KR100697967B1 - 디알킬포스핀산 염의 제조방법 - Google Patents

디알킬포스핀산 염의 제조방법 Download PDF

Info

Publication number
KR100697967B1
KR100697967B1 KR1020007005782A KR20007005782A KR100697967B1 KR 100697967 B1 KR100697967 B1 KR 100697967B1 KR 1020007005782 A KR1020007005782 A KR 1020007005782A KR 20007005782 A KR20007005782 A KR 20007005782A KR 100697967 B1 KR100697967 B1 KR 100697967B1
Authority
KR
South Korea
Prior art keywords
metal
mixture
acid
free radical
process according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020007005782A
Other languages
English (en)
Korean (ko)
Other versions
KR20010032539A (ko
Inventor
콜베권터
베페를링노르베르트
Original Assignee
클라리안트 프로두크테 (도이칠란트) 게엠베하
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26041979&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR100697967(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 클라리안트 프로두크테 (도이칠란트) 게엠베하 filed Critical 클라리안트 프로두크테 (도이칠란트) 게엠베하
Publication of KR20010032539A publication Critical patent/KR20010032539A/ko
Application granted granted Critical
Publication of KR100697967B1 publication Critical patent/KR100697967B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/30Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Catalysts (AREA)
KR1020007005782A 1997-11-28 1998-11-17 디알킬포스핀산 염의 제조방법 Expired - Fee Related KR100697967B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
DE19752726 1997-11-28
DE19752726.4 1997-11-28
DE19851768.8 1998-11-10
DE19851768A DE19851768C2 (de) 1997-11-28 1998-11-10 Verfahren zur Herstellung von Dialkylphosphinsäuresalzen
PCT/EP1998/007352 WO1999028329A1 (de) 1997-11-28 1998-11-17 Verfahren zur herstellung von dialkylphosphinsäuresalzen

Publications (2)

Publication Number Publication Date
KR20010032539A KR20010032539A (ko) 2001-04-25
KR100697967B1 true KR100697967B1 (ko) 2007-03-23

Family

ID=26041979

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020007005782A Expired - Fee Related KR100697967B1 (ko) 1997-11-28 1998-11-17 디알킬포스핀산 염의 제조방법

Country Status (13)

Country Link
US (1) US5973194A (enExample)
EP (1) EP1036080B1 (enExample)
JP (1) JP4113669B2 (enExample)
KR (1) KR100697967B1 (enExample)
CN (1) CN1142167C (enExample)
AT (1) ATE217628T1 (enExample)
AU (1) AU1338999A (enExample)
CA (1) CA2311925C (enExample)
DE (2) DE19851768C2 (enExample)
ES (1) ES2177092T3 (enExample)
TW (1) TW496883B (enExample)
WO (1) WO1999028329A1 (enExample)
ZA (1) ZA9810913B (enExample)

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19614424A1 (de) 1996-04-12 1997-10-16 Hoechst Ag Synergistische Flammschutzmittel-Kombination für Polymere
DE19828863C1 (de) * 1998-06-29 1999-09-02 Clariant Gmbh Verfahren zur Herstellung von Phosphinsäureestern und deren Verwendung
DE19903707C2 (de) * 1999-01-30 2003-05-28 Clariant Gmbh Flammwidrige duroplastische Massen
DE19923619C2 (de) 1999-05-25 2001-08-23 Clariant Gmbh Verfahren zur Herstellung von Dialkylphosphinsäuren und deren Salzen
DE19923830C1 (de) * 1999-05-25 2001-02-01 Clariant Gmbh Verfahren zur Herstellung von Metallsalzen von Alkylphosphonigen Säuren I
DE19923615C1 (de) * 1999-05-25 2000-12-14 Clariant Gmbh Verfahren zur Herstellung von Alkylphosphonigsäureestern
DE19923743C2 (de) * 1999-05-25 2002-03-07 Clariant Gmbh Verfahren zur Herstellung von (Metall)salzen von Alkylphosphonigen Säuren II
DE10244576A1 (de) * 2002-09-25 2004-04-08 Clariant Gmbh Flammwidrige duroplastische Massen
DE10244579A1 (de) * 2002-09-25 2004-04-08 Clariant Gmbh Flammwidrige duroplastische Massen
DE10244578A1 (de) * 2002-09-25 2004-04-08 Clariant Gmbh Flammwidrige duroplastische Massen
KR100863282B1 (ko) * 2006-09-14 2008-10-15 동국대학교 산학협력단 수산화 금속 인산염 제조방법
ES2365987T3 (es) * 2007-07-13 2011-10-14 Italmatch Chemicals S.P.A. Aditivo retardador de la llama libre de halógeno.
DE102007032669A1 (de) * 2007-07-13 2009-01-15 Clariant International Limited Alkylphosphonigsäuren, -salze und -ester, Verfahren zu deren Herstellung und ihre Verwendung
ES2525550T3 (es) * 2008-11-07 2014-12-26 Clariant Finance (Bvi) Limited Procedimiento para la preparación de ácidos, ésteres y sales dialquilfosfínicos mediante derivados del ácido acrílico y su uso
JP5743219B2 (ja) * 2008-11-11 2015-07-01 クラリアント・ファイナンス・(ビーブイアイ)・リミテッド アリル化合物を用いる、モノアリル官能性ジアルキルホスフィン酸、それらの塩およびエステルの製造方法およびそれらの使用
CN101665516B (zh) * 2009-10-20 2013-05-08 王彦林 酰乙基苯基次膦酰肼或其金属盐以及其制备方法
JP5468944B2 (ja) 2010-03-12 2014-04-09 矢崎総業株式会社 押出しフレキシブルフラットケーブル
CN101906117B (zh) * 2010-07-01 2013-01-09 叶金标 一种烷基次膦酸盐聚合物及其制备方法和应用
CN102020673B (zh) * 2010-12-07 2011-10-19 江西科技师范学院 常压合成二(2,4,4-三甲基戊基)次膦酸的方法
CN102225999B (zh) * 2011-04-20 2015-04-29 苏州科技学院 一种含氮有机次膦酸金属盐及其制备方法
WO2013045965A1 (en) 2011-09-28 2013-04-04 Italmatch Chemicals S.P.A. Halogen-free flame retardant polyesters composition
CN103946289B (zh) 2011-09-28 2017-03-29 伊塔尔麦奇化学股份公司 无卤素阻燃聚酰胺组合物
CN102617638B (zh) * 2012-03-02 2014-08-27 山东兄弟科技股份有限公司 二烷基次膦酸盐的常压两相相转移催化合成工艺
CN103172670B (zh) * 2013-03-04 2015-09-30 广州金凯新材料有限公司 一种单烷基/二烷基次膦酸盐及其制备方法
CN103172668A (zh) * 2013-03-04 2013-06-26 广州金凯新材料有限公司 一种单烷基/二烷基次膦酸盐及其制备方法
KR102096137B1 (ko) 2013-12-12 2020-04-01 이탈마치 케미칼스 에스피에이 글로우 와이어 및 내화성을 가지는 무-할로겐 난연제 폴리아미드 성형 조성물
US9802970B2 (en) * 2014-04-01 2017-10-31 Ningbo Inst. Of Materials Tech. & Eng., Chinese Acad. Of Sciences Process for preparing dialkylphosphinate and a product thereof
CN104725666B (zh) * 2015-03-16 2017-10-17 四川大学 具有高耐热性杂化阻燃剂及其制备方法和应用
CN107974003B (zh) * 2017-10-20 2020-08-07 安徽易恒信息科技有限公司 空间租赁用阻燃隔断墙的制备方法
KR102675718B1 (ko) 2018-12-03 2024-06-14 이탈마치 케미칼스 에스피에이 무기 하이포아인산 금속염을 포함하는 폴리올레핀 무할로겐 난연 성형 조성물
EP3947601B1 (en) 2019-04-02 2023-09-20 Italmatch Chemicals S.p.A. Non-flammable hypophosphite metal salt based powders and their use as flame retardant ingredients
CN111116988B (zh) 2020-01-07 2020-11-20 威海海润新材料科技有限公司 一种有机磷化物阻燃剂及其制备方法与应用
CN113480574B (zh) * 2020-12-10 2024-01-16 洪湖市一泰科技有限公司 一种含磷复合盐的回收利用方法
CN117550569B (zh) * 2023-11-28 2025-09-19 云南云天化股份有限公司 一种生产次磷酸的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2957931A (en) * 1949-07-28 1960-10-25 Socony Mobil Oil Co Inc Synthesis of compounds having a carbonphosphorus linkage
US3579576A (en) * 1964-02-25 1971-05-18 Sun Oil Co Organophosphorus compounds and a process for the making thereof
US3316293A (en) * 1965-07-26 1967-04-25 Hooker Chemical Corp Organic phosphorus compounds
US3488368A (en) * 1967-01-30 1970-01-06 Geigy Chem Corp Metal derivatives of alkylhydroxyphenylalkylphosphinic acids
DE2100779A1 (de) * 1971-01-08 1972-07-20 Farbwerke Hoechst AG vormals Meister Lucius & Brüning, 6000 Frankfurt Verfahren zur Herstellung von Dialkylphosphinsäureestern
US3914345A (en) * 1971-01-08 1975-10-21 Hoechst Ag Process for the manufacture of dialkyl-phosphinic acid esters
DE2447727A1 (de) * 1974-10-07 1976-04-08 Hoechst Ag Schwerentflammbare polyamidformmassen
US4590014A (en) * 1984-09-06 1986-05-20 Economics Laboratory, Inc. Synthesis of alkyl phosphinate salts
US4740332A (en) * 1986-05-12 1988-04-26 E. R. Squibb & Sons, Inc. Process for preparing phosphonous acids
DE4430932A1 (de) * 1994-08-31 1996-03-07 Hoechst Ag Flammgeschützte Polyesterformmasse

Also Published As

Publication number Publication date
DE19851768A1 (de) 1999-06-24
CA2311925C (en) 2009-03-17
JP2001525329A (ja) 2001-12-11
WO1999028329A1 (de) 1999-06-10
DE59804156D1 (de) 2002-06-20
AU1338999A (en) 1999-06-16
JP4113669B2 (ja) 2008-07-09
KR20010032539A (ko) 2001-04-25
CA2311925A1 (en) 1999-06-10
ES2177092T3 (es) 2002-12-01
EP1036080A1 (de) 2000-09-20
US5973194A (en) 1999-10-26
CN1280582A (zh) 2001-01-17
ATE217628T1 (de) 2002-06-15
DE19851768C2 (de) 2000-03-23
TW496883B (en) 2002-08-01
EP1036080B1 (de) 2002-05-15
CN1142167C (zh) 2004-03-17
ZA9810913B (en) 2000-07-11

Similar Documents

Publication Publication Date Title
US5973194A (en) Process for preparing dialkylphosphinate salts
US6534673B1 (en) Process for preparing salts of dialkylphosphinic acids
JP4308427B2 (ja) ジアルキルホスフィン酸の製造方法
US6359171B1 (en) Process for preparing dialkylphosphinic acids and their salts
CN102186863B (zh) 借助丙烯醛制备单羟基官能化的二烷基次膦酸、二烷基次膦酸酯和二烷基次膦酸盐的方法和它们的用途
Dibowski et al. Synthesis and investigation of phosphine ligands containing cationic guanidino functions in aqueous Heck reactions
US6278012B1 (en) Process for preparing phosphinate esters
EP1756126B1 (en) Process for the alkylation of phosphorus-containing compounds
CN102177165A (zh) 用于制备单氨基官能化的二烷基次膦酸、其盐或酯的方法和它们的用途
US6600068B2 (en) Process for preparing ethanebis(methylphosphinic) acid
US6232493B1 (en) Process for preparing metal salts of arylalkylphosphinic acids
CA2641112A1 (en) Use of salts of dialkylphosphinic acids for preparing flame retardants and as additives in polymeric molding compounds
US20040176580A1 (en) Modified polyethylenephosphinic acids and their salts
JP4280307B2 (ja) ビニルホスホン酸化合物の製造方法
DE19851618C2 (de) Verfahren zur Herstellung von Dialkylphosphinsäuren
JPH0544474B2 (enExample)

Legal Events

Date Code Title Description
E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

R15-X000 Change to inventor requested

St.27 status event code: A-3-3-R10-R15-oth-X000

R16-X000 Change to inventor recorded

St.27 status event code: A-3-3-R10-R16-oth-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

E801 Decision on dismissal of amendment
PE0801 Dismissal of amendment

St.27 status event code: A-2-2-P10-P12-nap-PE0801

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

PN2301 Change of applicant

St.27 status event code: A-3-3-R10-R13-asn-PN2301

St.27 status event code: A-3-3-R10-R11-asn-PN2301

J121 Written withdrawal of request for trial
PJ1201 Withdrawal of trial

St.27 status event code: A-3-3-V10-V13-apl-PJ1201

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

FPAY Annual fee payment

Payment date: 20130315

Year of fee payment: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

FPAY Annual fee payment

Payment date: 20140317

Year of fee payment: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

FPAY Annual fee payment

Payment date: 20150316

Year of fee payment: 9

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

FPAY Annual fee payment

Payment date: 20160307

Year of fee payment: 10

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 10

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20170316

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

R17-X000 Change to representative recorded

St.27 status event code: A-5-5-R10-R17-oth-X000

R17-X000 Change to representative recorded

St.27 status event code: A-5-5-R10-R17-oth-X000

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20170316