JPS54106427A - Purification of 2-acrylamide-2-methylpropane sulfonic acid - Google Patents

Purification of 2-acrylamide-2-methylpropane sulfonic acid

Info

Publication number
JPS54106427A
JPS54106427A JP1389778A JP1389778A JPS54106427A JP S54106427 A JPS54106427 A JP S54106427A JP 1389778 A JP1389778 A JP 1389778A JP 1389778 A JP1389778 A JP 1389778A JP S54106427 A JPS54106427 A JP S54106427A
Authority
JP
Japan
Prior art keywords
crystals
acetic acid
acrylamide
sulfonic acid
methylpropane sulfonic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1389778A
Other languages
English (en)
Other versions
JPS5653306B2 (ja
Inventor
Shunichi Doi
Masaki Kamogawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Rayon Co Ltd
Nitto Chemical Industry Co Ltd
Original Assignee
Mitsubishi Rayon Co Ltd
Nitto Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Rayon Co Ltd, Nitto Chemical Industry Co Ltd filed Critical Mitsubishi Rayon Co Ltd
Priority to JP1389778A priority Critical patent/JPS54106427A/ja
Priority to US06/008,114 priority patent/US4337215A/en
Priority to DE19792904444 priority patent/DE2904444A1/de
Publication of JPS54106427A publication Critical patent/JPS54106427A/ja
Publication of JPS5653306B2 publication Critical patent/JPS5653306B2/ja
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/01—Sulfonic acids
    • C07C309/02—Sulfonic acids having sulfo groups bound to acyclic carbon atoms
    • C07C309/03—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C309/13—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton containing nitrogen atoms, not being part of nitro or nitroso groups, bound to the carbon skeleton
    • C07C309/14—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton containing nitrogen atoms, not being part of nitro or nitroso groups, bound to the carbon skeleton containing amino groups bound to the carbon skeleton
    • C07C309/15—Sulfonic acids having sulfo groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton containing nitrogen atoms, not being part of nitro or nitroso groups, bound to the carbon skeleton containing amino groups bound to the carbon skeleton the nitrogen atom of at least one of the amino groups being part of any of the groups, X being a hetero atom, Y being any atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
JP1389778A 1978-02-09 1978-02-09 Purification of 2-acrylamide-2-methylpropane sulfonic acid Granted JPS54106427A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP1389778A JPS54106427A (en) 1978-02-09 1978-02-09 Purification of 2-acrylamide-2-methylpropane sulfonic acid
US06/008,114 US4337215A (en) 1978-02-09 1979-01-31 Process for purifying 2-acrylamido-2-methylpropanesulfonic acid
DE19792904444 DE2904444A1 (de) 1978-02-09 1979-02-06 Verfahren zum reinigen von 2-acrylamido-2-methylpropansulfonsaeure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1389778A JPS54106427A (en) 1978-02-09 1978-02-09 Purification of 2-acrylamide-2-methylpropane sulfonic acid

Publications (2)

Publication Number Publication Date
JPS54106427A true JPS54106427A (en) 1979-08-21
JPS5653306B2 JPS5653306B2 (ja) 1981-12-17

Family

ID=11845955

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1389778A Granted JPS54106427A (en) 1978-02-09 1978-02-09 Purification of 2-acrylamide-2-methylpropane sulfonic acid

Country Status (3)

Country Link
US (1) US4337215A (ja)
JP (1) JPS54106427A (ja)
DE (1) DE2904444A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015504441A (ja) * 2011-11-29 2015-02-12 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アクリルアミド−２−メチルプロパンスルホン酸（ａ）の塩を生成する方法、アクリルアミド−２−メチルプロパンスルホン酸（ａ）又はその塩、及びそれを用いた共重合体の製造方法
JP2020512330A (ja) * 2017-03-20 2020-04-23 エス・ペー・セー・エム・エスアー ２−アクリルアミド−２−メチルプロパンスルホン酸の水和された結晶形
JP2022051557A (ja) * 2020-09-18 2022-03-31 エスペーセーエム・エスアー アクリルアミド－２－メチル－２－プロパンスルホン酸の精製方法

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS54163524A (en) * 1978-06-12 1979-12-26 Nitto Chem Ind Co Ltd Production of high-purity 2-acrylamide-2- methylpropanesulfonic acid
US5080809A (en) * 1983-01-28 1992-01-14 Phillips Petroleum Company Polymers useful in the recovery and processing of natural resources
US5186257A (en) * 1983-01-28 1993-02-16 Phillips Petroleum Company Polymers useful in the recovery and processing of natural resources
JPH05508869A (ja) * 1991-06-03 1993-12-09 ザ ルブリゾル コーポレイション 精製したアクリルアミドスルホン酸モノマー誘導体の調製方法
US5510515A (en) * 1993-09-21 1996-04-23 Showa Denko K.K. Process for purifying polar vinyl compound
DE102004058071A1 (de) * 2004-12-01 2006-06-08 Basf Ag Verfahren zur Reinigung von polaren Vinylverbindungen
CN101066940B (zh) * 2007-06-06 2010-09-22 厦门长天企业有限公司 2-丙烯酰胺基-2-甲基丙磺酸的制备方法
CN102452965B (zh) * 2010-10-22 2013-08-14 中国石油化工股份有限公司 一种除去amps原料中阻聚剂的方法
CN102952045A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸粗产品的精制方法及其产品
CN102952051A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸及其精制方法
CN102952047A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸粗产品的精制方法及其产品
CN102952049A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸及其精制方法
CN102952046A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸粗产品的精制方法及其产品
CN102952050A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸及其精制方法
CN102952048A (zh) * 2011-08-30 2013-03-06 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸粗产品的精制方法及其产品
US9073826B2 (en) 2011-11-29 2015-07-07 Basf Se Process for preparing and purifying salts of acrylamido-2-methylpropanesulfonic acid
CN103664708B (zh) * 2012-09-07 2016-05-25 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸粗产品的精制方法及其产品
CN103086929B (zh) * 2013-02-04 2014-11-05 梅龙毅 一种制备固体丙烯酰胺基烷基磺酸盐的方法
CN103254102B (zh) 2013-06-06 2015-09-30 梅龙毅 一种纯化丙烯酰胺基烷基磺酸的方法
CN104230763B (zh) * 2013-06-07 2016-08-17 中国石油化工股份有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸的生产方法
FR3041344B1 (fr) * 2015-09-18 2019-12-13 S.P.C.M. Sa Procede d'obtention du monomere acide 2-acrylamido-2-methylpropanesulphonique et polymere comprenant ledit monomere
WO2017162545A1 (de) 2016-03-24 2017-09-28 Basf Se Verfahren zur herstellung von atbs und copolymeren daraus
FR3064005B1 (fr) 2017-03-20 2019-03-29 S.P.C.M. Sa Nouveau procede d'obtention de l'acide 2-acrylamido-2-methylpropane sulfonique
CN110857279B (zh) * 2018-08-22 2022-06-03 潍坊金石环保科技有限公司 一种2-丙烯酰胺基-2-甲基丙磺酸的制备方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1256650B (de) 1965-08-07 1967-12-21 Dr Dieter Arlt Verfahren zur Herstellung von N-acylierten 2-Amino-alkan-sulfonsaeuren-(1) bzw. von 2-Amino-alkan-sulfonsaeuren-(1)
US3506707A (en) * 1968-02-01 1970-04-14 Lubrizol Corp Preparation of acrylamidoalkanesulfonic acids
DE2523616B2 (de) 1975-05-28 1977-04-14 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von 2- acrylamido-2-alkylsulfonsaeuren

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015504441A (ja) * 2011-11-29 2015-02-12 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ アクリルアミド−２−メチルプロパンスルホン酸（ａ）の塩を生成する方法、アクリルアミド−２−メチルプロパンスルホン酸（ａ）又はその塩、及びそれを用いた共重合体の製造方法
JP2020512330A (ja) * 2017-03-20 2020-04-23 エス・ペー・セー・エム・エスアー ２−アクリルアミド−２−メチルプロパンスルホン酸の水和された結晶形
JP2022183267A (ja) * 2017-03-20 2022-12-08 エスペーセーエム・エスアー ２－アクリルアミド－２－メチルプロパンスルホン酸の水和された結晶形
JP2022051557A (ja) * 2020-09-18 2022-03-31 エスペーセーエム・エスアー アクリルアミド－２－メチル－２－プロパンスルホン酸の精製方法

Also Published As

Publication number Publication date
DE2904444A1 (de) 1979-09-13
US4337215A (en) 1982-06-29
JPS5653306B2 (ja) 1981-12-17

Similar Documents

Publication Publication Date Title
JPS54106427A (en) Purification of 2-acrylamide-2-methylpropane sulfonic acid
JPS5592400A (en) Purification of stevioside
NO890750D0 (no) Fremgangsmaate for fremstilling av oksydiftalsyreanhydrider
PT86074A (en) Process for preparing new substituted cephalosporin sulfones as anti-inflammatory and antidegenerative agents
IT1165252B (it) Procedimento di purificazione dell'acido ursodesossicolico attraverso nuovi derivati
ES8607937A1 (es) Un metodo de preparar un compuesto de beta-fluoropiridina
GB1519913A (en) Purification of naphthalene
Booth et al. 182. The synthesis of α-amino-acids. Part I. dl-Methionine
JPS55144422A (en) Purification of cis-dichlorodiammineplatinum(2)
JPS54106488A (en) Purification for d-penicillamine
JPS5212146A (en) Process for preparation of p- acetylaminobenzene-sufonylchloride
JPS53127891A (en) Crystallization of co-enzyme q
JPS53112837A (en) Method of isolation of alpha-phenylpropionic acid compound
MX9801569A (es) Procedimiento para preparar ester de acido glicidico trans-3-substituido opticamente activo.
GB1549533A (en) Process for the purification of phthalic anhydride
JPS5528951A (en) Crystallization of antibiotic substance
JPS5210214A (en) Process for recovery of methylmethacrylate dimer
JPS54145628A (en) Preparation of p-hydroxyphenylglycine
JPS54135760A (en) Purification of 19-norandrost-4-ene-3, 17-dione
JPS562999A (en) Purification of testosterone enanthate
JPS54119497A (en) N-acylamino-alpha-arylacetamidocephalosporin derivative
JPS51118754A (en) Process for preparation of anthraquinone
JPS5513245A (en) Preparation of m-aminoacetanilide
MX172536B (es) Proceso mejorado para separar y purificar el acido 6-aminopenicilanico (6-apa) preparado por hidrolisis enzimatica
JPS53130412A (en) Purification of gamma-oryzanol

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20031212

A711 Notification of change in applicant

Free format text: JAPANESE INTERMEDIATE CODE: A712

Effective date: 20040113

A131 Notification of reasons for refusal

Effective date: 20050524

Free format text: JAPANESE INTERMEDIATE CODE: A131

A977 Report on retrieval

Effective date: 20050518

Free format text: JAPANESE INTERMEDIATE CODE: A971007

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20050824

A602 Written permission of extension of time

Effective date: 20051007

Free format text: JAPANESE INTERMEDIATE CODE: A602

A521 Written amendment

Effective date: 20051107

Free format text: JAPANESE INTERMEDIATE CODE: A523

A72 Notification of change in name of applicant

Free format text: JAPANESE INTERMEDIATE CODE: A721

Effective date: 20051227

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20060523

A61 First payment of annual fees (during grant procedure)

Effective date: 20060529

Free format text: JAPANESE INTERMEDIATE CODE: A61

R150 Certificate of patent (=grant) or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090602

Year of fee payment: 3

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100602

Year of fee payment: 4

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100602

Year of fee payment: 4

FPAY Renewal fee payment (prs date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110602

Year of fee payment: 5

LAPS Cancellation because of no payment of annual fees