JPS623822B2 - - Google Patents
Info
- Publication number
- JPS623822B2 JPS623822B2 JP10597579A JP10597579A JPS623822B2 JP S623822 B2 JPS623822 B2 JP S623822B2 JP 10597579 A JP10597579 A JP 10597579A JP 10597579 A JP10597579 A JP 10597579A JP S623822 B2 JPS623822 B2 JP S623822B2
- Authority
- JP
- Japan
- Prior art keywords
- perfluoro
- oxa
- acid
- reaction
- fluorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 15
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 10
- 229910052731 fluorine Inorganic materials 0.000 claims description 10
- 239000011737 fluorine Substances 0.000 claims description 10
- SEWVLHHZBCQYLV-UHFFFAOYSA-N OC(=O)C(F)(F)C(F)(F)C(F)(F)OC(F)=C(F)C(F)(F)F Chemical class OC(=O)C(F)(F)C(F)(F)C(F)(F)OC(F)=C(F)C(F)(F)F SEWVLHHZBCQYLV-UHFFFAOYSA-N 0.000 claims description 8
- JVRUYYNHMKFOIU-UHFFFAOYSA-N 3,3,4,4,5,5-hexafluorooxolan-2-one Chemical compound FC1(F)OC(=O)C(F)(F)C1(F)F JVRUYYNHMKFOIU-UHFFFAOYSA-N 0.000 claims description 7
- 150000001728 carbonyl compounds Chemical class 0.000 claims description 7
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical compound FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 claims description 7
- 229940096017 silver fluoride Drugs 0.000 claims description 6
- REYHXKZHIMGNSE-UHFFFAOYSA-M silver monofluoride Chemical compound [F-].[Ag+] REYHXKZHIMGNSE-UHFFFAOYSA-M 0.000 claims description 6
- YUDUFRYTKFGQCL-UHFFFAOYSA-N 2,2,3,3-tetrafluorobutanedioic acid Chemical class OC(=O)C(F)(F)C(F)(F)C(O)=O YUDUFRYTKFGQCL-UHFFFAOYSA-N 0.000 claims description 4
- 125000005843 halogen group Chemical group 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 15
- 238000000034 method Methods 0.000 description 14
- -1 Perfluoro Chemical group 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- PJUUZEYHOMGCID-UHFFFAOYSA-N 4-prop-1-enoxybutanoyl fluoride Chemical compound C(CCCOC=CC)(=O)F PJUUZEYHOMGCID-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- KNURRSZDMIXZLO-UHFFFAOYSA-N 2,2,3,3-tetrafluorobutanedioyl difluoride Chemical compound FC(=O)C(F)(F)C(F)(F)C(F)=O KNURRSZDMIXZLO-UHFFFAOYSA-N 0.000 description 2
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 2
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 2
- 238000000862 absorption spectrum Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- XJHCXCQVJFPJIK-UHFFFAOYSA-M caesium fluoride Chemical compound [F-].[Cs+] XJHCXCQVJFPJIK-UHFFFAOYSA-M 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 238000001819 mass spectrum Methods 0.000 description 2
- RAMYRNBUYHMLMW-UHFFFAOYSA-N methyl 2,2,3,3,4-pentafluoro-4-oxobutanoate Chemical compound COC(=O)C(F)(F)C(F)(F)C(F)=O RAMYRNBUYHMLMW-UHFFFAOYSA-N 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000004611 spectroscopical analysis Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- 150000007960 acetonitrile Chemical class 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 229930188620 butyrolactone Natural products 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 229910000856 hastalloy Inorganic materials 0.000 description 1
- OPHKTJOQYYTIMJ-UHFFFAOYSA-N hex-4-enyl hydrogen carbonate Chemical class CC=CCCCOC(=O)O OPHKTJOQYYTIMJ-UHFFFAOYSA-N 0.000 description 1
- PGFXOWRDDHCDTE-UHFFFAOYSA-N hexafluoropropylene oxide Chemical compound FC(F)(F)C1(F)OC1(F)F PGFXOWRDDHCDTE-UHFFFAOYSA-N 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000000269 nucleophilic effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- VBKNTGMWIPUCRF-UHFFFAOYSA-M potassium;fluoride;hydrofluoride Chemical compound F.[F-].[K+] VBKNTGMWIPUCRF-UHFFFAOYSA-M 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10597579A JPS5655336A (en) | 1979-08-22 | 1979-08-22 | Perfluoro 5-oxa-6-octenoic acid derivative and its preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10597579A JPS5655336A (en) | 1979-08-22 | 1979-08-22 | Perfluoro 5-oxa-6-octenoic acid derivative and its preparation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5655336A JPS5655336A (en) | 1981-05-15 |
| JPS623822B2 true JPS623822B2 (de) | 1987-01-27 |
Family
ID=14421755
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10597579A Granted JPS5655336A (en) | 1979-08-22 | 1979-08-22 | Perfluoro 5-oxa-6-octenoic acid derivative and its preparation |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5655336A (de) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20200096927A (ko) | 2017-12-13 | 2020-08-14 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 퍼플루오르화 1-알콕시프로펜, 조성물, 및 이를 사용하기 위한 방법 및 장치 |
| JP7295858B2 (ja) | 2017-12-13 | 2023-06-21 | スリーエム イノベイティブ プロパティズ カンパニー | ハイドロフルオロオレフィンエーテル、組成物、これらを使用するための装置及び方法 |
| CN111433865B (zh) | 2017-12-13 | 2021-11-09 | 3M创新有限公司 | 电介质流体和电气装置中的全氟化1-烷氧基丙烯 |
-
1979
- 1979-08-22 JP JP10597579A patent/JPS5655336A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5655336A (en) | 1981-05-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR840001980B1 (ko) | 산 플루오라이드 단량체의 제조방법 | |
| US6388139B1 (en) | Production of perfluoro (alkyl vinyl) ethers | |
| JPS6226240A (ja) | ヘキサフルオルブタジエン及び高級ペルフルオル化ジエンの合成方法 | |
| JPS6145972B2 (de) | ||
| JPS63132851A (ja) | フルオルアルキルペルフルオルビニルエーテルの製造方法 | |
| KR20050105487A (ko) | 4-플루오로-1,3-디옥솔란-2-온의 제조 방법 | |
| GB2219292A (en) | Process of preparing 1,2,2,2-tetrafluoroethyl-difluoromethyl ether | |
| JP2562918B2 (ja) | ハロゲン化ポリエーテルの製造方法 | |
| JPS623822B2 (de) | ||
| JP2589108B2 (ja) | ペルフルオルアルカンジエンの合成方法 | |
| US4362672A (en) | Process for producing difluorohaloacetyl fluoride | |
| US5519151A (en) | Process for preparing polyfluorooxetanes | |
| JP3435596B2 (ja) | エポキシド | |
| JPS58194826A (ja) | ヘキサフルオロイソブテンおよび／またはヘキサフルオロブテンの製法 | |
| WO1992003397A1 (en) | Process for producing trifluorinated hydrocarbon compound | |
| JPH04139145A (ja) | パーフルオロ（２―低級アルコキシプロピオン酸）フロリドの製造法 | |
| JPH02152936A (ja) | 新規な分岐したペルフルオロアルキルハロゲン化物およびその製造 | |
| JPH07121904B2 (ja) | 新規な含窒素ペルフルオロアルカノイルペルオキシド及びその製造方法 | |
| US5185477A (en) | Halohydrin commpounds | |
| US4089869A (en) | Process for producing perfluorolactone | |
| US4581472A (en) | Process for preparing a perfluoroacrylic acid ester | |
| JPS59164772A (ja) | ペルフルオロラクタム類の製造方法 | |
| JPH0822823B2 (ja) | 有機化合物のフツ素化剤及び脱シリル化剤 | |
| JPH0637437B2 (ja) | 含窒素ペルフルオロアルキルヨ―ジド及びその製造方法 | |
| JPH09278704A (ja) | モノクロロピナコロンの製造方法 |