JPS57140398A - Manufacture of crystal of rare earth element phosphate - Google Patents
Manufacture of crystal of rare earth element phosphateInfo
- Publication number
- JPS57140398A JPS57140398A JP2335081A JP2335081A JPS57140398A JP S57140398 A JPS57140398 A JP S57140398A JP 2335081 A JP2335081 A JP 2335081A JP 2335081 A JP2335081 A JP 2335081A JP S57140398 A JPS57140398 A JP S57140398A
- Authority
- JP
- Japan
- Prior art keywords
- phosphate
- seed crystal
- crystal
- crucible
- temp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01S—DEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
- H01S3/00—Lasers, i.e. devices using stimulated emission of electromagnetic radiation in the infrared, visible or ultraviolet wave range
- H01S3/14—Lasers, i.e. devices using stimulated emission of electromagnetic radiation in the infrared, visible or ultraviolet wave range characterised by the material used as the active medium
- H01S3/16—Solid materials
Landscapes
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- Optics & Photonics (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Lasers (AREA)
Abstract
PURPOSE:To grow a crystal by providing a temp. gradient to phosphoric acid as a medium, placing rare earth element phosphate in the acid at one side where the solubility of the phosphate is higher and a seed crystal at the other side, carrying the phosphate toward the seed crystal after dissolution, and coagulating it on the seed crystal. CONSTITUTION:A heating wire 1b is wound around the heat insulating container 1a of a heating apparatus 1 in the longitudinal direction. A quartz reaction tube 2 is set in the apparatus 1, and an oblong crucible 3 of pure gold or the like with superior resistance to phosphoric acid is set in the tube 2. The crucible 3 is filled with phosphoric acid 4 as a medium, rare earth element phosphate 5 as starting material and a seed crystal 6 are placed in the crucible 3 at one end and a part away from the end, respectively, and the crucible 3 is tightly sealed with a lid 7. A temp. gradient is then provided to the acid 4 with the wire 1b so that a temp. section where the solubility of the phosphate is higher and a temp. section where the solubility is lower are formed at the phosphate placed part and the seed crystal placed part, respectively. The phosphate is dissolved, carried, and coagulated on the seed crystal 6 to grow a crystal.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2335081A JPS57140398A (en) | 1981-02-19 | 1981-02-19 | Manufacture of crystal of rare earth element phosphate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2335081A JPS57140398A (en) | 1981-02-19 | 1981-02-19 | Manufacture of crystal of rare earth element phosphate |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS57140398A true JPS57140398A (en) | 1982-08-30 |
Family
ID=12108127
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2335081A Pending JPS57140398A (en) | 1981-02-19 | 1981-02-19 | Manufacture of crystal of rare earth element phosphate |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS57140398A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103556214A (en) * | 2013-11-15 | 2014-02-05 | 青岛大学 | Method for growing rare earth lutetium phosphate laser host crystal |
-
1981
- 1981-02-19 JP JP2335081A patent/JPS57140398A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103556214A (en) * | 2013-11-15 | 2014-02-05 | 青岛大学 | Method for growing rare earth lutetium phosphate laser host crystal |
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