KR100215228B1 - N-메티롤 아크릴 아미드의 제조방법 - Google Patents

N-메티롤 아크릴 아미드의 제조방법 Download PDF

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Publication number
KR100215228B1
KR100215228B1 KR1019920006067A KR920006067A KR100215228B1 KR 100215228 B1 KR100215228 B1 KR 100215228B1 KR 1019920006067 A KR1019920006067 A KR 1019920006067A KR 920006067 A KR920006067 A KR 920006067A KR 100215228 B1 KR100215228 B1 KR 100215228B1
Authority
KR
South Korea
Prior art keywords
alkali metal
salts
group
alkali
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1019920006067A
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English (en)
Korean (ko)
Other versions
KR920019724A (ko
Inventor
다까야나기야스유끼
다까하시기요브미
나까무라도미오
Original Assignee
나가이 야타로
미쯔비시 레이온 가부시끼가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP3106385A external-priority patent/JPH04316547A/ja
Priority claimed from JP3116666A external-priority patent/JPH04321658A/ja
Priority claimed from JP3216526A external-priority patent/JP3014180B2/ja
Application filed by 나가이 야타로, 미쯔비시 레이온 가부시끼가이샤 filed Critical 나가이 야타로
Publication of KR920019724A publication Critical patent/KR920019724A/ko
Application granted granted Critical
Publication of KR100215228B1 publication Critical patent/KR100215228B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C235/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms
    • C07C235/02—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C235/28—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton being acyclic and unsaturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/08—Preparation of carboxylic acid amides from amides by reaction at nitrogen atoms of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/16—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms
    • C07C233/17—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/20—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a carbon atom of an acyclic unsaturated carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1019920006067A 1991-04-12 1992-04-11 N-메티롤 아크릴 아미드의 제조방법 Expired - Fee Related KR100215228B1 (ko)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
JP3106385A JPH04316547A (ja) 1991-04-12 1991-04-12 Ｎ−メチロールアクリルアミドの製造法
JP91-106385 1991-04-12
JP91-116666 1991-04-22
JP3116666A JPH04321658A (ja) 1991-04-22 1991-04-22 Ｎ−メチロールアクリルアミドの製造方法
JP3216526A JP3014180B2 (ja) 1991-08-02 1991-08-02 結晶状ｎ−メチロールアクリルアミドの製造法
JP91-216523 1991-08-02

Publications (2)

Publication Number Publication Date
KR920019724A KR920019724A (ko) 1992-11-19
KR100215228B1 true KR100215228B1 (ko) 1999-08-16

Family

ID=27310718

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019920006067A Expired - Fee Related KR100215228B1 (ko) 1991-04-12 1992-04-11 N-메티롤 아크릴 아미드의 제조방법

Country Status (5)

Country Link
US (1) US5220065A (enExample)
EP (1) EP0508455B1 (enExample)
KR (1) KR100215228B1 (enExample)
DE (1) DE69206307T2 (enExample)
TW (1) TW226364B (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4423740A1 (de) * 1994-07-06 1996-01-11 Basf Ag Verfahren zur Herstellung von kristallisiertem N-Methylol-(meth)acrylamid
CN1046703C (zh) * 1994-09-16 1999-11-24 三菱丽阳株式会社 N-羟甲基丙烯酰胺结晶及其制造方法以及贮存方法
KR20010078860A (ko) * 2001-04-30 2001-08-22 정성균 고수율의 n-메틸롤 아크릴아미드 용액 제조방법
CN112645831B (zh) * 2020-12-14 2022-12-13 浙江鑫甬生物化工股份有限公司 一种高纯级n-羟甲基丙烯酰胺的合成与结晶方法
CN112939799B (zh) * 2020-12-24 2023-06-27 湖北鑫甬生物环保科技有限公司 一种n-羟甲基丙烯酰胺的合成方法
CN115417784A (zh) * 2022-10-12 2022-12-02 浙江鑫甬生物化工股份有限公司 一种n-羟甲基丙烯酰胺粉剂及水剂产品的联产制备方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2760977A (en) * 1953-06-03 1956-08-28 Research Corp N-alkylol unsaturated amides
US2864861A (en) * 1956-06-05 1958-12-16 American Cyanamid Co Preparation of methylolacrylamide
US3087965A (en) * 1960-12-02 1963-04-30 Pittsburgh Plate Glass Co Preparation of nu-alkoxymethyl substituted amides
US3064050A (en) * 1961-01-03 1962-11-13 American Cyanamid Co Process for the preparation of methylolacrylamide
US3280189A (en) * 1961-11-17 1966-10-18 Devoe & Raynolds Co Preparation of alcohol blocked n-hydroxymethyl unsaturated acid amides
DE1468533A1 (de) * 1963-03-07 1969-03-13 Kuhn Dipl Chem Dr Manfred Verfahren zur Herstellung von N-Methylolmethacrylsaeureamid
US3712926A (en) * 1969-04-25 1973-01-23 Basf Ag Production of n-polyalkoxymethylamides
JPS4914418A (enExample) * 1972-06-10 1974-02-07
JPS5218689B2 (enExample) * 1972-08-11 1977-05-24
JPS49127912A (enExample) * 1973-04-21 1974-12-07
US3887618A (en) * 1974-02-28 1975-06-03 American Cyanamid Co Use of weak base resins as catalysts for the methylolation of acrylamide
JPH0678284B2 (ja) * 1985-12-16 1994-10-05 三菱化成株式会社 Ｎ−メチロ−ルアクリルアミドの製造方法

Also Published As

Publication number Publication date
KR920019724A (ko) 1992-11-19
EP0508455A2 (en) 1992-10-14
TW226364B (enExample) 1994-07-11
US5220065A (en) 1993-06-15
DE69206307T2 (de) 1996-05-15
EP0508455A3 (en) 1993-03-03
DE69206307D1 (de) 1996-01-11
EP0508455B1 (en) 1995-11-29

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