JPS61286207A - 窒化ホウ素の製造法 - Google Patents
窒化ホウ素の製造法Info
- Publication number
- JPS61286207A JPS61286207A JP12485885A JP12485885A JPS61286207A JP S61286207 A JPS61286207 A JP S61286207A JP 12485885 A JP12485885 A JP 12485885A JP 12485885 A JP12485885 A JP 12485885A JP S61286207 A JPS61286207 A JP S61286207A
- Authority
- JP
- Japan
- Prior art keywords
- precursor
- heating
- boron nitride
- mixture
- boric acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims description 37
- 229910052582 BN Inorganic materials 0.000 title claims description 34
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 24
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000004327 boric acid Substances 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000000465 moulding Methods 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 150000001923 cyclic compounds Chemical class 0.000 claims description 3
- 239000002243 precursor Substances 0.000 abstract description 35
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 abstract description 19
- 229920000877 Melamine resin Polymers 0.000 abstract description 18
- 238000000354 decomposition reaction Methods 0.000 abstract description 5
- 238000002156 mixing Methods 0.000 abstract description 2
- 125000004122 cyclic group Chemical group 0.000 abstract 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 22
- 235000010338 boric acid Nutrition 0.000 description 19
- 229960002645 boric acid Drugs 0.000 description 19
- 239000000843 powder Substances 0.000 description 13
- 239000007789 gas Substances 0.000 description 10
- 238000000034 method Methods 0.000 description 10
- 239000000047 product Substances 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 229910001873 dinitrogen Inorganic materials 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 238000007664 blowing Methods 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000012467 final product Substances 0.000 description 4
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 238000003763 carbonization Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 239000004484 Briquette Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 229910021538 borax Inorganic materials 0.000 description 2
- 239000004202 carbamide Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 235000010339 sodium tetraborate Nutrition 0.000 description 2
- 239000004328 sodium tetraborate Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- UBMLNOQRNOLESZ-UHFFFAOYSA-N (4,6-diamino-1,3,5-triazin-2-yl)cyanamide Chemical compound NC1=NC(N)=NC(NC#N)=N1 UBMLNOQRNOLESZ-UHFFFAOYSA-N 0.000 description 1
- QLVPICNVQBBOQP-UHFFFAOYSA-N 2-(4,6-diamino-1,3,5-triazin-2-yl)guanidine Chemical compound NC(N)=NC1=NC(N)=NC(N)=N1 QLVPICNVQBBOQP-UHFFFAOYSA-N 0.000 description 1
- YZEZMSPGIPTEBA-UHFFFAOYSA-N 2-n-(4,6-diamino-1,3,5-triazin-2-yl)-1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(NC=2N=C(N)N=C(N)N=2)=N1 YZEZMSPGIPTEBA-UHFFFAOYSA-N 0.000 description 1
- XDVOLDOITVSJGL-UHFFFAOYSA-N 3,7-dihydroxy-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound O1B(O)OB2OB(O)OB1O2 XDVOLDOITVSJGL-UHFFFAOYSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 241000219112 Cucumis Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- YSKUZVBSHIWEFK-UHFFFAOYSA-N ammelide Chemical compound NC1=NC(O)=NC(O)=N1 YSKUZVBSHIWEFK-UHFFFAOYSA-N 0.000 description 1
- MASBWURJQFFLOO-UHFFFAOYSA-N ammeline Chemical compound NC1=NC(N)=NC(O)=N1 MASBWURJQFFLOO-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 208000033365 congenital hypomelinating neuropathy Diseases 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 125000000471 iminomethylidene group Chemical group [H]N=C=* 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- YSRVJVDFHZYRPA-UHFFFAOYSA-N melem Chemical compound NC1=NC(N23)=NC(N)=NC2=NC(N)=NC3=N1 YSRVJVDFHZYRPA-UHFFFAOYSA-N 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- VGTPKLINSHNZRD-UHFFFAOYSA-N oxoborinic acid Chemical compound OB=O VGTPKLINSHNZRD-UHFFFAOYSA-N 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000008674 spewing Effects 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
- 238000003828 vacuum filtration Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Ceramic Products (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12485885A JPS61286207A (ja) | 1985-06-08 | 1985-06-08 | 窒化ホウ素の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12485885A JPS61286207A (ja) | 1985-06-08 | 1985-06-08 | 窒化ホウ素の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61286207A true JPS61286207A (ja) | 1986-12-16 |
| JPH0535083B2 JPH0535083B2 (enrdf_load_html_response) | 1993-05-25 |
Family
ID=14895836
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP12485885A Granted JPS61286207A (ja) | 1985-06-08 | 1985-06-08 | 窒化ホウ素の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61286207A (enrdf_load_html_response) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006188411A (ja) * | 2004-12-28 | 2006-07-20 | General Electric Co <Ge> | 窒化ホウ素の製造方法 |
| JP2009149469A (ja) * | 2007-12-20 | 2009-07-09 | Denki Kagaku Kogyo Kk | 六方晶窒化ホウ素の製造方法 |
| WO2013065556A1 (ja) * | 2011-11-02 | 2013-05-10 | 株式会社カネカ | 窒化ホウ素粉末の連続的製造方法 |
| JP2015107884A (ja) * | 2013-12-03 | 2015-06-11 | 株式会社トクヤマ | 窒化硼素の製造方法 |
| KR20180015683A (ko) | 2015-09-03 | 2018-02-13 | 쇼와 덴코 가부시키가이샤 | 육방정 질화붕소 분말, 그 제조 방법, 수지 조성물 및 수지 시트 |
| WO2018123788A1 (en) | 2016-12-28 | 2018-07-05 | Showa Denko K.K. | Hexagonal boron nitride powder, method for producing same, resin composition and resin sheet |
| WO2018124126A1 (ja) | 2016-12-28 | 2018-07-05 | 昭和電工株式会社 | 六方晶窒化ホウ素粉末、その製造方法、樹脂組成物及び樹脂シート |
| KR20180115673A (ko) | 2016-02-22 | 2018-10-23 | 쇼와 덴코 가부시키가이샤 | 육방정 질화 붕소 분말, 그 제조 방법, 수지 조성물 및 수지 시트 |
| WO2019130869A1 (en) | 2017-12-27 | 2019-07-04 | Showa Denko K.K. | Hexagonal boron nitride powder and method for producing the same, and composition and heat dissipation material using the same |
| CN111377742A (zh) * | 2020-03-23 | 2020-07-07 | 河北工业大学 | 一种三维多孔六方氮化硼的无模板合成方法 |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111453706A (zh) * | 2020-04-27 | 2020-07-28 | 信阳市德福鹏新材料有限公司 | 一种六方氮化硼的合成方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61191505A (ja) * | 1984-10-23 | 1986-08-26 | Natl Inst For Res In Inorg Mater | 窒化ほう素の製造法 |
-
1985
- 1985-06-08 JP JP12485885A patent/JPS61286207A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61191505A (ja) * | 1984-10-23 | 1986-08-26 | Natl Inst For Res In Inorg Mater | 窒化ほう素の製造法 |
Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006188411A (ja) * | 2004-12-28 | 2006-07-20 | General Electric Co <Ge> | 窒化ホウ素の製造方法 |
| JP2009149469A (ja) * | 2007-12-20 | 2009-07-09 | Denki Kagaku Kogyo Kk | 六方晶窒化ホウ素の製造方法 |
| WO2013065556A1 (ja) * | 2011-11-02 | 2013-05-10 | 株式会社カネカ | 窒化ホウ素粉末の連続的製造方法 |
| JPWO2013065556A1 (ja) * | 2011-11-02 | 2015-04-02 | 株式会社カネカ | 窒化ホウ素粉末の連続的製造方法 |
| JP2015107884A (ja) * | 2013-12-03 | 2015-06-11 | 株式会社トクヤマ | 窒化硼素の製造方法 |
| KR20180015683A (ko) | 2015-09-03 | 2018-02-13 | 쇼와 덴코 가부시키가이샤 | 육방정 질화붕소 분말, 그 제조 방법, 수지 조성물 및 수지 시트 |
| US10781352B2 (en) | 2015-09-03 | 2020-09-22 | Showa Denko K.K. | Powder of hexagonal boron nitride, process for producing same, resin composition, and resin sheet |
| KR20180115673A (ko) | 2016-02-22 | 2018-10-23 | 쇼와 덴코 가부시키가이샤 | 육방정 질화 붕소 분말, 그 제조 방법, 수지 조성물 및 수지 시트 |
| WO2018124126A1 (ja) | 2016-12-28 | 2018-07-05 | 昭和電工株式会社 | 六方晶窒化ホウ素粉末、その製造方法、樹脂組成物及び樹脂シート |
| KR20190082952A (ko) | 2016-12-28 | 2019-07-10 | 쇼와 덴코 가부시키가이샤 | 육방정 질화붕소 분말, 그 제조 방법, 수지 조성물 및 수지 시트 |
| KR20190082951A (ko) | 2016-12-28 | 2019-07-10 | 쇼와 덴코 가부시키가이샤 | 육방정 질화붕소 분말, 그 제조 방법, 수지 조성물 및 수지 시트 |
| WO2018123788A1 (en) | 2016-12-28 | 2018-07-05 | Showa Denko K.K. | Hexagonal boron nitride powder, method for producing same, resin composition and resin sheet |
| US11305993B2 (en) | 2016-12-28 | 2022-04-19 | Showa Denko K.K. | Hexagonal boron nitride powder, method for producing same, resin composition and resin sheet |
| US11577957B2 (en) | 2016-12-28 | 2023-02-14 | Showa Denko K.K. | Hexagonal boron nitride powder, method for producing same, resin composition and resin sheet |
| WO2019130869A1 (en) | 2017-12-27 | 2019-07-04 | Showa Denko K.K. | Hexagonal boron nitride powder and method for producing the same, and composition and heat dissipation material using the same |
| KR20200031140A (ko) | 2017-12-27 | 2020-03-23 | 쇼와 덴코 가부시키가이샤 | 육방정 질화붕소 분말 및 그 제조 방법, 및 그것을 사용한 조성물 및 방열재 |
| CN111377742A (zh) * | 2020-03-23 | 2020-07-07 | 河北工业大学 | 一种三维多孔六方氮化硼的无模板合成方法 |
| CN111377742B (zh) * | 2020-03-23 | 2022-04-26 | 河北工业大学 | 一种三维多孔六方氮化硼的无模板合成方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0535083B2 (enrdf_load_html_response) | 1993-05-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |