JPS6126979B2 - - Google Patents

Info

Publication number

JPS6126979B2

JPS6126979B2 JP3920280A JP3920280A JPS6126979B2 JP S6126979 B2 JPS6126979 B2 JP S6126979B2 JP 3920280 A JP3920280 A JP 3920280A JP 3920280 A JP3920280 A JP 3920280A JP S6126979 B2 JPS6126979 B2 JP S6126979B2

Authority

JP

Japan

Prior art keywords

trans

liquid crystal

cyclohexanecarboxylic acid

formula

substituted cyclohexyl

Prior art date

1980-03-27

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Links

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• 239000004973 liquid crystal related substance Substances 0.000 claims description 25
• 239000000203 mixture Substances 0.000 claims description 10
• -1 trans-4-(trans-4'-substituted cyclohexyl)cyclohexanecarboxylic acid Chemical class 0.000 claims description 8
• 150000001875 compounds Chemical class 0.000 claims description 6
• 125000000217 alkyl group Chemical group 0.000 claims description 4
• 125000004432 carbon atom Chemical group C* 0.000 claims description 4
• 150000002148 esters Chemical class 0.000 claims description 4
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
• 239000000126 substance Substances 0.000 description 8
• FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 6
• JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
• NZNMSOFKMUBTKW-UHFFFAOYSA-N cyclohexanecarboxylic acid Chemical compound OC(=O)C1CCCCC1 NZNMSOFKMUBTKW-UHFFFAOYSA-N 0.000 description 4
• 239000000463 material Substances 0.000 description 4
• 239000004988 Nematic liquid crystal Substances 0.000 description 3
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 2
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• VZFUCHSFHOYXIS-UHFFFAOYSA-N cycloheptane carboxylic acid Natural products OC(=O)C1CCCCCC1 VZFUCHSFHOYXIS-UHFFFAOYSA-N 0.000 description 2
• 238000002844 melting Methods 0.000 description 2
• 230000008018 melting Effects 0.000 description 2
• UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
• JMAUQQIVJIRNDQ-UHFFFAOYSA-N 4-heptylcyclohexane-1-carboxylic acid Chemical compound CCCCCCCC1CCC(C(O)=O)CC1 JMAUQQIVJIRNDQ-UHFFFAOYSA-N 0.000 description 1
• POEBGIQSFIJHAX-UHFFFAOYSA-N 4-hexylcyclohexane-1-carboxylic acid Chemical compound CCCCCCC1CCC(C(O)=O)CC1 POEBGIQSFIJHAX-UHFFFAOYSA-N 0.000 description 1
• RVLAXPQGTRTHEV-UHFFFAOYSA-N 4-pentylcyclohexane-1-carboxylic acid Chemical compound CCCCCC1CCC(C(O)=O)CC1 RVLAXPQGTRTHEV-UHFFFAOYSA-N 0.000 description 1
• FLJRBFMGAYFGNF-VVPTUSLJSA-N C(CCCCCC)[C@@H]1CC[C@H](CC1)[C@@H]1CC[C@H](CC1)C(=O)O Chemical compound C(CCCCCC)[C@@H]1CC[C@H](CC1)[C@@H]1CC[C@H](CC1)C(=O)O FLJRBFMGAYFGNF-VVPTUSLJSA-N 0.000 description 1
• XXUSEPRYHRDKFV-CTYIDZIISA-N C1C[C@@H](CCC)CC[C@@H]1C1=CC=C(C#N)C=C1 Chemical compound C1C[C@@H](CCC)CC[C@@H]1C1=CC=C(C#N)C=C1 XXUSEPRYHRDKFV-CTYIDZIISA-N 0.000 description 1
• FURZYCFZFBYJBT-JCNLHEQBSA-N C1C[C@@H](CCCCC)CC[C@@H]1C1=CC=C(C#N)C=C1 Chemical compound C1C[C@@H](CCCCC)CC[C@@H]1C1=CC=C(C#N)C=C1 FURZYCFZFBYJBT-JCNLHEQBSA-N 0.000 description 1
• 239000004986 Cholesteric liquid crystals (ChLC) Substances 0.000 description 1
• VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 1
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
• 239000004990 Smectic liquid crystal Substances 0.000 description 1
• PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
• 210000004027 cell Anatomy 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 210000002858 crystal cell Anatomy 0.000 description 1
• 125000000113 cyclohexyl group Chemical class [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
• 238000001035 drying Methods 0.000 description 1
• 238000000921 elemental analysis Methods 0.000 description 1
• 239000011521 glass Substances 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 230000007935 neutral effect Effects 0.000 description 1
• 239000003921 oil Substances 0.000 description 1
• 230000003287 optical effect Effects 0.000 description 1
• 230000000704 physical effect Effects 0.000 description 1
• 230000000630 rising effect Effects 0.000 description 1
• 229910052814 silicon oxide Inorganic materials 0.000 description 1
• 235000011121 sodium hydroxide Nutrition 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 239000000758 substrate Substances 0.000 description 1
• XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
• 229910001887 tin oxide Inorganic materials 0.000 description 1
• 230000007704 transition Effects 0.000 description 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1