JPH0138438B2 - - Google Patents

Info

Publication number
JPH0138438B2
JPH0138438B2 JP59044180A JP4418084A JPH0138438B2 JP H0138438 B2 JPH0138438 B2 JP H0138438B2 JP 59044180 A JP59044180 A JP 59044180A JP 4418084 A JP4418084 A JP 4418084A JP H0138438 B2 JPH0138438 B2 JP H0138438B2
Authority
JP
Japan
Prior art keywords
trimethylcyclohexyl
trans
hexan
cis
composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP59044180A
Other languages
English (en)
Japanese (ja)
Other versions
JPS606657A (ja
Inventor
Shuruteeerute Kaaruuhainritsuhi
Oorofu Gyuntaa
Rushian Myuraa Berunaaru
Kurausu Giirushu Uorufugangu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Firmenich SA
Original Assignee
Firmenich SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Firmenich SA filed Critical Firmenich SA
Publication of JPS606657A publication Critical patent/JPS606657A/ja
Publication of JPH0138438B2 publication Critical patent/JPH0138438B2/ja
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • C07C29/175—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds with simultaneous reduction of an oxo group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/13—Monohydroxylic alcohols containing saturated rings
    • C07C31/133—Monohydroxylic alcohols containing saturated rings monocyclic
    • C07C31/135—Monohydroxylic alcohols containing saturated rings monocyclic with a five or six-membered rings; Naphthenic alcohols
    • C07C31/1355—Monohydroxylic alcohols containing saturated rings monocyclic with a five or six-membered rings; Naphthenic alcohols with a six-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C33/00—Unsaturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C33/05—Alcohols containing rings other than six-membered aromatic rings
    • C07C33/14—Alcohols containing rings other than six-membered aromatic rings containing six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
    • C07C403/06—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by singly-bound oxygen atoms
    • C07C403/08—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by singly-bound oxygen atoms by hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
    • C07C403/14—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by doubly-bound oxygen atoms
    • C07C403/16—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by doubly-bound oxygen atoms not being part of —CHO groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/28—Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings
    • C07C47/32—Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings with a six-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
    • C07C49/105—Saturated compounds containing keto groups bound to acyclic carbon atoms containing rings
    • C07C49/11—Saturated compounds containing keto groups bound to acyclic carbon atoms containing rings monocyclic
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/09—Geometrical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP59044180A 1983-03-09 1984-03-09 調合香料、ベース香料およびエッセンスの香気特性を改善または増強する方法 Granted JPS606657A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH125983 1983-03-09
CH1259/83-6 1983-03-09

Publications (2)

Publication Number Publication Date
JPS606657A JPS606657A (ja) 1985-01-14
JPH0138438B2 true JPH0138438B2 (en, 2012) 1989-08-14

Family

ID=4206202

Family Applications (2)

Application Number Title Priority Date Filing Date
JP59044180A Granted JPS606657A (ja) 1983-03-09 1984-03-09 調合香料、ベース香料およびエッセンスの香気特性を改善または増強する方法
JP61039359A Granted JPS61191636A (ja) 1983-03-09 1986-02-26 トランス―１―（２，６，６―トリメチルシクロヘキシル）―ヘキサン―３―オールを含有する組成物の製造法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP61039359A Granted JPS61191636A (ja) 1983-03-09 1986-02-26 トランス―１―（２，６，６―トリメチルシクロヘキシル）―ヘキサン―３―オールを含有する組成物の製造法

Country Status (4)

Country Link
US (2) US4623750A (en, 2012)
EP (1) EP0118809B1 (en, 2012)
JP (2) JPS606657A (en, 2012)
DE (1) DE3471092D1 (en, 2012)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0118809B1 (en) * 1983-03-09 1988-05-11 Firmenich Sa Composition essentially consisting of trans-1-(2,6,6-trimethylcyclohexyl)-hexan-3-ol, utilization of same and process for its preparation; cycloaliphatic ketone and alcohol intermediates
EP0255904B1 (fr) * 1986-08-06 1991-01-02 Firmenich Sa Procédé pour la préparation de dihydrocyclocitral
FR2623805B1 (fr) * 1987-12-01 1990-04-13 Rhone Poulenc Sante Procede de preparation de la vitamine a
US6054426A (en) * 1990-05-16 2000-04-25 Firmenich Sa Optically active aliphatic alcohols and their use as perfuming ingredients
EP0457022B1 (fr) * 1990-05-16 1994-08-03 Firmenich Sa Alcools aliphatiques optiquement actifs nouveaux et leur utilisation à titre d'ingrédients parfumants
US5250512A (en) * 1990-05-17 1993-10-05 Takasago International Corporation Propanol derivatives and perfumes containing the same
JPH0725709B2 (ja) * 1990-05-17 1995-03-22 高砂香料工業株式会社 新規なプロパノール誘導体及びそれを有効成分とする香料
USRE37159E1 (en) * 1990-05-17 2001-05-01 Takasago International Corporation Propanol derivatives and perfumes containing the same
US5329053A (en) * 1992-09-03 1994-07-12 Givaudan-Roure Corporation Process for the manufacture of known odorants
EP1053988B1 (en) 1998-02-02 2008-12-31 Takasago International Corporation Trimethylcyclohexane derivatives and melanin-formation inhibitors and perfume-holding agents with the use of the same
JP2001127516A (ja) 1999-10-25 2001-05-11 Nec Corp 携帯無線機
US6376708B1 (en) 2000-04-11 2002-04-23 Monsanto Technology Llc Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
DE10062771A1 (de) * 2000-12-15 2002-07-11 Haarmann & Reimer Gmbh Verfahren zur Herstellung von 1-(2,2,6-Trimethylcyclohexyl)-3-alkanolen
CA2463776A1 (en) 2001-10-18 2003-04-24 Monsanto Technology Llc Process and catalyst for dehydrogenating primary alcohols to make carboxylic acid salts
DE10243466A1 (de) * 2002-09-19 2004-04-08 Symrise Gmbh & Co. Kg Verfahren zur Herstellung von Trimethylcyclohexyl-alkan-3-olen mit einem hohen Anteil an trans-Isomeren
DE102005036672A1 (de) 2005-08-04 2007-02-08 Symrise Gmbh & Co. Kg Verfahren zur Herstellung von 1-(2,2,6-Trimethylcyclohexyl)-hexan-3-ol
CN101636373B (zh) * 2007-03-22 2013-05-22 帝斯曼知识产权资产管理有限公司 用于制备木材酮的新方法
CN103467247B (zh) * 2013-10-09 2015-09-09 浦城县永芳香料科技有限公司 一种制备特木倍醇的方法
GB2528480A (en) * 2014-07-23 2016-01-27 Givaudan Sa Improvements in or relating to organic compounds
MX2017006545A (es) 2014-11-18 2017-08-09 Basf Se Proceso para la preparacion de 1-(2,6,6-trimetilciclohexil)-alcan- 3-oles.

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3928645A (en) * 1973-08-07 1975-12-23 Int Flavors & Fragrances Inc Enhancing red-berry flavor with 4-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-butanone and 4-(6,6-dimethyl-2-methylene-3-cyclohexen-1-yl)-2-butanone
US3928248A (en) 1974-04-17 1975-12-23 Int Flavors & Fragrances Inc Fragrance materials containing 4-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-butanol and/or 4-(6,6-dimethyl-2-methylene-3-cyclo-hexen-1-yl)-2-butanol, and/or acetals thereof, and methods for producing same
DE2455761C2 (de) * 1974-11-26 1982-04-22 Haarmann & Reimer Gmbh, 3450 Holzminden Verwendung von hydrierten Methyljononen und deren Derivaten als Riechstoffe, Verfahren zu ihrer Herstellung und neue hydrierte Methyljononderivate
US4088681A (en) 1975-12-27 1978-05-09 Basf Aktiengesellschaft Substituted 1-alkenynyl-cyclohexanols and -cyclohexenes and processes for their preparation
CH601218A5 (en, 2012) * 1976-07-15 1978-06-30 Hoffmann La Roche
SU739055A1 (ru) * 1978-02-17 1980-06-05 Всесоюзный научно-исследовательский институт синтетических и натуральных душистых веществ Способ получени псевдоиралии
DE2807584C3 (de) 1978-02-22 1981-05-07 Dragoco Gerberding & Co Gmbh, 3450 Holzminden Fixateur für Parfümkompositionen
US4313855A (en) 1978-02-22 1982-02-02 Dragoco Gerberding & Co. Gmbh Fixative for perfume compositions
US4169109A (en) * 1978-08-10 1979-09-25 International Flavors & Fragrances Inc. Process for preparing ketones using zinc acetate condensation catalysts, products produced thereby and organoleptic uses of same
US4311860A (en) 1978-11-24 1982-01-19 Givaudan Corporation Microbiological transformations of ionone compounds
US4324704A (en) 1978-12-15 1982-04-13 International Flavors & Fragrances Inc. Process for hydrogenation of damascenone, products produced thereby and organoleptic uses of said products
US4460792A (en) * 1981-09-07 1984-07-17 Firmenich S.A. Process for the preparation of delta- and epsilon-damascones
EP0118809B1 (en) * 1983-03-09 1988-05-11 Firmenich Sa Composition essentially consisting of trans-1-(2,6,6-trimethylcyclohexyl)-hexan-3-ol, utilization of same and process for its preparation; cycloaliphatic ketone and alcohol intermediates
EP0118817B1 (en) * 1983-03-11 1986-04-02 Firmenich Sa Process for the preparation of an isomeric composition of 1-(2,6,6-trimethylcyclohexyl)-hexan-3-ol, use of the obtained composition and intermediate carbinols

Also Published As

Publication number Publication date
EP0118809B1 (en) 1988-05-11
EP0118809A3 (en) 1986-07-30
JPS606657A (ja) 1985-01-14
US4711875A (en) 1987-12-08
JPS61191636A (ja) 1986-08-26
US4623750A (en) 1986-11-18
EP0118809A2 (en) 1984-09-19
JPH0380780B2 (en, 2012) 1991-12-26
DE3471092D1 (en) 1988-06-16

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Legal Events

Date Code Title Description
EXPY Cancellation because of completion of term