JPS57203056A - Synthesis of sulfonyl chloride - Google Patents
Synthesis of sulfonyl chlorideInfo
- Publication number
- JPS57203056A JPS57203056A JP56088419A JP8841981A JPS57203056A JP S57203056 A JPS57203056 A JP S57203056A JP 56088419 A JP56088419 A JP 56088419A JP 8841981 A JP8841981 A JP 8841981A JP S57203056 A JPS57203056 A JP S57203056A
- Authority
- JP
- Japan
- Prior art keywords
- acid
- sulfolane
- chloride
- formulai
- sulfur
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Abstract
PURPOSE: To prepare the titled compound useful as a dye-releasing agent for color photography, synthetic intermediate of pharmaceuticals, etc., in high purity and yield, by reacting an aromatic sulfonic acid with an acid chloride containing phosphorus or sulfur in the presence of sulfolane.
CONSTITUTION: The sulfonyl chloride of formula II (Ar is aromatic group) can be prepared by reacting the sulfonic acid of formulaIwith an acid chloride containing phosphorus or sulfur, in the presence of sulfolane. The P- or S-containing acid chloride is preferably phosphorus oxychloride, thionyl chloride, etc., and its amount is about 1W20mol per 1mol of the acid of formulaI. The amount of sulfolane is about 50mlW5l per 1mol of the acid of formulaI. The reaction is carried out at 30W100°C usually for about 5minW3hr. The objective compound can be prepared under mild conditions with simple procedure.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56088419A JPS57203056A (en) | 1981-06-09 | 1981-06-09 | Synthesis of sulfonyl chloride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56088419A JPS57203056A (en) | 1981-06-09 | 1981-06-09 | Synthesis of sulfonyl chloride |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS57203056A true JPS57203056A (en) | 1982-12-13 |
JPH0128742B2 JPH0128742B2 (en) | 1989-06-05 |
Family
ID=13942261
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP56088419A Granted JPS57203056A (en) | 1981-06-09 | 1981-06-09 | Synthesis of sulfonyl chloride |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS57203056A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5436370A (en) * | 1990-03-03 | 1995-07-25 | Hoechst Ag | Process for the preparation of 3-nitrobenzenesulfonyl chloride |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5115029A (en) * | 1974-07-26 | 1976-02-06 | Negishi Kogyo Kenkyusho Kk | Jidotamaagehoho oyobi sochi |
JPS54161332A (en) * | 1978-06-09 | 1979-12-20 | Fuji Photo Film Co Ltd | Photographic photosensitive sheet for color diffusion transfer |
-
1981
- 1981-06-09 JP JP56088419A patent/JPS57203056A/en active Granted
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5115029A (en) * | 1974-07-26 | 1976-02-06 | Negishi Kogyo Kenkyusho Kk | Jidotamaagehoho oyobi sochi |
JPS54161332A (en) * | 1978-06-09 | 1979-12-20 | Fuji Photo Film Co Ltd | Photographic photosensitive sheet for color diffusion transfer |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5436370A (en) * | 1990-03-03 | 1995-07-25 | Hoechst Ag | Process for the preparation of 3-nitrobenzenesulfonyl chloride |
Also Published As
Publication number | Publication date |
---|---|
JPH0128742B2 (en) | 1989-06-05 |
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