KR101195783B1 - 폴리실록산 가수분해산물의 중화방법 - Google Patents

폴리실록산 가수분해산물의 중화방법 Download PDF

Info

Publication number
KR101195783B1
KR101195783B1 KR1020077015944A KR20077015944A KR101195783B1 KR 101195783 B1 KR101195783 B1 KR 101195783B1 KR 1020077015944 A KR1020077015944 A KR 1020077015944A KR 20077015944 A KR20077015944 A KR 20077015944A KR 101195783 B1 KR101195783 B1 KR 101195783B1
Authority
KR
South Korea
Prior art keywords
carbon
polysiloxane
hydrolyzate
hydrolysates
neutralized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020077015944A
Other languages
English (en)
Korean (ko)
Other versions
KR20070099604A (ko
Inventor
로버트 엔. 필립스
찰스 엘. 우스터
Original Assignee
다우 코닝 코포레이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 다우 코닝 코포레이션 filed Critical 다우 코닝 코포레이션
Publication of KR20070099604A publication Critical patent/KR20070099604A/ko
Application granted granted Critical
Publication of KR101195783B1 publication Critical patent/KR101195783B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/06Preparatory processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/12Polysiloxanes containing silicon bound to hydrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/32Post-polymerisation treatment
    • C08G77/34Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Polymers (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Carbon And Carbon Compounds (AREA)
KR1020077015944A 2005-01-13 2005-12-16 폴리실록산 가수분해산물의 중화방법 Expired - Fee Related KR101195783B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US64369505P 2005-01-13 2005-01-13
US60/643,695 2005-01-13
PCT/US2005/046320 WO2006076137A1 (en) 2005-01-13 2005-12-16 Method of neutralizing polysiloxane hydrolyzates

Publications (2)

Publication Number Publication Date
KR20070099604A KR20070099604A (ko) 2007-10-09
KR101195783B1 true KR101195783B1 (ko) 2012-11-05

Family

ID=36218739

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020077015944A Expired - Fee Related KR101195783B1 (ko) 2005-01-13 2005-12-16 폴리실록산 가수분해산물의 중화방법

Country Status (9)

Country Link
US (1) US7479566B2 (enExample)
EP (1) EP1848757B1 (enExample)
JP (1) JP2008527141A (enExample)
KR (1) KR101195783B1 (enExample)
CN (1) CN101084255B (enExample)
AT (1) ATE404612T1 (enExample)
BR (1) BRPI0519857A2 (enExample)
DE (1) DE602005009029D1 (enExample)
WO (1) WO2006076137A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7696293B2 (en) * 2005-05-23 2010-04-13 Dow Corning Corporation Method of neutralizing polysiloxanes containing acidic residuals
JP5101598B2 (ja) 2006-03-31 2012-12-19 ダウ・コーニング・コーポレイション シリコーンポリエーテルの製造方法
CN102284271B (zh) * 2011-06-20 2012-12-19 钟洪兵 一种利用阔叶林木屑制作回收蒸发汽油的活性炭及其制作方法
CN107177344A (zh) * 2017-05-27 2017-09-19 湖北兴瑞化工有限公司 一种以二甲基二氯硅烷水解物为原料生产高透明度107胶的方法
KR20210021453A (ko) * 2018-06-19 2021-02-26 닛산 가가쿠 가부시키가이샤 염류가 제거된 폴리실록산의 제조방법
CN110550773A (zh) * 2019-08-16 2019-12-10 江西蓝星星火有机硅有限公司 一种降低二甲基二氯硅烷水解物中氯离子及其它杂质含量的方法和装置
CN110343248A (zh) * 2019-08-20 2019-10-18 江西蓝星星火有机硅有限公司 一种提高含氢硅油质量的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003327699A (ja) 2002-05-13 2003-11-19 Shin Etsu Chem Co Ltd シリコーン油の精製法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3853933A (en) 1974-01-14 1974-12-10 Gen Electric Continuous process for producing polysiloxane oils utilizing a carbon black catalyst
JPS5938993B2 (ja) 1980-03-11 1984-09-20 電気化学工業株式会社 カ−ボンブラックの製造装置
US4382145A (en) 1981-09-02 1983-05-03 General Electric Company Method of hydrolyzing organochlorosilanes
US5075479A (en) * 1991-05-20 1991-12-24 Dow Corning Corporation Anhydrous hydrogen chloride evolving one-step process for producing siloxanes
JP2885295B2 (ja) 1991-11-22 1999-04-19 信越化学工業株式会社 シロキサン類の精製方法
US5276173A (en) * 1992-10-05 1994-01-04 Dow Corning Corporation Method for removal for ionic chloride from hydroxyl-terminated siloxanes
US5766565A (en) * 1993-01-21 1998-06-16 Dow Corning Corporation Purification of hydrochloric acid
US5483040A (en) 1993-02-05 1996-01-09 Fortune; William S. Electrically heated hot gas soldering instrument
DE4422813A1 (de) * 1994-06-29 1996-01-04 Wacker Chemie Gmbh Verfahren zum Stabilisieren von Organpolysiloxanen
MXPA02004706A (es) 1999-11-10 2002-09-02 Gen Electric Procedimiento para estabilizar compuestos de siloxano.
JP2004083883A (ja) * 2002-06-27 2004-03-18 Dow Corning Toray Silicone Co Ltd オルガノポリシロキサンレジンの製造方法
DE102004019377A1 (de) 2004-04-21 2005-11-10 Wacker-Chemie Gmbh Verfahren zur Herstellung von linearen Si-H Gruppen aufweisenden Organopolysiloxanen
US7208617B2 (en) 2004-10-05 2007-04-24 Dow Corning Corporation Hydrolysis of chlorosilanes

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003327699A (ja) 2002-05-13 2003-11-19 Shin Etsu Chem Co Ltd シリコーン油の精製法

Also Published As

Publication number Publication date
KR20070099604A (ko) 2007-10-09
WO2006076137A1 (en) 2006-07-20
EP1848757B1 (en) 2008-08-13
ATE404612T1 (de) 2008-08-15
WO2006076137B1 (en) 2006-09-14
CN101084255B (zh) 2010-10-27
US20080125600A1 (en) 2008-05-29
US7479566B2 (en) 2009-01-20
BRPI0519857A2 (pt) 2009-03-24
EP1848757A1 (en) 2007-10-31
JP2008527141A (ja) 2008-07-24
CN101084255A (zh) 2007-12-05
DE602005009029D1 (de) 2008-09-25

Similar Documents

Publication Publication Date Title
Ochs et al. Coordinative and hydrophobic interaction of humic substances with hydrophilic Al2O3 and hydrophobic mercury surfaces
US6100418A (en) Lessening residual halogen content and improving color number in alkoxysilanes or alkoxysilane-based compositions
AU1227101A (en) Process for removal of odors from silicones
KR101195783B1 (ko) 폴리실록산 가수분해산물의 중화방법
DE102008054537A1 (de) Entfernung von Fremdmetallen aus Siliciumverbindungen durch Adsorption und/oder Filtration
JPS62142188A (ja) シロキサンの精製法
US5445742A (en) Process for purifying halosilanes
US4962221A (en) Chloride reduction in polysiloxanes
Channa et al. Design of experiment for treatment of arsenic-contaminated water using Schiff’s base metal complex modified Amberlite XAD-2
EP0592149A2 (en) Method for removal of ionic chloride from hydroxyl-terminated siloxanes
CA2466169C (en) Solid materials for removing metals and fabrication method
JPH1033975A (ja) 無機粉末を疎水性にする方法
US20090270646A1 (en) Method for preparation of alkoxysilanes having reduced halide
US6168652B1 (en) Process for purifying halosilanes
US5569775A (en) Process for separation of dimethyldichlorosilane from methyltrichlorosilane
US7696293B2 (en) Method of neutralizing polysiloxanes containing acidic residuals
EP1362878B1 (en) Purification of silicone oil
Tighadouini et al. Adsorption of Cu (II) onto novel silica gel-immobilized bithiophene tripodal receptor
US6030660A (en) Method of steam stripping an inorganic powder
TWI878228B (zh) 除去鹽類之聚矽氧烷之製造方法
EP0776902A1 (en) Process for separation of methyltrichlorosilane from dimethyldichlorosilane
Goldberg A stability study of octadecylalumina columns for use in HPLC
JPH0376303B2 (enExample)
Bhakta et al. Impregnation of Cupper into Kanuma Volcanic Ash Soil to Improve Mercury Sorption Capacity
AU2005232258A1 (en) Process for removal of odors from silicones

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R18-X000 Changes to party contact information recorded

St.27 status event code: A-3-3-R10-R18-oth-X000

PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20151025

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20151025

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000