JPH0135769B2 - - Google Patents
Info
- Publication number
- JPH0135769B2 JPH0135769B2 JP56157808A JP15780881A JPH0135769B2 JP H0135769 B2 JPH0135769 B2 JP H0135769B2 JP 56157808 A JP56157808 A JP 56157808A JP 15780881 A JP15780881 A JP 15780881A JP H0135769 B2 JPH0135769 B2 JP H0135769B2
- Authority
- JP
- Japan
- Prior art keywords
- graphite
- mgf
- stage
- intercalation compound
- ternary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 105
- 229910002804 graphite Inorganic materials 0.000 claims description 93
- 239000010439 graphite Substances 0.000 claims description 93
- 150000001875 compounds Chemical class 0.000 claims description 75
- 238000009830 intercalation Methods 0.000 claims description 57
- 230000002687 intercalation Effects 0.000 claims description 55
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 30
- 229910052731 fluorine Inorganic materials 0.000 claims description 30
- 239000011737 fluorine Substances 0.000 claims description 30
- 229910001635 magnesium fluoride Inorganic materials 0.000 claims description 11
- ORUIBWPALBXDOA-UHFFFAOYSA-L magnesium fluoride Chemical compound [F-].[F-].[Mg+2] ORUIBWPALBXDOA-UHFFFAOYSA-L 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 6
- 239000004020 conductor Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 description 34
- 239000007789 gas Substances 0.000 description 13
- 229910052799 carbon Inorganic materials 0.000 description 11
- 229910016569 AlF 3 Inorganic materials 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- 238000002441 X-ray diffraction Methods 0.000 description 7
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 6
- LVTJOONKWUXEFR-FZRMHRINSA-N protoneodioscin Natural products O(C[C@@H](CC[C@]1(O)[C@H](C)[C@@H]2[C@]3(C)[C@H]([C@H]4[C@@H]([C@]5(C)C(=CC4)C[C@@H](O[C@@H]4[C@H](O[C@H]6[C@@H](O)[C@@H](O)[C@@H](O)[C@H](C)O6)[C@@H](O)[C@H](O[C@H]6[C@@H](O)[C@@H](O)[C@@H](O)[C@H](C)O6)[C@H](CO)O4)CC5)CC3)C[C@@H]2O1)C)[C@H]1[C@H](O)[C@H](O)[C@H](O)[C@@H](CO)O1 LVTJOONKWUXEFR-FZRMHRINSA-N 0.000 description 6
- QLOAVXSYZAJECW-UHFFFAOYSA-N methane;molecular fluorine Chemical compound C.FF QLOAVXSYZAJECW-UHFFFAOYSA-N 0.000 description 5
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 230000000737 periodic effect Effects 0.000 description 4
- 239000002296 pyrolytic carbon Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000007770 graphite material Substances 0.000 description 3
- 229910021382 natural graphite Inorganic materials 0.000 description 3
- 238000001228 spectrum Methods 0.000 description 3
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910021383 artificial graphite Inorganic materials 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910017488 Cu K Inorganic materials 0.000 description 1
- 229910017541 Cu-K Inorganic materials 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 229910003110 Mg K Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- -1 aluminum halides Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000011889 copper foil Substances 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 238000005087 graphitization Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910001512 metal fluoride Inorganic materials 0.000 description 1
- 238000006053 organic reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000002006 petroleum coke Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000002411 thermogravimetry Methods 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Carbon And Carbon Compounds (AREA)
- Conductive Materials (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56157808A JPS5860608A (ja) | 1981-10-03 | 1981-10-03 | 黒鉛とフッ化マグネシウム及びフッ素との３成分系黒鉛層間化合物，及びその製造方法ならびにそれから成る電導材料 |
| US06/394,530 US4477374A (en) | 1981-10-03 | 1982-07-02 | Ternary intercalation compound of a graphite with a metal fluoride and fluorine, a process for producing the same, and an electrically conductive material comprising the ternary intercalation compound |
| GB08219748A GB2107296B (en) | 1981-10-03 | 1982-07-08 | A ternary intercalation compound of graphite with a metal fluoride and fluorine a process for producing the same and an electrically conductive material comprising the ternary intercalation compound |
| IT22633/82A IT1152305B (it) | 1981-10-03 | 1982-07-29 | Composto ternario intercalare di grafite con un fluoruro metallico e fluoro,procedimento per la sua produzione e materiale elettroconduttore comprendente il composto ternario intercalare |
| NL8203056A NL8203056A (nl) | 1981-10-03 | 1982-07-30 | Nieuwe intercalaire verbinding van grafiet. |
| FR8213413A FR2513981B1 (fr) | 1981-10-03 | 1982-07-30 | Compose ternaire d'intercalation d'un graphite avec un fluorure d'un metal et du fluor, procede pour sa production et materiau electriquement conducteur le contenant |
| DE3235596A DE3235596A1 (de) | 1981-10-03 | 1982-09-25 | Ternaere einlagerungsverbindung, verfahren zu ihrer herstellung und elektrisch leitendes material, enthaltend die verbindung |
| NL8603066A NL8603066A (nl) | 1981-10-03 | 1986-12-01 | Nieuwe intercalatieverbindingen van grafiet. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56157808A JPS5860608A (ja) | 1981-10-03 | 1981-10-03 | 黒鉛とフッ化マグネシウム及びフッ素との３成分系黒鉛層間化合物，及びその製造方法ならびにそれから成る電導材料 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5860608A JPS5860608A (ja) | 1983-04-11 |
| JPH0135769B2 true JPH0135769B2 (ko) | 1989-07-27 |
Family
ID=15657733
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP56157808A Granted JPS5860608A (ja) | 1981-10-03 | 1981-10-03 | 黒鉛とフッ化マグネシウム及びフッ素との３成分系黒鉛層間化合物，及びその製造方法ならびにそれから成る電導材料 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5860608A (ko) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2598792B2 (ja) * | 1987-08-27 | 1997-04-09 | 日機装 株式会社 | 導電性インク |
-
1981
- 1981-10-03 JP JP56157808A patent/JPS5860608A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5860608A (ja) | 1983-04-11 |
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