JPS632812A - 磁気記録用板状Ｂａフエライト微粒子粉末の製造法 - Google Patents

Info

Publication number

JPS632812A

JPS632812A JP14770986A JP14770986A JPS632812A JP S632812 A JPS632812 A JP S632812A JP 14770986 A JP14770986 A JP 14770986A JP 14770986 A JP14770986 A JP 14770986A JP S632812 A JPS632812 A JP S632812A

Authority

JP

Japan

Prior art keywords

zinc

particles

ferrite

plate

shaped

Prior art date

1986-06-24

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Granted

Links

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• 229910000859 α-Fe Inorganic materials 0.000 title claims abstract description 77
• 239000000843 powder Substances 0.000 title claims abstract description 12
• 230000005291 magnetic effect Effects 0.000 title claims description 16
• 238000004519 manufacturing process Methods 0.000 title claims description 8
• 239000002245 particle Substances 0.000 claims abstract description 84
• 239000010419 fine particle Substances 0.000 claims abstract description 52
• 230000004907 flux Effects 0.000 claims abstract description 27
• 239000011701 zinc Substances 0.000 claims abstract description 25
• 229940007718 zinc hydroxide Drugs 0.000 claims abstract description 25
• 229910021511 zinc hydroxide Inorganic materials 0.000 claims abstract description 25
• UGZADUVQMDAIAO-UHFFFAOYSA-L zinc hydroxide Chemical compound [OH-].[OH-].[Zn+2] UGZADUVQMDAIAO-UHFFFAOYSA-L 0.000 claims abstract description 24
• 229910052725 zinc Inorganic materials 0.000 claims abstract description 23
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 22
• 238000010438 heat treatment Methods 0.000 claims abstract description 21
• 239000007864 aqueous solution Substances 0.000 claims description 17
• 238000010304 firing Methods 0.000 claims description 16
• 241000276425 Xiphophorus maculatus Species 0.000 claims description 8
• 238000002844 melting Methods 0.000 claims description 7
• 230000008018 melting Effects 0.000 claims description 7
• 238000005406 washing Methods 0.000 claims description 2
• 230000005415 magnetization Effects 0.000 abstract description 38
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract description 8
• JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract description 8
• ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical compound [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 abstract description 6
• 238000001914 filtration Methods 0.000 abstract description 4
• 150000004820 halides Chemical class 0.000 abstract description 4
• 239000011780 sodium chloride Substances 0.000 abstract description 4
• VNDYJBBGRKZCSX-UHFFFAOYSA-L zinc bromide Chemical compound Br[Zn]Br VNDYJBBGRKZCSX-UHFFFAOYSA-L 0.000 abstract description 4
• 239000011592 zinc chloride Substances 0.000 abstract description 4
• 235000005074 zinc chloride Nutrition 0.000 abstract description 4
• UAYWVJHJZHQCIE-UHFFFAOYSA-L zinc iodide Chemical compound I[Zn]I UAYWVJHJZHQCIE-UHFFFAOYSA-L 0.000 abstract description 4
• ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 abstract description 3
• 239000000463 material Substances 0.000 abstract description 3
• 239000004246 zinc acetate Substances 0.000 abstract description 3
• 229910052783 alkali metal Inorganic materials 0.000 abstract description 2
• 150000001340 alkali metals Chemical class 0.000 abstract description 2
• 229910052784 alkaline earth metal Inorganic materials 0.000 abstract description 2
• 150000001342 alkaline earth metals Chemical class 0.000 abstract description 2
• 238000001035 drying Methods 0.000 abstract description 2
• 229940102001 zinc bromide Drugs 0.000 abstract description 2
• NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 abstract description 2
• 229960001763 zinc sulfate Drugs 0.000 abstract description 2
• 229910000368 zinc sulfate Inorganic materials 0.000 abstract description 2
• WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 abstract 2
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
• WDIHJSXYQDMJHN-UHFFFAOYSA-L barium chloride Chemical compound [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 abstract 1
• 229910001626 barium chloride Inorganic materials 0.000 abstract 1
• 238000001354 calcination Methods 0.000 abstract 1
• 238000000034 method Methods 0.000 description 19
• XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 14
• 239000006104 solid solution Substances 0.000 description 11
• 238000001027 hydrothermal synthesis Methods 0.000 description 9
• 239000011787 zinc oxide Substances 0.000 description 7
• 238000004458 analytical method Methods 0.000 description 6
• 230000000052 comparative effect Effects 0.000 description 6
• 239000000126 substance Substances 0.000 description 6
• 238000005245 sintering Methods 0.000 description 5
• 239000012670 alkaline solution Substances 0.000 description 4
• 238000000151 deposition Methods 0.000 description 4
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
• 238000002441 X-ray diffraction Methods 0.000 description 3
• 238000006243 chemical reaction Methods 0.000 description 3
• 230000000694 effects Effects 0.000 description 3
• 238000001704 evaporation Methods 0.000 description 3
• 239000007858 starting material Substances 0.000 description 3
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 description 2
• 239000003638 chemical reducing agent Substances 0.000 description 2
• 239000003795 chemical substances by application Substances 0.000 description 2
• 239000013078 crystal Substances 0.000 description 2
• 230000005294 ferromagnetic effect Effects 0.000 description 2
• 238000010335 hydrothermal treatment Methods 0.000 description 2
• 150000002500 ions Chemical class 0.000 description 2
• 239000000696 magnetic material Substances 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• 239000000725 suspension Substances 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
• 229910000831 Steel Inorganic materials 0.000 description 1
• 229910001422 barium ion Inorganic materials 0.000 description 1
• WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 1
• 229910002091 carbon monoxide Inorganic materials 0.000 description 1
• 238000000975 co-precipitation Methods 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 238000009826 distribution Methods 0.000 description 1
• 238000000635 electron micrograph Methods 0.000 description 1
• 238000005516 engineering process Methods 0.000 description 1
• 230000005307 ferromagnetism Effects 0.000 description 1
• 239000010436 fluorite Substances 0.000 description 1
• 238000005755 formation reaction Methods 0.000 description 1
• 239000011521 glass Substances 0.000 description 1
• 238000007496 glass forming Methods 0.000 description 1
• 229910000042 hydrogen bromide Inorganic materials 0.000 description 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
• 239000006249 magnetic particle Substances 0.000 description 1
• 230000005389 magnetism Effects 0.000 description 1
• 239000000155 melt Substances 0.000 description 1
• 229910021645 metal ion Inorganic materials 0.000 description 1
• 238000002156 mixing Methods 0.000 description 1
• 229910017604 nitric acid Inorganic materials 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000012827 research and development Methods 0.000 description 1
• 239000010959 steel Substances 0.000 description 1
• 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
• 230000002195 synergetic effect Effects 0.000 description 1

Cited By (1)