CN105452304B - 用于再循环制备聚丁烯时所用的原料的装置和方法 - Google Patents

用于再循环制备聚丁烯时所用的原料的装置和方法 Download PDF

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Publication number
CN105452304B
CN105452304B CN201480043574.5A CN201480043574A CN105452304B CN 105452304 B CN105452304 B CN 105452304B CN 201480043574 A CN201480043574 A CN 201480043574A CN 105452304 B CN105452304 B CN 105452304B
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polybutene
catalyst
reactor
organic solvent
reaction
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Chinese (zh)
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CN105452304A (zh
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金明奭
朴敏燮
闵庚台
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DL Chemical Co Ltd
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Daelim Industrial Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F110/04—Monomers containing three or four carbon atoms
    • C08F110/08—Butenes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/01—Processes of polymerisation characterised by special features of the polymerisation apparatus used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0457—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being placed in separate reactors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F10/04—Monomers containing three or four carbon atoms
    • C08F10/08—Butenes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C08F6/003—Removal of residual monomers by physical means from polymer solutions, suspensions, dispersions or emulsions without recovery of the polymer therefrom
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/02—Neutralisation of the polymerisation mass, e.g. killing the catalyst also removal of catalyst residues
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/02—Recovery or working-up of waste materials of solvents, plasticisers or unreacted monomers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
CN201480043574.5A 2013-07-30 2014-07-29 用于再循环制备聚丁烯时所用的原料的装置和方法 Active CN105452304B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
KR20130090023A KR101511701B1 (ko) 2013-07-30 2013-07-30 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법
KR10-2013-0090023 2013-07-30
PCT/KR2014/006933 WO2015016577A1 (ko) 2013-07-30 2014-07-29 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법

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CN105452304A CN105452304A (zh) 2016-03-30
CN105452304B true CN105452304B (zh) 2017-09-01

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US (1) US9637576B2 (enExample)
EP (1) EP3029075B1 (enExample)
JP (1) JP6731848B2 (enExample)
KR (1) KR101511701B1 (enExample)
CN (1) CN105452304B (enExample)
BR (1) BR112016001935B1 (enExample)
MY (1) MY182889A (enExample)
SA (1) SA516370500B1 (enExample)
SG (1) SG11201600697QA (enExample)
WO (1) WO2015016577A1 (enExample)

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Publication number Priority date Publication date Assignee Title
KR101511701B1 (ko) * 2013-07-30 2015-04-13 대림산업 주식회사 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법
KR101511708B1 (ko) * 2013-08-28 2015-04-13 대림산업 주식회사 폴리부텐 제조 시 발생되는 할로겐의 제거 장치 및 방법
KR101988508B1 (ko) * 2015-10-29 2019-09-30 주식회사 엘지화학 스티렌-부타디엔 용액 중합 시 용매 내 불순물 저감 방법
CN106832070B (zh) * 2017-02-27 2020-07-14 山东省滕州瑞达化工有限公司 用于连续生产聚丁烯-1的方法及装置
KR102351986B1 (ko) * 2019-01-18 2022-01-18 주식회사 엘지화학 폴리부텐의 분리방법
KR102203006B1 (ko) * 2019-04-24 2021-01-13 대림산업 주식회사 고반응성 폴리부텐의 제조 방법
KR102202777B1 (ko) * 2019-09-16 2021-01-13 한화토탈 주식회사 비반응성 폴리부텐의 제조시 원료의 재순환 장치 및 그 방법
CN115725010A (zh) * 2023-01-05 2023-03-03 浙江信汇新材料股份有限公司 一种中、高分子量聚异丁烯制备方法及其引发体系、应用

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JP4907771B2 (ja) * 2001-01-29 2012-04-04 Ｊｘ日鉱日石エネルギー株式会社 ブテンポリマー処理における分解反応抑制方法
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Publication number Publication date
US9637576B2 (en) 2017-05-02
KR20150014632A (ko) 2015-02-09
SG11201600697QA (en) 2016-03-30
WO2015016577A1 (ko) 2015-02-05
EP3029075A1 (en) 2016-06-08
JP6731848B2 (ja) 2020-07-29
SA516370500B1 (ar) 2017-12-21
US20160176994A1 (en) 2016-06-23
KR101511701B1 (ko) 2015-04-13
BR112016001935B1 (pt) 2022-11-16
BR112016001935A2 (enExample) 2017-08-29
CN105452304A (zh) 2016-03-30
EP3029075B1 (en) 2023-09-20
EP3029075A4 (en) 2017-04-12
EP3029075C0 (en) 2023-09-20
JP2016530251A (ja) 2016-09-29
MY182889A (en) 2021-02-05

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Effective date of registration: 20210827

Address after: 134 Tongyi Road, Chung Road, Seoul, Korea

Patentee after: DL Chemical Co.,Ltd.

Address before: Zhonglu District, Seoul Special City, Korea

Patentee before: DAELIM INDUSTRIAL Co.,Ltd.