JPS6141558B2 - - Google Patents
Info
- Publication number
- JPS6141558B2 JPS6141558B2 JP12241778A JP12241778A JPS6141558B2 JP S6141558 B2 JPS6141558 B2 JP S6141558B2 JP 12241778 A JP12241778 A JP 12241778A JP 12241778 A JP12241778 A JP 12241778A JP S6141558 B2 JPS6141558 B2 JP S6141558B2
- Authority
- JP
- Japan
- Prior art keywords
- aqueous solution
- glucose
- bed
- oligosaccharides
- fructose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920001542 oligosaccharide Polymers 0.000 claims description 103
- 150000002482 oligosaccharides Chemical class 0.000 claims description 103
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 63
- 239000007864 aqueous solution Substances 0.000 claims description 63
- 239000008103 glucose Substances 0.000 claims description 63
- 239000005715 Fructose Substances 0.000 claims description 55
- 229930091371 Fructose Natural products 0.000 claims description 53
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 53
- 235000000346 sugar Nutrition 0.000 claims description 35
- 238000000034 method Methods 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 28
- 238000000605 extraction Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000003463 adsorbent Substances 0.000 claims description 15
- 239000003729 cation exchange resin Substances 0.000 claims description 8
- 229910021536 Zeolite Inorganic materials 0.000 claims description 6
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 6
- 239000010457 zeolite Substances 0.000 claims description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 5
- 150000008163 sugars Chemical class 0.000 claims description 3
- 238000011144 upstream manufacturing Methods 0.000 claims description 3
- 238000000746 purification Methods 0.000 description 15
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 12
- 239000007788 liquid Substances 0.000 description 12
- 239000002994 raw material Substances 0.000 description 8
- 238000000926 separation method Methods 0.000 description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 4
- 229910052788 barium Inorganic materials 0.000 description 4
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 4
- 229910052791 calcium Inorganic materials 0.000 description 4
- 239000011575 calcium Substances 0.000 description 4
- 238000007796 conventional method Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 229910052712 strontium Inorganic materials 0.000 description 4
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 3
- 229940023913 cation exchange resins Drugs 0.000 description 3
- 150000001768 cations Chemical class 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 238000003795 desorption Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002425 crystallisation Methods 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000006317 isomerization reaction Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011591 potassium Chemical group 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 239000011734 sodium Chemical group 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- -1 alkaline earth metal salts Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 150000002016 disaccharides Chemical class 0.000 description 1
- 235000019534 high fructose corn syrup Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 150000004043 trisaccharides Chemical class 0.000 description 1
Landscapes
- Treatment Of Liquids With Adsorbents In General (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12241778A JPS5548400A (en) | 1978-10-04 | 1978-10-04 | Removing of oligosaccharide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12241778A JPS5548400A (en) | 1978-10-04 | 1978-10-04 | Removing of oligosaccharide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5548400A JPS5548400A (en) | 1980-04-07 |
| JPS6141558B2 true JPS6141558B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1986-09-16 |
Family
ID=14835299
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP12241778A Granted JPS5548400A (en) | 1978-10-04 | 1978-10-04 | Removing of oligosaccharide |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5548400A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6067000A (ja) * | 1983-09-19 | 1985-04-17 | 三菱化学株式会社 | マルト−スの分離法 |
| JPS6193192A (ja) * | 1984-10-12 | 1986-05-12 | Sanwa Kosan Kk | オリゴ糖粉末の製造法 |
| JP2001000200A (ja) * | 1999-06-23 | 2001-01-09 | Nippon Rensui Co Ltd | 高果糖異性化糖の製造方法 |
| FI115919B (fi) * | 2002-06-27 | 2005-08-15 | Danisco Sweeteners Oy | Menetelmä kiteytysinhibiittoreiden poistamiseksi monosakkaridisokeriliuoksista |
| JP6820194B2 (ja) * | 2016-12-19 | 2021-01-27 | 日本コーンスターチ株式会社 | 液状甘味料組成物、その製造方法及び飲料の製造方法 |
| CN109053823A (zh) * | 2018-08-10 | 2018-12-21 | 太仓沪试试剂有限公司 | 一种从葡萄糖浆中分离纯化葡萄糖的方法 |
-
1978
- 1978-10-04 JP JP12241778A patent/JPS5548400A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5548400A (en) | 1980-04-07 |
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