JPS6041155B2 - アルミニウム表面を酸化し引続き封孔することにより処理する方法 - Google Patents
アルミニウム表面を酸化し引続き封孔することにより処理する方法Info
- Publication number
- JPS6041155B2 JPS6041155B2 JP52133359A JP13335977A JPS6041155B2 JP S6041155 B2 JPS6041155 B2 JP S6041155B2 JP 52133359 A JP52133359 A JP 52133359A JP 13335977 A JP13335977 A JP 13335977A JP S6041155 B2 JPS6041155 B2 JP S6041155B2
- Authority
- JP
- Japan
- Prior art keywords
- acid
- sealing
- aluminum
- oxidizing
- carried out
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000007789 sealing Methods 0.000 title claims description 41
- 238000000034 method Methods 0.000 title claims description 29
- 229910052782 aluminium Inorganic materials 0.000 title claims description 18
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims description 18
- 230000001590 oxidative effect Effects 0.000 title claims description 6
- 239000000243 solution Substances 0.000 claims description 20
- 239000002253 acid Substances 0.000 claims description 19
- YDSWCNNOKPMOTP-UHFFFAOYSA-N mellitic acid Chemical compound OC(=O)C1=C(C(O)=O)C(C(O)=O)=C(C(O)=O)C(C(O)=O)=C1C(O)=O YDSWCNNOKPMOTP-UHFFFAOYSA-N 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 13
- WLWKIJKUDWYINL-UHFFFAOYSA-N cyclohexane-1,1,2,2,3,3-hexacarboxylic acid Chemical compound OC(=O)C1(C(O)=O)CCCC(C(O)=O)(C(O)=O)C1(C(O)=O)C(O)=O WLWKIJKUDWYINL-UHFFFAOYSA-N 0.000 claims description 12
- 239000011148 porous material Substances 0.000 claims description 11
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 9
- GCAIEATUVJFSMC-UHFFFAOYSA-N benzene-1,2,3,4-tetracarboxylic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1C(O)=O GCAIEATUVJFSMC-UHFFFAOYSA-N 0.000 claims description 6
- 229910000838 Al alloy Inorganic materials 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- RZIPTXDCNDIINL-UHFFFAOYSA-N cyclohexane-1,1,2,2-tetracarboxylic acid Chemical compound OC(=O)C1(C(O)=O)CCCCC1(C(O)=O)C(O)=O RZIPTXDCNDIINL-UHFFFAOYSA-N 0.000 claims description 3
- 238000007743 anodising Methods 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 30
- 238000000576 coating method Methods 0.000 description 25
- 239000011248 coating agent Substances 0.000 description 23
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 6
- 150000007513 acids Chemical class 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 230000007797 corrosion Effects 0.000 description 5
- 238000005260 corrosion Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 230000004580 weight loss Effects 0.000 description 5
- 239000013543 active substance Substances 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- HVBSAKJJOYLTQU-UHFFFAOYSA-N 4-aminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C=C1 HVBSAKJJOYLTQU-UHFFFAOYSA-N 0.000 description 2
- MQRWBMAEBQOWAF-UHFFFAOYSA-N acetic acid;nickel Chemical compound [Ni].CC(O)=O.CC(O)=O MQRWBMAEBQOWAF-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
- -1 inter alia Chemical class 0.000 description 2
- 229940078494 nickel acetate Drugs 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- SDGNNLQZAPXALR-UHFFFAOYSA-N 3-sulfophthalic acid Chemical compound OC(=O)C1=CC=CC(S(O)(=O)=O)=C1C(O)=O SDGNNLQZAPXALR-UHFFFAOYSA-N 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 241001330002 Bambuseae Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229920001732 Lignosulfonate Polymers 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- GTDPSWPPOUPBNX-UHFFFAOYSA-N ac1mqpva Chemical compound CC12C(=O)OC(=O)C1(C)C1(C)C2(C)C(=O)OC1=O GTDPSWPPOUPBNX-UHFFFAOYSA-N 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 229940011182 cobalt acetate Drugs 0.000 description 1
- QAHREYKOYSIQPH-UHFFFAOYSA-L cobalt(II) acetate Chemical compound [Co+2].CC([O-])=O.CC([O-])=O QAHREYKOYSIQPH-UHFFFAOYSA-L 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 229940074391 gallic acid Drugs 0.000 description 1
- 235000004515 gallic acid Nutrition 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 125000005842 heteroatom Chemical group 0.000 description 1
- DPZWPLRSNKLEDZ-UHFFFAOYSA-N hexane-1,1,1,2,2,3-hexacarboxylic acid Chemical compound CCCC(C(O)=O)C(C(O)=O)(C(O)=O)C(C(O)=O)(C(O)=O)C(O)=O DPZWPLRSNKLEDZ-UHFFFAOYSA-N 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- MJGFBOZCAJSGQW-UHFFFAOYSA-N mercury sodium Chemical compound [Na].[Hg] MJGFBOZCAJSGQW-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- MYHXWQZHYLEHIU-UHFFFAOYSA-N oxalic acid;sulfuric acid Chemical compound OS(O)(=O)=O.OC(=O)C(O)=O MYHXWQZHYLEHIU-UHFFFAOYSA-N 0.000 description 1
- 150000003009 phosphonic acids Chemical class 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 238000012031 short term test Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910001023 sodium amalgam Inorganic materials 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 229950000244 sulfanilic acid Drugs 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/18—After-treatment, e.g. pore-sealing
- C25D11/24—Chemical after-treatment
- C25D11/246—Chemical after-treatment for sealing layers
Landscapes
- Chemical & Material Sciences (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Chemical Treatment Of Metals (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Electrochemical Coating By Surface Reaction (AREA)
- Sealing Material Composition (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Superconductors And Manufacturing Methods Therefor (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2650989A DE2650989C2 (de) | 1976-11-08 | 1976-11-08 | Verfahren zur Behandlung von Aluminiumoberflächen durch Oxidation mit einer nachfolgenden Verdichtung |
| DE2650989.7 | 1976-11-08 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5358445A JPS5358445A (en) | 1978-05-26 |
| JPS6041155B2 true JPS6041155B2 (ja) | 1985-09-14 |
Family
ID=5992670
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP52133359A Expired JPS6041155B2 (ja) | 1976-11-08 | 1977-11-07 | アルミニウム表面を酸化し引続き封孔することにより処理する方法 |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US4121980A (enExample) |
| JP (1) | JPS6041155B2 (enExample) |
| AT (1) | AT350870B (enExample) |
| BE (1) | BE860529A (enExample) |
| BR (1) | BR7707444A (enExample) |
| CA (1) | CA1105872A (enExample) |
| CH (1) | CH636131A5 (enExample) |
| DE (1) | DE2650989C2 (enExample) |
| DK (1) | DK148753C (enExample) |
| ES (1) | ES463951A1 (enExample) |
| FR (1) | FR2370110A1 (enExample) |
| GB (1) | GB1574161A (enExample) |
| IT (1) | IT1088144B (enExample) |
| NL (1) | NL7711105A (enExample) |
| NO (1) | NO146245C (enExample) |
| SE (1) | SE427122B (enExample) |
| ZA (1) | ZA776620B (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH654853A5 (de) * | 1982-08-07 | 1986-03-14 | Sandoz Ag | Verfahren zum verdichten von anodisch oxydierten aluminiumoberflaechen. |
| GB8309571D0 (en) * | 1983-04-08 | 1983-05-11 | Albright & Wilson | Accelerated sealing of anodised aluminium |
| DE3820650A1 (de) * | 1988-06-18 | 1989-12-21 | Henkel Kgaa | Verfahren zum verdichten von anodisierten oxidschichten auf aluminium und aluminiumlegierungen |
| US5367196A (en) * | 1992-09-17 | 1994-11-22 | Olin Corporation | Molded plastic semiconductor package including an aluminum alloy heat spreader |
| US5608267A (en) * | 1992-09-17 | 1997-03-04 | Olin Corporation | Molded plastic semiconductor package including heat spreader |
| DE19524828A1 (de) * | 1995-07-07 | 1997-01-09 | Henkel Kgaa | Verfahren zum schwermetallfreien Verdichten anodisierter Metalle mit Lithium- und Fluorid-haltigen Lösungen |
| DE59604329D1 (de) * | 1995-10-18 | 2000-03-02 | Henkel Kgaa | Kurzzeit-heissverdichtung anodisierter metalloberflächen |
| DE19621818A1 (de) * | 1996-05-31 | 1997-12-04 | Henkel Kgaa | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen Lösungen |
| JPH102452A (ja) * | 1996-06-14 | 1998-01-06 | Smc Corp | 高真空バルブ |
| US6664019B2 (en) | 1996-06-19 | 2003-12-16 | Printing Developments Inc. | Aluminum printing plates and method of making |
| CA2300859A1 (en) * | 1997-08-22 | 1999-03-04 | Henkel Corporation | Faster two-step sealing of anodized aluminum surfaces |
| EP1230445A1 (en) * | 1999-11-18 | 2002-08-14 | Houghton Metal Finishing | A sealant composition |
| DE10161478A1 (de) * | 2001-12-14 | 2003-06-26 | Henkel Kgaa | Verfahren zum Verdichten von anodisierten Metalloberflächen im mittleren Temperaturbereich |
| US8609254B2 (en) | 2010-05-19 | 2013-12-17 | Sanford Process Corporation | Microcrystalline anodic coatings and related methods therefor |
| US8512872B2 (en) | 2010-05-19 | 2013-08-20 | Dupalectpa-CHN, LLC | Sealed anodic coatings |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3012917A (en) * | 1957-03-26 | 1961-12-12 | Pechiney Prod Chimiques Sa | Method of protecting metal surfaces |
| US3440150A (en) * | 1966-02-10 | 1969-04-22 | Martin Marietta Corp | Dual-seal anodized aluminum |
| BE792852A (fr) * | 1971-12-17 | 1973-06-15 | Henkel & Cie Gmbh | Procede de traitement de surfaces d'aluminium par oxydation suivie d'une densification |
-
1976
- 1976-11-08 DE DE2650989A patent/DE2650989C2/de not_active Expired
-
1977
- 1977-10-10 SE SE7711380A patent/SE427122B/xx not_active IP Right Cessation
- 1977-10-10 NL NL7711105A patent/NL7711105A/xx not_active Application Discontinuation
- 1977-10-10 DK DK448777A patent/DK148753C/da not_active IP Right Cessation
- 1977-10-10 NO NO773454A patent/NO146245C/no unknown
- 1977-10-28 IT IT29089/77A patent/IT1088144B/it active
- 1977-11-02 US US05/847,773 patent/US4121980A/en not_active Expired - Lifetime
- 1977-11-04 GB GB45906/77A patent/GB1574161A/en not_active Expired
- 1977-11-04 CA CA290,255A patent/CA1105872A/en not_active Expired
- 1977-11-07 AT AT792877A patent/AT350870B/de not_active IP Right Cessation
- 1977-11-07 BR BR7707444A patent/BR7707444A/pt unknown
- 1977-11-07 BE BE182384A patent/BE860529A/xx not_active IP Right Cessation
- 1977-11-07 JP JP52133359A patent/JPS6041155B2/ja not_active Expired
- 1977-11-07 CH CH1352577A patent/CH636131A5/de not_active IP Right Cessation
- 1977-11-07 ZA ZA00776620A patent/ZA776620B/xx unknown
- 1977-11-08 FR FR7733497A patent/FR2370110A1/fr active Granted
- 1977-11-08 ES ES463951A patent/ES463951A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| AT350870B (de) | 1979-06-25 |
| DE2650989A1 (de) | 1978-05-11 |
| US4121980A (en) | 1978-10-24 |
| NO146245B (no) | 1982-05-18 |
| NO146245C (no) | 1982-08-25 |
| ATA792877A (de) | 1978-11-15 |
| DK148753B (da) | 1985-09-16 |
| SE7711380L (sv) | 1978-05-09 |
| NL7711105A (nl) | 1978-05-10 |
| BE860529A (fr) | 1978-05-08 |
| SE427122B (sv) | 1983-03-07 |
| DE2650989C2 (de) | 1985-01-24 |
| CH636131A5 (de) | 1983-05-13 |
| ZA776620B (en) | 1978-08-30 |
| BR7707444A (pt) | 1978-07-18 |
| ES463951A1 (es) | 1978-07-01 |
| IT1088144B (it) | 1985-06-10 |
| JPS5358445A (en) | 1978-05-26 |
| DK148753C (da) | 1986-02-10 |
| FR2370110B1 (enExample) | 1980-10-31 |
| DK448777A (da) | 1978-05-09 |
| GB1574161A (en) | 1980-09-03 |
| NO773454L (no) | 1978-05-09 |
| CA1105872A (en) | 1981-07-28 |
| FR2370110A1 (fr) | 1978-06-02 |
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