JPH0253500B2 - - Google Patents
Info
- Publication number
- JPH0253500B2 JPH0253500B2 JP1166473A JP16647389A JPH0253500B2 JP H0253500 B2 JPH0253500 B2 JP H0253500B2 JP 1166473 A JP1166473 A JP 1166473A JP 16647389 A JP16647389 A JP 16647389A JP H0253500 B2 JPH0253500 B2 JP H0253500B2
- Authority
- JP
- Japan
- Prior art keywords
- crystals
- liquid
- gallium
- container
- dam
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000013078 crystal Substances 0.000 claims abstract description 62
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims abstract description 43
- 229910052733 gallium Inorganic materials 0.000 claims abstract description 43
- 239000007788 liquid Substances 0.000 claims abstract description 36
- 238000000034 method Methods 0.000 claims abstract description 30
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims description 13
- 230000033001 locomotion Effects 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 4
- 230000005496 eutectics Effects 0.000 claims description 3
- 238000007790 scraping Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 239000002344 surface layer Substances 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims 1
- 230000000630 rising effect Effects 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000007711 solidification Methods 0.000 abstract description 2
- 230000008023 solidification Effects 0.000 abstract description 2
- 229910052751 metal Inorganic materials 0.000 description 9
- 239000002184 metal Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- 238000002425 crystallisation Methods 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 150000002739 metals Chemical class 0.000 description 5
- 230000008025 crystallization Effects 0.000 description 4
- 238000001640 fractional crystallisation Methods 0.000 description 4
- 239000012452 mother liquor Substances 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 229910052797 bismuth Inorganic materials 0.000 description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 2
- 239000012809 cooling fluid Substances 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- JBRZTFJDHDCESZ-UHFFFAOYSA-N AsGa Chemical compound [As]#[Ga] JBRZTFJDHDCESZ-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910005540 GaP Inorganic materials 0.000 description 1
- 229910001218 Gallium arsenide Inorganic materials 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000009529 body temperature measurement Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000003479 dental cement Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 239000006023 eutectic alloy Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- HZXMRANICFIONG-UHFFFAOYSA-N gallium phosphide Chemical compound [Ga]#P HZXMRANICFIONG-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 229910001338 liquidmetal Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B58/00—Obtaining gallium or indium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Acoustics & Sound (AREA)
- Physics & Mathematics (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8809503A FR2633640B1 (US07655688-20100202-C00086.png) | 1988-07-01 | 1988-07-01 | |
| FR8809503 | 1988-07-01 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0273929A JPH0273929A (ja) | 1990-03-13 |
| JPH0253500B2 true JPH0253500B2 (US07655688-20100202-C00086.png) | 1990-11-16 |
Family
ID=9368386
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1166473A Granted JPH0273929A (ja) | 1988-07-01 | 1989-06-28 | 部分固化によるガリウム精製法 |
Country Status (10)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0482300U (US07655688-20100202-C00086.png) * | 1990-11-28 | 1992-07-17 |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06136467A (ja) * | 1992-10-28 | 1994-05-17 | Sumitomo Chem Co Ltd | 金属ガリウムの精製方法 |
| JP3909364B2 (ja) * | 1998-10-29 | 2007-04-25 | Ｄｏｗａエレクトロニクス株式会社 | ガリウムの精製方法および装置 |
| JP2007270237A (ja) * | 2006-03-31 | 2007-10-18 | Dowa Holdings Co Ltd | ガリウムの精製方法 |
| JP4916203B2 (ja) * | 2006-03-31 | 2012-04-11 | Ｄｏｗａホールディングス株式会社 | ガリウムの精製方法 |
| CN100460534C (zh) * | 2007-06-22 | 2009-02-11 | 东南大学 | 一种高纯镓的制备方法 |
| CN101497947B (zh) * | 2008-01-29 | 2010-10-13 | 中国铝业股份有限公司 | 一种高纯镓生产的粗镓预处理除杂质装置 |
| JP4899034B2 (ja) * | 2008-02-14 | 2012-03-21 | Ｄｏｗａエレクトロニクス株式会社 | 化合物半導体作成用のガリウム原料 |
| CN102071328A (zh) * | 2010-12-09 | 2011-05-25 | 中国铝业股份有限公司 | 一种树脂吸附法生产的次品镓的提纯方法 |
| CN102618735B (zh) * | 2012-04-23 | 2013-05-08 | 南京金美镓业有限公司 | 一种去除金属镓中杂质铋的方法 |
| CN106048262A (zh) * | 2016-08-17 | 2016-10-26 | 广东先导稀材股份有限公司 | 一种镓的提纯方法及装置 |
| CN110938755B (zh) * | 2019-11-20 | 2021-06-11 | 中南大学 | 镓提纯装置及方法 |
| CN113373325A (zh) * | 2021-06-07 | 2021-09-10 | 东阿阿华医疗科技有限公司 | 一种镓合金液高真空蒸馏提纯方法 |
| CN113652553B (zh) * | 2021-08-19 | 2022-07-05 | 武汉拓材科技有限公司 | 一种高纯镓的生产装置及方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3088853A (en) * | 1959-11-17 | 1963-05-07 | Texas Instruments Inc | Method of purifying gallium by recrystallization |
| US3211547A (en) * | 1961-02-10 | 1965-10-12 | Aluminum Co Of America | Treatment of molten aluminum |
| FR1594154A (US07655688-20100202-C00086.png) * | 1968-12-06 | 1970-06-01 | ||
| US4221590A (en) * | 1978-12-26 | 1980-09-09 | Aluminum Company Of America | Fractional crystallization process |
| FR2524489A1 (fr) * | 1982-03-30 | 1983-10-07 | Pechiney Aluminium | Procede de purification de metaux par segregation |
| JPS5976837A (ja) * | 1982-10-27 | 1984-05-02 | Mitsubishi Keikinzoku Kogyo Kk | 金属の純化装置 |
| JPS60228625A (ja) * | 1984-04-26 | 1985-11-13 | Nippon Light Metal Co Ltd | 溶融金属の濾過方法 |
| FR2592663B1 (fr) * | 1986-01-06 | 1992-07-24 | Pechiney Aluminium | Procede ameliore de purification de metaux par cristallisation fractionnee |
-
1988
- 1988-07-01 FR FR8809503A patent/FR2633640B1/fr not_active Expired - Fee Related
-
1989
- 1989-06-27 DE DE8989420231T patent/DE68901500D1/de not_active Expired - Fee Related
- 1989-06-27 EP EP89420231A patent/EP0349449B1/fr not_active Expired - Lifetime
- 1989-06-27 AT AT89420231T patent/ATE76106T1/de not_active IP Right Cessation
- 1989-06-28 CN CN89104310A patent/CN1039064A/zh active Pending
- 1989-06-28 JP JP1166473A patent/JPH0273929A/ja active Granted
- 1989-06-28 AU AU37129/89A patent/AU608165B2/en not_active Ceased
- 1989-06-30 RU SU894614437A patent/RU1782247C/ru active
- 1989-06-30 HU HU893342A patent/HU205392B/hu not_active IP Right Cessation
-
1992
- 1992-05-14 GR GR910402169T patent/GR3004592T3/el unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0482300U (US07655688-20100202-C00086.png) * | 1990-11-28 | 1992-07-17 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0349449B1 (fr) | 1992-05-13 |
| HU205392B (en) | 1992-04-28 |
| AU3712989A (en) | 1990-01-04 |
| HUT53679A (en) | 1990-11-28 |
| FR2633640B1 (US07655688-20100202-C00086.png) | 1991-04-19 |
| AU608165B2 (en) | 1991-03-21 |
| EP0349449A1 (fr) | 1990-01-03 |
| CN1039064A (zh) | 1990-01-24 |
| DE68901500D1 (de) | 1992-06-17 |
| ATE76106T1 (de) | 1992-05-15 |
| FR2633640A1 (US07655688-20100202-C00086.png) | 1990-01-05 |
| RU1782247C (ru) | 1992-12-15 |
| JPH0273929A (ja) | 1990-03-13 |
| GR3004592T3 (US07655688-20100202-C00086.png) | 1993-04-28 |
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