JPS585957B2 - 潤滑油の溶媒精製方法 - Google Patents
潤滑油の溶媒精製方法Info
- Publication number
- JPS585957B2 JPS585957B2 JP55140684A JP14068480A JPS585957B2 JP S585957 B2 JPS585957 B2 JP S585957B2 JP 55140684 A JP55140684 A JP 55140684A JP 14068480 A JP14068480 A JP 14068480A JP S585957 B2 JPS585957 B2 JP S585957B2
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- extraction
- zone
- phase
- feedstock
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002904 solvent Substances 0.000 title claims description 145
- 238000000034 method Methods 0.000 title claims description 47
- 238000000746 purification Methods 0.000 title claims description 25
- 239000010687 lubricating oil Substances 0.000 title claims description 23
- 238000000605 extraction Methods 0.000 claims description 70
- 239000000203 mixture Substances 0.000 claims description 37
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical group CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 33
- 239000011261 inert gas Substances 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 29
- 239000007789 gas Substances 0.000 claims description 28
- 239000000284 extract Substances 0.000 claims description 26
- 238000010992 reflux Methods 0.000 claims description 19
- 125000003118 aryl group Chemical group 0.000 claims description 12
- 238000007670 refining Methods 0.000 claims description 11
- 238000001704 evaporation Methods 0.000 claims description 10
- 238000000926 separation method Methods 0.000 claims description 10
- 230000008020 evaporation Effects 0.000 claims description 9
- 238000000638 solvent extraction Methods 0.000 claims description 9
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- 239000000314 lubricant Substances 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims 3
- 230000005494 condensation Effects 0.000 claims 3
- 239000012442 inert solvent Substances 0.000 claims 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 19
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 18
- 239000003921 oil Substances 0.000 description 14
- 238000011084 recovery Methods 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 9
- 238000010521 absorption reaction Methods 0.000 description 8
- 239000012071 phase Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 6
- 239000003208 petroleum Substances 0.000 description 5
- 239000002199 base oil Substances 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 238000007738 vacuum evaporation Methods 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000007701 flash-distillation Methods 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 description 2
- 239000011877 solvent mixture Substances 0.000 description 2
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229910001867 inorganic solvent Inorganic materials 0.000 description 1
- 239000003049 inorganic solvent Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000011403 purification operation Methods 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 239000013557 residual solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
- C10G21/28—Recovery of used solvent
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
- C10G21/06—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
- C10G21/12—Organic compounds only
- C10G21/18—Halogen-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
- C10G2400/10—Lubricating oil
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12157280A | 1980-02-14 | 1980-02-14 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS56116786A JPS56116786A (en) | 1981-09-12 |
JPS585957B2 true JPS585957B2 (ja) | 1983-02-02 |
Family
ID=22397575
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55140684A Expired JPS585957B2 (ja) | 1980-02-14 | 1980-10-09 | 潤滑油の溶媒精製方法 |
Country Status (18)
Country | Link |
---|---|
JP (1) | JPS585957B2 (en)van) |
KR (1) | KR840000578B1 (en)van) |
AU (1) | AU6616381A (en)van) |
BR (1) | BR8007934A (en)van) |
CA (1) | CA1150179A (en)van) |
DE (1) | DE3049204A1 (en)van) |
EG (1) | EG15434A (en)van) |
ES (1) | ES499438A0 (en)van) |
FR (1) | FR2476117A1 (en)van) |
GB (1) | GB2069525B (en)van) |
GR (1) | GR73847B (en)van) |
IT (1) | IT1141967B (en)van) |
MA (1) | MA19063A1 (en)van) |
NL (1) | NL8100515A (en)van) |
PH (1) | PH17150A (en)van) |
PT (1) | PT72462B (en)van) |
YU (1) | YU28781A (en)van) |
ZA (1) | ZA81221B (en)van) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60148444A (ja) * | 1983-12-28 | 1985-08-05 | 日成通商株式会社 | 包装用紐状体 |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2548912B1 (fr) * | 1983-07-13 | 1985-12-13 | Moreno Gilbert | Appareil de musculation destine notamment aux alpinistes |
KR101605053B1 (ko) * | 2009-12-30 | 2016-03-21 | 아이알피씨 퍼블릭 컴퍼니 리미티드 | 낮은 폴리아로마틱 탄화수소 함량을 갖는 프로세스 오일의 제조방법 |
RU2532808C1 (ru) * | 2013-08-20 | 2014-11-10 | Общество с ограниченной ответственностью "ВОКСТЭК" | Способ регенерации растворителя в процессах депарафинизации и обезмасливания |
CN103911172B (zh) * | 2014-04-10 | 2016-06-29 | 辽宁石油化工大学 | 一种超声波辅助柴油溶剂精制的方法 |
RU2651547C1 (ru) * | 2017-06-05 | 2018-04-20 | Общество с ограниченной ответственностью "ВОКСТЭК" | Способ регенерации растворителя в процессах депарафинизации и обезмасливания |
RU2688686C2 (ru) * | 2017-08-21 | 2019-05-22 | Открытое акционерное общество "Славнефть-Ярославнефтеоргсинтез" (ОАО "Славнефть-ЯНОС") | Способ регенерации растворителя в процессах депарафинизации и обезмасливания |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2923680A (en) * | 1956-12-31 | 1960-02-02 | Exxon Research Engineering Co | Extraction process for refining lubricating oils |
US4013549A (en) * | 1972-12-01 | 1977-03-22 | Exxon Research And Engineering Company | Lube extraction with NMP/phenol/water mixtures |
US4057491A (en) * | 1976-03-26 | 1977-11-08 | Exxon Research & Engineering Co. | Solvent recovery process for N-methyl-2-pyrrolidone in hydrocarbon extraction |
-
1980
- 1980-09-02 PH PH24529A patent/PH17150A/en unknown
- 1980-10-09 JP JP55140684A patent/JPS585957B2/ja not_active Expired
- 1980-12-04 BR BR8007934A patent/BR8007934A/pt unknown
- 1980-12-27 DE DE19803049204 patent/DE3049204A1/de not_active Withdrawn
-
1981
- 1981-01-05 GB GB8100118A patent/GB2069525B/en not_active Expired
- 1981-01-13 ZA ZA00810221A patent/ZA81221B/xx unknown
- 1981-01-13 AU AU66163/81A patent/AU6616381A/en not_active Abandoned
- 1981-01-29 CA CA000369680A patent/CA1150179A/en not_active Expired
- 1981-02-03 YU YU00287/81A patent/YU28781A/xx unknown
- 1981-02-03 NL NL8100515A patent/NL8100515A/nl not_active Application Discontinuation
- 1981-02-05 PT PT72462A patent/PT72462B/pt unknown
- 1981-02-09 MA MA19266A patent/MA19063A1/fr unknown
- 1981-02-11 EG EG62/81A patent/EG15434A/xx active
- 1981-02-12 GR GR64111A patent/GR73847B/el unknown
- 1981-02-12 KR KR1019810000413A patent/KR840000578B1/ko not_active Expired
- 1981-02-12 IT IT19704/81A patent/IT1141967B/it active
- 1981-02-13 FR FR8102884A patent/FR2476117A1/fr active Granted
- 1981-02-13 ES ES499438A patent/ES499438A0/es active Granted
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60148444A (ja) * | 1983-12-28 | 1985-08-05 | 日成通商株式会社 | 包装用紐状体 |
Also Published As
Publication number | Publication date |
---|---|
PT72462A (en) | 1981-03-01 |
GB2069525A (en) | 1981-08-26 |
EG15434A (en) | 1986-09-30 |
AU6616381A (en) | 1981-08-20 |
PH17150A (en) | 1984-06-13 |
FR2476117A1 (fr) | 1981-08-21 |
ZA81221B (en) | 1982-05-26 |
MA19063A1 (fr) | 1981-10-01 |
CA1150179A (en) | 1983-07-19 |
ES8202053A1 (es) | 1982-01-01 |
GB2069525B (en) | 1984-02-15 |
KR830005335A (ko) | 1983-08-13 |
PT72462B (en) | 1982-02-04 |
KR840000578B1 (ko) | 1984-04-23 |
YU28781A (en) | 1983-04-30 |
DE3049204A1 (de) | 1981-09-10 |
IT1141967B (it) | 1986-10-08 |
ES499438A0 (es) | 1982-01-01 |
JPS56116786A (en) | 1981-09-12 |
BR8007934A (pt) | 1981-08-25 |
GR73847B (en)van) | 1984-05-07 |
FR2476117B1 (en)van) | 1984-11-09 |
IT8119704A0 (it) | 1981-02-12 |
NL8100515A (nl) | 1981-09-16 |
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