JPS6114144B2 - - Google Patents
Info
- Publication number
- JPS6114144B2 JPS6114144B2 JP51104319A JP10431976A JPS6114144B2 JP S6114144 B2 JPS6114144 B2 JP S6114144B2 JP 51104319 A JP51104319 A JP 51104319A JP 10431976 A JP10431976 A JP 10431976A JP S6114144 B2 JPS6114144 B2 JP S6114144B2
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- coo
- benzyl benzoate
- producing
- ch3coo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 claims description 26
- 238000000034 method Methods 0.000 claims description 22
- 238000006243 chemical reaction Methods 0.000 claims description 20
- QPJVMBTYPHYUOC-UHFFFAOYSA-N methyl benzoate Chemical compound COC(=O)C1=CC=CC=C1 QPJVMBTYPHYUOC-UHFFFAOYSA-N 0.000 claims description 16
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 15
- 229960002903 benzyl benzoate Drugs 0.000 claims description 13
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 239000003054 catalyst Substances 0.000 claims description 8
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 claims description 8
- 229940095102 methyl benzoate Drugs 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 6
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 5
- XLYOFNOQVPJJNP-ZSJDYOACSA-N heavy water Substances [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 claims description 4
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 3
- 238000005809 transesterification reaction Methods 0.000 claims description 3
- 229910005793 GeO 2 Inorganic materials 0.000 claims description 2
- -1 NaCH3COO Substances 0.000 claims description 2
- 239000006227 byproduct Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 description 8
- 238000009835 boiling Methods 0.000 description 6
- 239000002994 raw material Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000005711 Benzoic acid Substances 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910001882 dioxygen Inorganic materials 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- FXLOVSHXALFLKQ-UHFFFAOYSA-N p-tolualdehyde Chemical compound CC1=CC=C(C=O)C=C1 FXLOVSHXALFLKQ-UHFFFAOYSA-N 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10431976A JPS5331639A (en) | 1976-09-02 | 1976-09-02 | Preparation of benzyl benzoate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10431976A JPS5331639A (en) | 1976-09-02 | 1976-09-02 | Preparation of benzyl benzoate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5331639A JPS5331639A (en) | 1978-03-25 |
| JPS6114144B2 true JPS6114144B2 (US06650917-20031118-M00005.png) | 1986-04-17 |
Family
ID=14377605
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10431976A Granted JPS5331639A (en) | 1976-09-02 | 1976-09-02 | Preparation of benzyl benzoate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5331639A (US06650917-20031118-M00005.png) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0114932Y2 (US06650917-20031118-M00005.png) * | 1980-03-19 | 1989-05-02 | ||
| JPH0124629Y2 (US06650917-20031118-M00005.png) * | 1980-09-24 | 1989-07-25 | ||
| DE3128930A1 (de) * | 1981-07-22 | 1983-02-10 | Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe | "probenflaschenwechsler" |
| JPS6113160A (ja) * | 1984-06-28 | 1986-01-21 | Konishiroku Photo Ind Co Ltd | 生化学分析装置 |
| JPH06725B2 (ja) * | 1985-01-29 | 1994-01-05 | ダイセル化学工業株式会社 | 炭酸ジフエニルの製造方法 |
| JPS63150250A (ja) * | 1986-12-12 | 1988-06-22 | Toray Ind Inc | ジベンジルフタレ−ト類の製造法 |
| WO1992018459A1 (en) * | 1991-04-18 | 1992-10-29 | Yoshitomi Pharmaceutical Industries, Ltd. | Benzoic ester compound and production thereof |
| JP2001226323A (ja) | 2000-02-17 | 2001-08-21 | Nippon Steel Chem Co Ltd | 安息香酸ベンジルの回収方法 |
-
1976
- 1976-09-02 JP JP10431976A patent/JPS5331639A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5331639A (en) | 1978-03-25 |
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