B1 - 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법 - Google Patents

폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법 Download PDF

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KR101511701B1
KR101511701B1 KR20130090023A KR20130090023A KR101511701B1 KR 101511701 B1 KR101511701 B1 KR 101511701B1 KR 20130090023 A KR20130090023 A KR 20130090023A KR 20130090023 A KR20130090023 A KR 20130090023A KR 101511701 B1 KR101511701 B1 KR 101511701B1
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catalyst
polybutene
raw material
organic solvent
inert organic
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Korean (ko)
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KR20150014632A (ko
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김명석
박민섭
민경태
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대림산업 주식회사
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Priority to KR20130090023A priority Critical patent/KR101511701B1/ko
Application filed by 대림산업 주식회사 filed Critical 대림산업 주식회사
Priority to MYPI2016700326A priority patent/MY182889A/en
Priority to JP2016531521A priority patent/JP6731848B2/ja
Priority to SG11201600697QA priority patent/SG11201600697QA/en
Priority to BR112016001935-0A priority patent/BR112016001935B1/pt
Priority to PCT/KR2014/006933 priority patent/WO2015016577A1/ko
Priority to CN201480043574.5A priority patent/CN105452304B/zh
Priority to EP14832215.9A priority patent/EP3029075B1/en
Priority to US14/908,702 priority patent/US9637576B2/en
Publication of KR20150014632A publication Critical patent/KR20150014632A/ko
Application granted granted Critical
Publication of KR101511701B1 publication Critical patent/KR101511701B1/ko
Priority to SA516370500A priority patent/SA516370500B1/ar
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F110/00Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F110/04Monomers containing three or four carbon atoms
    • C08F110/08Butenes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/01Processes of polymerisation characterised by special features of the polymerisation apparatus used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1862Stationary reactors having moving elements inside placed in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0457Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being placed in separate reactors
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F10/04Monomers containing three or four carbon atoms
    • C08F10/08Butenes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/001Removal of residual monomers by physical means
    • C08F6/003Removal of residual monomers by physical means from polymer solutions, suspensions, dispersions or emulsions without recovery of the polymer therefrom
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/02Neutralisation of the polymerisation mass, e.g. killing the catalyst also removal of catalyst residues
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00Recovery or working-up of waste materials
    • C08J11/02Recovery or working-up of waste materials of solvents, plasticisers or unreacted monomers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
KR20130090023A 2013-07-30 2013-07-30 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법 Active KR101511701B1 (ko)

Priority Applications (10)

Application Number Priority Date Filing Date Title
KR20130090023A KR101511701B1 (ko) 2013-07-30 2013-07-30 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법
US14/908,702 US9637576B2 (en) 2013-07-30 2014-07-29 Device and method for re-circulating raw material used when manufacturing polybutene
SG11201600697QA SG11201600697QA (en) 2013-07-30 2014-07-29 Device and method for re-circulating raw material used when manufacturing polybutene
BR112016001935-0A BR112016001935B1 (pt) 2013-07-30 2014-07-29 Dispositivo e método para recirculação de matéria-prima utilizada na fabricação de polibuteno
PCT/KR2014/006933 WO2015016577A1 (ko) 2013-07-30 2014-07-29 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법
CN201480043574.5A CN105452304B (zh) 2013-07-30 2014-07-29 用于再循环制备聚丁烯时所用的原料的装置和方法
MYPI2016700326A MY182889A (en) 2013-07-30 2014-07-29 Apparatus and method for recirculating of raw material used during the polyisobutylene preparation process
JP2016531521A JP6731848B2 (ja) 2013-07-30 2014-07-29 ポリブテン製造の際に使用される原料の再循環装置および方法
EP14832215.9A EP3029075B1 (en) 2013-07-30 2014-07-29 Device and method for re-circulating raw material used when manufacturing polybutene
SA516370500A SA516370500B1 (ar) 2013-07-30 2016-01-30 جهاز وطريقة لإعادة تدوير مادة خام مستخدمة عند تصنيع بولي بيوتين

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR20130090023A KR101511701B1 (ko) 2013-07-30 2013-07-30 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법

Publications (2)

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KR20150014632A KR20150014632A (ko) 2015-02-09
KR101511701B1 true KR101511701B1 (ko) 2015-04-13

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Country Status (10)

Country Link
US (1) US9637576B2 (enExample)
EP (1) EP3029075B1 (enExample)
JP (1) JP6731848B2 (enExample)
KR (1) KR101511701B1 (enExample)
CN (1) CN105452304B (enExample)
BR (1) BR112016001935B1 (enExample)
MY (1) MY182889A (enExample)
SA (1) SA516370500B1 (enExample)
SG (1) SG11201600697QA (enExample)
WO (1) WO2015016577A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102202777B1 (ko) * 2019-09-16 2021-01-13 한화토탈 주식회사 비반응성 폴리부텐의 제조시 원료의 재순환 장치 및 그 방법

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KR101511701B1 (ko) * 2013-07-30 2015-04-13 대림산업 주식회사 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법
KR101511708B1 (ko) * 2013-08-28 2015-04-13 대림산업 주식회사 폴리부텐 제조 시 발생되는 할로겐의 제거 장치 및 방법
KR101988508B1 (ko) * 2015-10-29 2019-09-30 주식회사 엘지화학 스티렌-부타디엔 용액 중합 시 용매 내 불순물 저감 방법
CN106832070B (zh) * 2017-02-27 2020-07-14 山东省滕州瑞达化工有限公司 用于连续生产聚丁烯-1的方法及装置
CN113056490B (zh) * 2019-01-18 2023-07-28 株式会社Lg化学 聚丁烯的分离方法
KR102203006B1 (ko) * 2019-04-24 2021-01-13 대림산업 주식회사 고반응성 폴리부텐의 제조 방법
CN115725010A (zh) * 2023-01-05 2023-03-03 浙江信汇新材料股份有限公司 一种中、高分子量聚异丁烯制备方法及其引发体系、应用

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JP2002220411A (ja) * 2001-01-29 2002-08-09 Nippon Petrochem Co Ltd ブテンポリマー処理における分解反応抑制方法
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102202777B1 (ko) * 2019-09-16 2021-01-13 한화토탈 주식회사 비반응성 폴리부텐의 제조시 원료의 재순환 장치 및 그 방법

Also Published As

Publication number Publication date
MY182889A (en) 2021-02-05
KR20150014632A (ko) 2015-02-09
EP3029075A4 (en) 2017-04-12
BR112016001935B1 (pt) 2022-11-16
US9637576B2 (en) 2017-05-02
EP3029075A1 (en) 2016-06-08
CN105452304A (zh) 2016-03-30
EP3029075B1 (en) 2023-09-20
EP3029075C0 (en) 2023-09-20
WO2015016577A1 (ko) 2015-02-05
CN105452304B (zh) 2017-09-01
JP6731848B2 (ja) 2020-07-29
SG11201600697QA (en) 2016-03-30
JP2016530251A (ja) 2016-09-29
US20160176994A1 (en) 2016-06-23
BR112016001935A2 (enExample) 2017-08-29
SA516370500B1 (ar) 2017-12-21

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