JPS61122121A - 酸化イットリウム粉体の製造方法 - Google Patents
酸化イットリウム粉体の製造方法Info
- Publication number
- JPS61122121A JPS61122121A JP59244059A JP24405984A JPS61122121A JP S61122121 A JPS61122121 A JP S61122121A JP 59244059 A JP59244059 A JP 59244059A JP 24405984 A JP24405984 A JP 24405984A JP S61122121 A JPS61122121 A JP S61122121A
- Authority
- JP
- Japan
- Prior art keywords
- rare earth
- earth metal
- powder
- aqueous solution
- hydroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 30
- SIWVEOZUMHYXCS-UHFFFAOYSA-N oxo(oxoyttriooxy)yttrium Chemical compound O=[Y]O[Y]=O SIWVEOZUMHYXCS-UHFFFAOYSA-N 0.000 title claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 31
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 28
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 25
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 22
- -1 rare earth metal salt Chemical class 0.000 claims abstract description 22
- 239000010419 fine particle Substances 0.000 claims abstract description 21
- 239000007864 aqueous solution Substances 0.000 claims abstract description 20
- 239000002245 particle Substances 0.000 claims abstract description 17
- 150000002910 rare earth metals Chemical class 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 11
- 239000006229 carbon black Substances 0.000 claims abstract description 10
- 239000003513 alkali Substances 0.000 claims abstract description 9
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 9
- 239000002244 precipitate Substances 0.000 claims abstract description 9
- 229910001404 rare earth metal oxide Inorganic materials 0.000 claims abstract description 9
- 238000001354 calcination Methods 0.000 claims abstract 3
- 238000000034 method Methods 0.000 claims description 5
- 230000001376 precipitating effect Effects 0.000 claims description 3
- 150000003746 yttrium Chemical class 0.000 claims 1
- 239000000243 solution Substances 0.000 abstract description 7
- NGDQQLAVJWUYSF-UHFFFAOYSA-N 4-methyl-2-phenyl-1,3-thiazole-5-sulfonyl chloride Chemical compound S1C(S(Cl)(=O)=O)=C(C)N=C1C1=CC=CC=C1 NGDQQLAVJWUYSF-UHFFFAOYSA-N 0.000 abstract description 5
- 239000012535 impurity Substances 0.000 abstract description 3
- 238000005245 sintering Methods 0.000 abstract description 3
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 abstract 1
- 230000015271 coagulation Effects 0.000 abstract 1
- 238000005345 coagulation Methods 0.000 abstract 1
- 239000004927 clay Substances 0.000 description 24
- 239000011148 porous material Substances 0.000 description 15
- 238000005054 agglomeration Methods 0.000 description 11
- 230000002776 aggregation Effects 0.000 description 11
- 238000009826 distribution Methods 0.000 description 8
- 239000011164 primary particle Substances 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000000919 ceramic Substances 0.000 description 5
- 238000010304 firing Methods 0.000 description 5
- 239000002689 soil Substances 0.000 description 5
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000002209 hydrophobic effect Effects 0.000 description 3
- 239000004570 mortar (masonry) Substances 0.000 description 3
- 238000000465 moulding Methods 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052727 yttrium Inorganic materials 0.000 description 2
- DEXZEPDUSNRVTN-UHFFFAOYSA-K yttrium(3+);trihydroxide Chemical compound [OH-].[OH-].[OH-].[Y+3] DEXZEPDUSNRVTN-UHFFFAOYSA-K 0.000 description 2
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 235000016496 Panda oleosa Nutrition 0.000 description 1
- 240000000220 Panda oleosa Species 0.000 description 1
- 241001465382 Physalis alkekengi Species 0.000 description 1
- 241000872198 Serjania polyphylla Species 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- KZNMRPQBBZBTSW-UHFFFAOYSA-N [Au]=O Chemical compound [Au]=O KZNMRPQBBZBTSW-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012776 electronic material Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 229910001922 gold oxide Inorganic materials 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- IBSDADOZMZEYKD-UHFFFAOYSA-H oxalate;yttrium(3+) Chemical compound [Y+3].[Y+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O IBSDADOZMZEYKD-UHFFFAOYSA-H 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011163 secondary particle Substances 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000011882 ultra-fine particle Substances 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59244059A JPS61122121A (ja) | 1984-11-19 | 1984-11-19 | 酸化イットリウム粉体の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59244059A JPS61122121A (ja) | 1984-11-19 | 1984-11-19 | 酸化イットリウム粉体の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61122121A true JPS61122121A (ja) | 1986-06-10 |
| JPH0529606B2 JPH0529606B2 (en, 2012) | 1993-05-06 |
Family
ID=17113113
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59244059A Granted JPS61122121A (ja) | 1984-11-19 | 1984-11-19 | 酸化イットリウム粉体の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61122121A (en, 2012) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5466428A (en) * | 1987-06-26 | 1995-11-14 | Rhone-Poulenc Chimie | Morphologically improved ceric oxide particulates |
| JP2002255515A (ja) * | 2000-12-27 | 2002-09-11 | National Institute Of Advanced Industrial & Technology | 金属酸化物微粒子の製造方法 |
| JP2007055880A (ja) * | 2005-07-28 | 2007-03-08 | National Institute Of Advanced Industrial & Technology | 金属酸化物微粒子粉末の製造方法 |
| CN104386732A (zh) * | 2014-11-17 | 2015-03-04 | 赣州有色冶金研究所 | 一种采用吸附隔离剂制备纳米氧化铈的方法与系统 |
| US20150344991A1 (en) * | 2012-12-26 | 2015-12-03 | Hitachi Metals, Ltd. | Method for recovering rare earth element |
-
1984
- 1984-11-19 JP JP59244059A patent/JPS61122121A/ja active Granted
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5466428A (en) * | 1987-06-26 | 1995-11-14 | Rhone-Poulenc Chimie | Morphologically improved ceric oxide particulates |
| JP2002255515A (ja) * | 2000-12-27 | 2002-09-11 | National Institute Of Advanced Industrial & Technology | 金属酸化物微粒子の製造方法 |
| US6780393B2 (en) * | 2000-12-27 | 2004-08-24 | National Institute Of Advanced Industrial Science And Technology | Method of producing fine particles of metal oxide |
| JP2007055880A (ja) * | 2005-07-28 | 2007-03-08 | National Institute Of Advanced Industrial & Technology | 金属酸化物微粒子粉末の製造方法 |
| US20150344991A1 (en) * | 2012-12-26 | 2015-12-03 | Hitachi Metals, Ltd. | Method for recovering rare earth element |
| US10081040B2 (en) * | 2012-12-26 | 2018-09-25 | Hitachi Metals, Ltd. | Method for recovering rare earth element |
| CN104386732A (zh) * | 2014-11-17 | 2015-03-04 | 赣州有色冶金研究所 | 一种采用吸附隔离剂制备纳米氧化铈的方法与系统 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0529606B2 (en, 2012) | 1993-05-06 |
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