JPS6153113A - 湿式法による易焼結性ペロブスカイト及びその固溶体の原料粉末の製造方法 - Google Patents
湿式法による易焼結性ペロブスカイト及びその固溶体の原料粉末の製造方法Info
- Publication number
- JPS6153113A JPS6153113A JP59171244A JP17124484A JPS6153113A JP S6153113 A JPS6153113 A JP S6153113A JP 59171244 A JP59171244 A JP 59171244A JP 17124484 A JP17124484 A JP 17124484A JP S6153113 A JPS6153113 A JP S6153113A
- Authority
- JP
- Japan
- Prior art keywords
- precipitate
- component
- solution
- raw material
- perovskite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 22
- 239000006104 solid solution Substances 0.000 title claims abstract description 15
- 239000002994 raw material Substances 0.000 title claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000034 method Methods 0.000 title abstract description 22
- 239000002244 precipitate Substances 0.000 claims abstract description 47
- 239000000243 solution Substances 0.000 claims abstract description 18
- 229910052751 metal Inorganic materials 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims abstract description 11
- 239000007864 aqueous solution Substances 0.000 claims abstract 4
- 239000001301 oxygen Substances 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- 229910052719 titanium Inorganic materials 0.000 abstract description 11
- 230000001476 alcoholic effect Effects 0.000 abstract description 8
- 238000001354 calcination Methods 0.000 abstract description 6
- 239000002184 metal Substances 0.000 abstract description 6
- 229910052726 zirconium Inorganic materials 0.000 abstract description 5
- 230000015572 biosynthetic process Effects 0.000 abstract description 4
- 229910052745 lead Inorganic materials 0.000 abstract description 3
- 229910052776 Thorium Inorganic materials 0.000 abstract description 2
- 229910052788 barium Inorganic materials 0.000 abstract description 2
- 229910052746 lanthanum Inorganic materials 0.000 abstract description 2
- 229910052758 niobium Inorganic materials 0.000 abstract description 2
- 229910052761 rare earth metal Inorganic materials 0.000 abstract description 2
- 229910052721 tungsten Inorganic materials 0.000 abstract description 2
- 125000004430 oxygen atom Chemical group O* 0.000 abstract 4
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 229910052735 hafnium Inorganic materials 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 229910052706 scandium Inorganic materials 0.000 abstract 1
- 239000010936 titanium Substances 0.000 description 11
- 238000000975 co-precipitation Methods 0.000 description 7
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
- 230000007547 defect Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 150000001450 anions Chemical class 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 210000000941 bile Anatomy 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- -1 chlorine ions Chemical class 0.000 description 2
- 150000004679 hydroxides Chemical class 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 229910019704 Nb2O Inorganic materials 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 235000012501 ammonium carbonate Nutrition 0.000 description 1
- 239000001099 ammonium carbonate Substances 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- RCJVRSBWZCNNQT-UHFFFAOYSA-N dichloridooxygen Chemical compound ClOCl RCJVRSBWZCNNQT-UHFFFAOYSA-N 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 150000004675 formic acid derivatives Chemical class 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- RLJMLMKIBZAXJO-UHFFFAOYSA-N lead nitrate Chemical compound [O-][N+](=O)O[Pb]O[N+]([O-])=O RLJMLMKIBZAXJO-UHFFFAOYSA-N 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 235000012149 noodles Nutrition 0.000 description 1
- 230000005693 optoelectronics Effects 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000011163 secondary particle Substances 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP59171244A JPS6153113A (ja) | 1984-08-18 | 1984-08-18 | 湿式法による易焼結性ペロブスカイト及びその固溶体の原料粉末の製造方法 |
US06/847,148 US4696810A (en) | 1984-08-16 | 1986-04-02 | Wet process for the production of a readily sinterable powder material of perovskite or its solid solution |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP59171244A JPS6153113A (ja) | 1984-08-18 | 1984-08-18 | 湿式法による易焼結性ペロブスカイト及びその固溶体の原料粉末の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6153113A true JPS6153113A (ja) | 1986-03-17 |
JPS6214488B2 JPS6214488B2 (enrdf_load_stackoverflow) | 1987-04-02 |
Family
ID=15919713
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP59171244A Granted JPS6153113A (ja) | 1984-08-16 | 1984-08-18 | 湿式法による易焼結性ペロブスカイト及びその固溶体の原料粉末の製造方法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6153113A (enrdf_load_stackoverflow) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3612705A1 (de) | 1985-04-17 | 1986-10-23 | Murata Manufacturing Co., Ltd., Nagaokakyo, Kyoto | Verfahren zur herstellung gepulverter keramischer ausgangsstoffe von komplexen oxiden |
DE3614437A1 (de) | 1985-04-30 | 1986-10-30 | Murata Manufacturing Co., Ltd., Nagaokakyo, Kyoto | Verfahren zur herstellung pulverisierter keramischer rohstoffe komplexer oxide |
JPS62241825A (ja) * | 1986-04-14 | 1987-10-22 | Sumitomo Metal Mining Co Ltd | 赤外線センサー用焦電体磁器の製法 |
JPS62241826A (ja) * | 1986-04-14 | 1987-10-22 | Sumitomo Metal Mining Co Ltd | 赤外線センサー用焦電体磁器製造用微粉末の製法 |
JPS6325223A (ja) * | 1986-07-17 | 1988-02-02 | Natl Inst For Res In Inorg Mater | セラミツク原料粉末の製造方法 |
JPS63265822A (ja) * | 1987-04-23 | 1988-11-02 | Ube Ind Ltd | 低温焼結用複合ペロブスカイトの原料粉末の製造方法 |
JPS63319214A (ja) * | 1987-06-23 | 1988-12-27 | Ube Ind Ltd | コンデンサ−材料用粉末 |
JPH01259583A (ja) * | 1988-04-11 | 1989-10-17 | Mitsui Toatsu Chem Inc | Pb−Ba−Zr−Ti系均一酸化物粉末の合成方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59133172U (ja) * | 1983-01-27 | 1984-09-06 | 株式会社早川製作所 | 調理用鋏 |
-
1984
- 1984-08-18 JP JP59171244A patent/JPS6153113A/ja active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59133172U (ja) * | 1983-01-27 | 1984-09-06 | 株式会社早川製作所 | 調理用鋏 |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3612705A1 (de) | 1985-04-17 | 1986-10-23 | Murata Manufacturing Co., Ltd., Nagaokakyo, Kyoto | Verfahren zur herstellung gepulverter keramischer ausgangsstoffe von komplexen oxiden |
DE3614437A1 (de) | 1985-04-30 | 1986-10-30 | Murata Manufacturing Co., Ltd., Nagaokakyo, Kyoto | Verfahren zur herstellung pulverisierter keramischer rohstoffe komplexer oxide |
JPS62241825A (ja) * | 1986-04-14 | 1987-10-22 | Sumitomo Metal Mining Co Ltd | 赤外線センサー用焦電体磁器の製法 |
JPS62241826A (ja) * | 1986-04-14 | 1987-10-22 | Sumitomo Metal Mining Co Ltd | 赤外線センサー用焦電体磁器製造用微粉末の製法 |
JPS6325223A (ja) * | 1986-07-17 | 1988-02-02 | Natl Inst For Res In Inorg Mater | セラミツク原料粉末の製造方法 |
JPS63265822A (ja) * | 1987-04-23 | 1988-11-02 | Ube Ind Ltd | 低温焼結用複合ペロブスカイトの原料粉末の製造方法 |
JPS63319214A (ja) * | 1987-06-23 | 1988-12-27 | Ube Ind Ltd | コンデンサ−材料用粉末 |
JPH01259583A (ja) * | 1988-04-11 | 1989-10-17 | Mitsui Toatsu Chem Inc | Pb−Ba−Zr−Ti系均一酸化物粉末の合成方法 |
Also Published As
Publication number | Publication date |
---|---|
JPS6214488B2 (enrdf_load_stackoverflow) | 1987-04-02 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EXPY | Cancellation because of completion of term |